Holdings: C-C coupling reactions catalyzed by supported palladium in liquid phase

C-C coupling reactions catalyzed by supported palladium in liquid phase:

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Bibliographic Details
Main Author:	Soomro, Saeeda 1975- (Author)
Format:	Thesis Book
Language:	English
Published:	München Verl. Dr. Hut 2009
Edition:	1. Aufl.
Series:	Anorganische Chemie
Subjects:	Palladiumkomplexe Flüssiger Zustand Reaktionsmechanismus Kohlenstoff-Kohlenstoff-Bindung Kupplungsreaktion Heterogene Katalyse Palladiumverbindungen Palladiumorganische Verbindungen Hochschulschrift
Online Access:	Inhaltsverzeichnis
Physical Description:	126 S. Ill., graph. Darst. 210 mm x 148 mm, 191 gr.
ISBN:	9783868531251

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Record in the Search Index

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adam_text	2.2.6 PD-LEACHING INVESTIGATIONS AT 65 C 44 TABLE OF CONTENTS 1. SUPPORTED PALLADIUM CATALYSTS FOR C-C COUPLING REACTIONS: PROBLEMS AND PERSPECTIVES 1 1.1 GENERAL ITRODUCTION 2 1.2 SUZUKI COUPLING REACTION 5 1.2.1 MECHANISM 6 1.2.2 CATALYTIC SYSTEMS 7 1.2.2.1 LIGAND-FREE SYSTEMS 7 1.2.2.2 HOMOGENEOUS CATALYSTS 8 1.2.2.3 SUPPORTED CATALYSTS 9 1.2.3 SUZUKI COUPLING REACTIONS IN WATEI 13 1.3 OXIDATIVE C-C COUPLING REACTIONS 16 1.3.1 MECHANISTIC DETAILS 17 1.3.2 CATALYTIC SYSTEMS FOR OXIDATIVE COUPLING OF BENZENE (DERIVATIVES) WITH OLEFINS 19 1.4 AIM OF WORK 23 2. SUZUKI COUPLING REACTIONS 25 2.1 GENERAL INTRODUCTION 26 2.2 SUZUKI COUPLING REACTIONS IN NMP/WATER 28 2.2.1 SUZUKI REACTIONS OF ARYL BROMIDES AT 120 C 28 2.2.1.1 NON-TREATED VS. TREATED CATALYSTS 28 2.2.1.2 COMPARISON OF DIFFERENT SUPPORTED MATERIALS 29 2.2.1.3 RECYCLING EXPERIMENTS 31 2.2.2 SUZUKI REACTIONS OF ARYL CHLORIDES AT 120 C 31 2.2.3 PD-LEACHING INVESTIGATIONS AT 120 C 34 2.2.4 SUZUKI REACTIONS OF ARYL BROMIDES AT 65 C 36 2.2.4.1 COMPARISON OF DIFFERENT PD PRECURSORS 36 2.2.4.2 INFLUENCE OF ADDED WATER 37 2.2.4.3 INFLUENCE OF THE CATALYST AMOUNT AND PRETREATMENT 38 2.2.4.4 SCOPE OF PD/AL2U3 CATALYZED SUZUKI COUPLING REACTIONS AT 65 C... 40 2.2.5 SUZUKI REACTIONS OF ARYL CHLORIDES AT 65 C 42 2.2.5.1 INFLUENCE OF CATALYST AMOUNT AND PRETREATMENT 43 BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/99573576X DIGITALISIERT DURCH TABLE OF CONTENTS 2.2.6.1 KINETIC EXPERIMENTS ON CORRELATION OF PD-LEACHING AND CONVERSION...44 2.2.6.2 PALLADIUM LEACHING AS FUNCTION OF REACTION PARAMETERS 48 2.2.7 11 B NMR EXPERIMENT 51 2.2.8 TEM CHARACTERIZATION OF THE CATALYST BEFORE AND AFTER SUZUKI COUPLING REACTIONS 54 2.2.9 CONCLUSIVE REMARKS: SUZUKI COUPLING REACTIONS IN NMP/WATER AT 65 C..56 2.3 SUZUKI COUPLING REACTIONS IN PURE WATER 58 2.3.1 GENERAL INTRODUCTION 58 2.3.2 PD/C CATALYZED SUZUKI COUPLING REACTIONS IN WATER UNDER MILD CONDITIONS 59 2.3.2.1 VARIATION OF AMOUNT OF WATER 59 2.3.2.2 SUBSTRATE SCOPE FOR PD/C CATALYZED SUZUKI COUPLING REACTIONS OF ARYL BROMIDES IN WATER 60 2.3.3 PD/MOX CATALYZED SUZUKI COUPLING REACTIONS AT 65 C 60 2.3.3.1 INFLUENCE OF METAL OXIDE SUPPORT 61 2.3.3.2 VARIATION OF CATALYST AMOUNT 65 2.3.3.3 OPTIMIZATION OF REACTION PARAMETERS 65 2.3.3.4 PD/MODIFIED METAL OXIDES CATALYZED SUZUKI COUPLING REACTIONS OF ARYL BROMIDES IN WATER 66 2.3.4 CONCLUSIVE REMARKS: SUZUKI COUPLING REACTIONS IN WATER 67 3. OXIDATIVE COUPLING REACTIONS 69 3.1 GENERAL INTRODUCTION 70 3.1.1 SCREENING OF OXIDANTS AT DIFFERENT TEMPERATURES 71 3.1.2 TIME-DEPENDANT CORRELATION OF ACTIVITY AND SELECTIVITY IN OXIDATIVE COUPLING REACTIONS 73 3.1.3 INFLUENCE OF MOLAR EXCESS OF BENZENE AND REACTION ATMOSPHERE 74 3.1.4 VARIATION OF OXIDANT AMOUNT 76 3.1.5 VARYING THE PD-SOURCE IN OXIDATIVE COUPLING REACTIONS 78 3.1. TABLE OF CONTENTS 3.2.2 VARIATION OF PD SOURCES 83 3.2.3 VARIATION OF OXIDANT AMOUNT 84 3.2.4 VARIATION OF LIGAND AND BASE 85 3.2.5 CONCLUSIVE REMARKS: TEMPO AS OXIDIZING AGENT 87 3.3 INVESTIGATIONS ON SOME OTHER CATALYTIC SYSTEMS FOR OXIDATIVE COUPLING REACTIONS 88 3.3.1 PD/HPA CATALYTIC SYSTEM 88 3.3.2 PEROXIDES (TBUOOH OR H 2 O 2 ) AS OXIDANTS 90 4. SUMMARY 91 5. ZUSAMMENFASSUNG 97 6. EXPERIMENTAL SECTION 103 6.1 GENERAL REMARKS 104 6.2 ANALYTICAL METHODS 104 6.2.1 ELEMENTAL ANALYSIS 104 6.2.2 GAS CHROMATOGRAPHY 104 6.2.3 NMR SPECTROSCOPY 105 6.2.4 EPR SPECTROSCOPY 106 6.2.5 TRANSMISSION ELECTRON MICROSCOPY 106 6.3 CATALYST PREPARATION 106 6.3.1 MODIFICATION OF AI2O3 SURFACE (AI2O3-C8 PREPARATION) 106 6.3.2 PREPARATION OF 1 WT% PD/MO X 108 6.3.3 PREPARATION OF 1 WT% PD/T2000 (AMPHIPHILIC SUPPORT) 108 6.3.4 PREPARATION OF PD/T805 AND PD/AI 2 O 3 -C 8 (HYDROPHOBIC SUPPORTS) 108 6.3.5 PRE-TREATMENT OF PD/AI 2 O 3 CATALYST 108 6.3.6 PREPARATION OF 1 WT% PD/NAY 109 6.3.7 PD/C CATALYST 109 6.4 GENERAL PROCEDURES FOR CATALYTIC TESTS 109 6.4.1 SUZUKI COUPLING REACTIONS OF ARYL HALIDES IN NMP/WATER AT 120 C 109 6.4. TABLE OF CONTENTS 6.4.8 OXIDATIVE COUPLING OF BENZENE AND STYRENE 113 6.5 STRUCTURAL DATA OF REACTION PRODUCTS 113 7. APPENDIX 117 8. REFERENCES 119
any_adam_object	1
author	Soomro, Saeeda 1975-
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classification_tum	CHE 609d CHE 167d CHE 620d
ctrlnum	(OCoLC)642992240 (DE-599)DNB99573576X
dewey-full	547.215 546.6362
dewey-hundreds	500 - Natural sciences and mathematics
dewey-ones	547 - Organic chemistry 546 - Inorganic chemistry
dewey-raw	547.215 546.6362
dewey-search	547.215 546.6362
dewey-sort	3547.215
dewey-tens	540 - Chemistry and allied sciences
discipline	Chemie / Pharmazie Physik Chemie
edition	1. Aufl.
format	Thesis Book
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physical	126 S. Ill., graph. Darst. 210 mm x 148 mm, 191 gr.
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spelling	Soomro, Saeeda 1975- Verfasser (DE-588)13887557X aut C-C coupling reactions catalyzed by supported palladium in liquid phase Saeeda Shahid Soomro 1. Aufl. München Verl. Dr. Hut 2009 126 S. Ill., graph. Darst. 210 mm x 148 mm, 191 gr. txt rdacontent n rdamedia nc rdacarrier Anorganische Chemie Zugl.: München, Techn. Univ., Diss., 2009 Palladiumkomplexe (DE-588)4223138-3 gnd rswk-swf Flüssiger Zustand (DE-588)4336025-7 gnd rswk-swf Reaktionsmechanismus (DE-588)4177123-0 gnd rswk-swf Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 gnd rswk-swf Kupplungsreaktion (DE-588)4166199-0 gnd rswk-swf Heterogene Katalyse (DE-588)4123377-3 gnd rswk-swf Palladiumverbindungen (DE-588)4173148-7 gnd rswk-swf Palladiumorganische Verbindungen (DE-588)4353954-3 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Kupplungsreaktion (DE-588)4166199-0 s Palladiumverbindungen (DE-588)4173148-7 s Heterogene Katalyse (DE-588)4123377-3 s Flüssiger Zustand (DE-588)4336025-7 s DE-604 Palladiumkomplexe (DE-588)4223138-3 s Reaktionsmechanismus (DE-588)4177123-0 s 1\p DE-604 Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 s Palladiumorganische Verbindungen (DE-588)4353954-3 s 2\p DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017719461&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk
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subject_GND	(DE-588)4223138-3 (DE-588)4336025-7 (DE-588)4177123-0 (DE-588)4164549-2 (DE-588)4166199-0 (DE-588)4123377-3 (DE-588)4173148-7 (DE-588)4353954-3 (DE-588)4113937-9
title	C-C coupling reactions catalyzed by supported palladium in liquid phase
title_auth	C-C coupling reactions catalyzed by supported palladium in liquid phase
title_exact_search	C-C coupling reactions catalyzed by supported palladium in liquid phase
title_full	C-C coupling reactions catalyzed by supported palladium in liquid phase Saeeda Shahid Soomro
title_fullStr	C-C coupling reactions catalyzed by supported palladium in liquid phase Saeeda Shahid Soomro
title_full_unstemmed	C-C coupling reactions catalyzed by supported palladium in liquid phase Saeeda Shahid Soomro
title_short	C-C coupling reactions catalyzed by supported palladium in liquid phase
title_sort	c c coupling reactions catalyzed by supported palladium in liquid phase
topic	Palladiumkomplexe (DE-588)4223138-3 gnd Flüssiger Zustand (DE-588)4336025-7 gnd Reaktionsmechanismus (DE-588)4177123-0 gnd Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 gnd Kupplungsreaktion (DE-588)4166199-0 gnd Heterogene Katalyse (DE-588)4123377-3 gnd Palladiumverbindungen (DE-588)4173148-7 gnd Palladiumorganische Verbindungen (DE-588)4353954-3 gnd
topic_facet	Palladiumkomplexe Flüssiger Zustand Reaktionsmechanismus Kohlenstoff-Kohlenstoff-Bindung Kupplungsreaktion Heterogene Katalyse Palladiumverbindungen Palladiumorganische Verbindungen Hochschulschrift
url	http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017719461&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT soomrosaeeda cccouplingreactionscatalyzedbysupportedpalladiuminliquidphase

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