C-C coupling reactions catalyzed by supported palladium in liquid phase:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
München
Verl. Dr. Hut
2009
|
| Ausgabe: | 1. Aufl. |
| Schriftenreihe: | Anorganische Chemie
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 126 S. Ill., graph. Darst. 210 mm x 148 mm, 191 gr. |
| ISBN: | 9783868531251 |
Internformat
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Datensatz im Suchindex
| _version_ | 1804139357865508864 |
|---|---|
| adam_text | 2.2.6 PD-LEACHING INVESTIGATIONS AT 65 C 44 TABLE OF CONTENTS 1.
SUPPORTED PALLADIUM CATALYSTS FOR C-C COUPLING REACTIONS: PROBLEMS AND
PERSPECTIVES 1 1.1 GENERAL ITRODUCTION 2 1.2 SUZUKI COUPLING REACTION 5
1.2.1 MECHANISM 6 1.2.2 CATALYTIC SYSTEMS 7 1.2.2.1 LIGAND-FREE SYSTEMS
7 1.2.2.2 HOMOGENEOUS CATALYSTS 8 1.2.2.3 SUPPORTED CATALYSTS 9 1.2.3
SUZUKI COUPLING REACTIONS IN WATEI 13 1.3 OXIDATIVE C-C COUPLING
REACTIONS 16 1.3.1 MECHANISTIC DETAILS 17 1.3.2 CATALYTIC SYSTEMS FOR
OXIDATIVE COUPLING OF BENZENE (DERIVATIVES) WITH OLEFINS 19 1.4 AIM OF
WORK 23 2. SUZUKI COUPLING REACTIONS 25 2.1 GENERAL INTRODUCTION 26 2.2
SUZUKI COUPLING REACTIONS IN NMP/WATER 28 2.2.1 SUZUKI REACTIONS OF ARYL
BROMIDES AT 120 C 28 2.2.1.1 NON-TREATED VS. TREATED CATALYSTS 28
2.2.1.2 COMPARISON OF DIFFERENT SUPPORTED MATERIALS 29 2.2.1.3 RECYCLING
EXPERIMENTS 31 2.2.2 SUZUKI REACTIONS OF ARYL CHLORIDES AT 120 C 31
2.2.3 PD-LEACHING INVESTIGATIONS AT 120 C 34 2.2.4 SUZUKI REACTIONS OF
ARYL BROMIDES AT 65 C 36 2.2.4.1 COMPARISON OF DIFFERENT PD PRECURSORS
36 2.2.4.2 INFLUENCE OF ADDED WATER 37 2.2.4.3 INFLUENCE OF THE CATALYST
AMOUNT AND PRETREATMENT 38 2.2.4.4 SCOPE OF PD/AL2U3 CATALYZED SUZUKI
COUPLING REACTIONS AT 65 C... 40 2.2.5 SUZUKI REACTIONS OF ARYL
CHLORIDES AT 65 C 42 2.2.5.1 INFLUENCE OF CATALYST AMOUNT AND
PRETREATMENT 43 BIBLIOGRAFISCHE INFORMATIONEN HTTP://D-NB.INFO/99573576X
DIGITALISIERT DURCH TABLE OF CONTENTS 2.2.6.1 KINETIC EXPERIMENTS ON
CORRELATION OF PD-LEACHING AND CONVERSION...44 2.2.6.2 PALLADIUM
LEACHING AS FUNCTION OF REACTION PARAMETERS 48 2.2.7 11 B NMR EXPERIMENT
51 2.2.8 TEM CHARACTERIZATION OF THE CATALYST BEFORE AND AFTER SUZUKI
COUPLING REACTIONS 54 2.2.9 CONCLUSIVE REMARKS: SUZUKI COUPLING
REACTIONS IN NMP/WATER AT 65 C..56 2.3 SUZUKI COUPLING REACTIONS IN
PURE WATER 58 2.3.1 GENERAL INTRODUCTION 58 2.3.2 PD/C CATALYZED SUZUKI
COUPLING REACTIONS IN WATER UNDER MILD CONDITIONS 59 2.3.2.1 VARIATION
OF AMOUNT OF WATER 59 2.3.2.2 SUBSTRATE SCOPE FOR PD/C CATALYZED SUZUKI
COUPLING REACTIONS OF ARYL BROMIDES IN WATER 60 2.3.3 PD/MOX CATALYZED
SUZUKI COUPLING REACTIONS AT 65 C 60 2.3.3.1 INFLUENCE OF METAL OXIDE
SUPPORT 61 2.3.3.2 VARIATION OF CATALYST AMOUNT 65 2.3.3.3 OPTIMIZATION
OF REACTION PARAMETERS 65 2.3.3.4 PD/MODIFIED METAL OXIDES CATALYZED
SUZUKI COUPLING REACTIONS OF ARYL BROMIDES IN WATER 66 2.3.4 CONCLUSIVE
REMARKS: SUZUKI COUPLING REACTIONS IN WATER 67 3. OXIDATIVE COUPLING
REACTIONS 69 3.1 GENERAL INTRODUCTION 70 3.1.1 SCREENING OF OXIDANTS AT
DIFFERENT TEMPERATURES 71 3.1.2 TIME-DEPENDANT CORRELATION OF ACTIVITY
AND SELECTIVITY IN OXIDATIVE COUPLING REACTIONS 73 3.1.3 INFLUENCE OF
MOLAR EXCESS OF BENZENE AND REACTION ATMOSPHERE 74 3.1.4 VARIATION OF
OXIDANT AMOUNT 76 3.1.5 VARYING THE PD-SOURCE IN OXIDATIVE COUPLING
REACTIONS 78 3.1. TABLE OF CONTENTS 3.2.2 VARIATION OF PD SOURCES 83
3.2.3 VARIATION OF OXIDANT AMOUNT 84 3.2.4 VARIATION OF LIGAND AND BASE
85 3.2.5 CONCLUSIVE REMARKS: TEMPO AS OXIDIZING AGENT 87 3.3
INVESTIGATIONS ON SOME OTHER CATALYTIC SYSTEMS FOR OXIDATIVE COUPLING
REACTIONS 88 3.3.1 PD/HPA CATALYTIC SYSTEM 88 3.3.2 PEROXIDES (TBUOOH OR
H 2 O 2 ) AS OXIDANTS 90 4. SUMMARY 91 5. ZUSAMMENFASSUNG 97 6.
EXPERIMENTAL SECTION 103 6.1 GENERAL REMARKS 104 6.2 ANALYTICAL METHODS
104 6.2.1 ELEMENTAL ANALYSIS 104 6.2.2 GAS CHROMATOGRAPHY 104 6.2.3 NMR
SPECTROSCOPY 105 6.2.4 EPR SPECTROSCOPY 106 6.2.5 TRANSMISSION ELECTRON
MICROSCOPY 106 6.3 CATALYST PREPARATION 106 6.3.1 MODIFICATION OF AI2O3
SURFACE (AI2O3-C8 PREPARATION) 106 6.3.2 PREPARATION OF 1 WT% PD/MO X
108 6.3.3 PREPARATION OF 1 WT% PD/T2000 (AMPHIPHILIC SUPPORT) 108 6.3.4
PREPARATION OF PD/T805 AND PD/AI 2 O 3 -C 8 (HYDROPHOBIC SUPPORTS) 108
6.3.5 PRE-TREATMENT OF PD/AI 2 O 3 CATALYST 108 6.3.6 PREPARATION OF 1
WT% PD/NAY 109 6.3.7 PD/C CATALYST 109 6.4 GENERAL PROCEDURES FOR
CATALYTIC TESTS 109 6.4.1 SUZUKI COUPLING REACTIONS OF ARYL HALIDES IN
NMP/WATER AT 120 C 109 6.4. TABLE OF CONTENTS 6.4.8 OXIDATIVE COUPLING
OF BENZENE AND STYRENE 113 6.5 STRUCTURAL DATA OF REACTION PRODUCTS 113
7. APPENDIX 117 8. REFERENCES 119
|
| any_adam_object | 1 |
| author | Soomro, Saeeda 1975- |
| author_GND | (DE-588)13887557X |
| author_facet | Soomro, Saeeda 1975- |
| author_role | aut |
| author_sort | Soomro, Saeeda 1975- |
| author_variant | s s ss |
| building | Verbundindex |
| bvnumber | BV035665093 |
| classification_tum | CHE 609d CHE 167d CHE 620d |
| ctrlnum | (OCoLC)642992240 (DE-599)DNB99573576X |
| dewey-full | 547.215 546.6362 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry 546 - Inorganic chemistry |
| dewey-raw | 547.215 546.6362 |
| dewey-search | 547.215 546.6362 |
| dewey-sort | 3547.215 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik Chemie |
| edition | 1. Aufl. |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV035665093 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T21:42:48Z |
| institution | BVB |
| isbn | 9783868531251 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-017719461 |
| oclc_num | 642992240 |
| open_access_boolean | |
| owner | DE-12 DE-19 DE-BY-UBM DE-91 DE-BY-TUM |
| owner_facet | DE-12 DE-19 DE-BY-UBM DE-91 DE-BY-TUM |
| physical | 126 S. Ill., graph. Darst. 210 mm x 148 mm, 191 gr. |
| publishDate | 2009 |
| publishDateSearch | 2009 |
| publishDateSort | 2009 |
| publisher | Verl. Dr. Hut |
| record_format | marc |
| series2 | Anorganische Chemie |
| spelling | Soomro, Saeeda 1975- Verfasser (DE-588)13887557X aut C-C coupling reactions catalyzed by supported palladium in liquid phase Saeeda Shahid Soomro 1. Aufl. München Verl. Dr. Hut 2009 126 S. Ill., graph. Darst. 210 mm x 148 mm, 191 gr. txt rdacontent n rdamedia nc rdacarrier Anorganische Chemie Zugl.: München, Techn. Univ., Diss., 2009 Palladiumkomplexe (DE-588)4223138-3 gnd rswk-swf Flüssiger Zustand (DE-588)4336025-7 gnd rswk-swf Reaktionsmechanismus (DE-588)4177123-0 gnd rswk-swf Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 gnd rswk-swf Kupplungsreaktion (DE-588)4166199-0 gnd rswk-swf Heterogene Katalyse (DE-588)4123377-3 gnd rswk-swf Palladiumverbindungen (DE-588)4173148-7 gnd rswk-swf Palladiumorganische Verbindungen (DE-588)4353954-3 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Kupplungsreaktion (DE-588)4166199-0 s Palladiumverbindungen (DE-588)4173148-7 s Heterogene Katalyse (DE-588)4123377-3 s Flüssiger Zustand (DE-588)4336025-7 s DE-604 Palladiumkomplexe (DE-588)4223138-3 s Reaktionsmechanismus (DE-588)4177123-0 s 1\p DE-604 Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 s Palladiumorganische Verbindungen (DE-588)4353954-3 s 2\p DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017719461&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Soomro, Saeeda 1975- C-C coupling reactions catalyzed by supported palladium in liquid phase Palladiumkomplexe (DE-588)4223138-3 gnd Flüssiger Zustand (DE-588)4336025-7 gnd Reaktionsmechanismus (DE-588)4177123-0 gnd Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 gnd Kupplungsreaktion (DE-588)4166199-0 gnd Heterogene Katalyse (DE-588)4123377-3 gnd Palladiumverbindungen (DE-588)4173148-7 gnd Palladiumorganische Verbindungen (DE-588)4353954-3 gnd |
| subject_GND | (DE-588)4223138-3 (DE-588)4336025-7 (DE-588)4177123-0 (DE-588)4164549-2 (DE-588)4166199-0 (DE-588)4123377-3 (DE-588)4173148-7 (DE-588)4353954-3 (DE-588)4113937-9 |
| title | C-C coupling reactions catalyzed by supported palladium in liquid phase |
| title_auth | C-C coupling reactions catalyzed by supported palladium in liquid phase |
| title_exact_search | C-C coupling reactions catalyzed by supported palladium in liquid phase |
| title_full | C-C coupling reactions catalyzed by supported palladium in liquid phase Saeeda Shahid Soomro |
| title_fullStr | C-C coupling reactions catalyzed by supported palladium in liquid phase Saeeda Shahid Soomro |
| title_full_unstemmed | C-C coupling reactions catalyzed by supported palladium in liquid phase Saeeda Shahid Soomro |
| title_short | C-C coupling reactions catalyzed by supported palladium in liquid phase |
| title_sort | c c coupling reactions catalyzed by supported palladium in liquid phase |
| topic | Palladiumkomplexe (DE-588)4223138-3 gnd Flüssiger Zustand (DE-588)4336025-7 gnd Reaktionsmechanismus (DE-588)4177123-0 gnd Kohlenstoff-Kohlenstoff-Bindung (DE-588)4164549-2 gnd Kupplungsreaktion (DE-588)4166199-0 gnd Heterogene Katalyse (DE-588)4123377-3 gnd Palladiumverbindungen (DE-588)4173148-7 gnd Palladiumorganische Verbindungen (DE-588)4353954-3 gnd |
| topic_facet | Palladiumkomplexe Flüssiger Zustand Reaktionsmechanismus Kohlenstoff-Kohlenstoff-Bindung Kupplungsreaktion Heterogene Katalyse Palladiumverbindungen Palladiumorganische Verbindungen Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=017719461&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT soomrosaeeda cccouplingreactionscatalyzedbysupportedpalladiuminliquidphase |