A practical guide to transmission electron microscopy :: fundamentals /
Transmission electron microscope (TEM) is a very powerful tool for characterizing various types of materials. Using a light microscope, the imaging resolution is at several hundred nanometers, and for a scanning electron microscope, SEM, at several nanometers. The imaging resolution of the TEM, howe...
Gespeichert in:
1. Verfasser: | |
---|---|
Format: | Elektronisch E-Book |
Sprache: | English |
Veröffentlicht: |
New York [New York] (222 East 46th Street, New York, NY 10017) :
Momentum Press,
2016.
|
Ausgabe: | First edition. |
Schriftenreihe: | Materials characterization and analysis collection.
|
Schlagworte: | |
Online-Zugang: | Volltext |
Zusammenfassung: | Transmission electron microscope (TEM) is a very powerful tool for characterizing various types of materials. Using a light microscope, the imaging resolution is at several hundred nanometers, and for a scanning electron microscope, SEM, at several nanometers. The imaging resolution of the TEM, however, can routinely reach several angstroms on a modem instrument. In addition, the TEM can also provide material structural information, since the electrons penetrate through the thin specimens, and chemical compositional information due to the strong electron-specimen atom interactions. Nowadays, TEM is widely applied in diverse areas in both physical sciences (chemistry, engineering, geosciences, materials science, and physics) and life sciences (agriculture, biology, and medicine), playing a key role in research or development for material design, synthesis, processing, or performance. This book provides a concise practical guide to the TEM user, starting from the beginner level, including upper-division undergraduates, graduates, researchers, and engineers, on how to learn TEM efficiently in a short period of time. It is written primarily for materials science and engineering or related disciplines, while some applications in life sciences are also included. It covers most of the areas using TEM, including the instrumentation, sample preparation, diffraction, imaging, analytical microscopy, and some newly developed advanced microscopy techniques. In each topic, a theoretical background is firstly briefly outlined, followed with step-by-step instructions in experimental operation or computation. Some technical tips are given in order to obtain the best results. The practical procedures to acquire, analyze, and interpret the TEM data are therefore provided. This book may serve as a textbook for a TEM course or workshop, or a reference book for the TEM user to improve their TEM skills. |
Beschreibung: | Title from PDF title page (viewed on December 27, 2015). |
Beschreibung: | 1 online resource (1 PDF (xiv, 152 pages)) : illustrations |
Bibliographie: | Includes bibliographical references and index. |
ISBN: | 9781606507032 1606507036 9781606507049 1606507044 |
ISSN: | 2377-4355 |
Internformat
MARC
LEADER | 00000cam a2200000Mi 4500 | ||
---|---|---|---|
001 | ZDB-4-EBA-ocn936210003 | ||
003 | OCoLC | ||
005 | 20241004212047.0 | ||
006 | m eo d | ||
007 | cr cn||||m|||a | ||
008 | 151227s2016 nyua foab 001 0 eng d | ||
040 | |a NYMPP |b eng |e rda |e pn |c NYMPP |d OCLCO |d OCLCF |d YDXCP |d N$T |d NRC |d STF |d G3B |d IGB |d OCLCQ |d OCLCO |d OCLCQ |d OCLCO |d OCLCL | ||
019 | |a 959328517 |a 962433050 |a 965415489 |a 1058498835 |a 1096237258 | ||
020 | |a 9781606507032 |q (electronic bk.) | ||
020 | |a 1606507036 |q (electronic bk.) | ||
020 | |a 9781606507049 |q (electronic bk.) | ||
020 | |a 1606507044 |q (electronic bk.) | ||
024 | 7 | |a 10.5643/9781606507049 |2 doi | |
035 | |a (OCoLC)936210003 |z (OCoLC)959328517 |z (OCoLC)962433050 |z (OCoLC)965415489 |z (OCoLC)1058498835 |z (OCoLC)1096237258 | ||
050 | 4 | |a QH212.T7 |b L866 2016 | |
072 | 7 | |a SCI |x 000000 |2 bisacsh | |
082 | 7 | |a 502.825 |2 23 | |
049 | |a MAIN | ||
100 | 1 | |a Luo, Zhiping., |e author. | |
245 | 1 | 2 | |a A practical guide to transmission electron microscopy : |b fundamentals / |c Zhiping Luo. |
250 | |a First edition. | ||
264 | 1 | |a New York [New York] (222 East 46th Street, New York, NY 10017) : |b Momentum Press, |c 2016. | |
300 | |a 1 online resource (1 PDF (xiv, 152 pages)) : |b illustrations | ||
336 | |a text |b txt |2 rdacontent | ||
337 | |a electronic |2 isbdmedia | ||
338 | |a online resource |b cr |2 rdacarrier | ||
490 | 1 | |a Materials characterization and analysis collection, |x 2377-4355 | |
500 | |a Title from PDF title page (viewed on December 27, 2015). | ||
504 | |a Includes bibliographical references and index. | ||
505 | 0 | |a 1. Introduction -- 1.1 Microscope resolution -- 1.2 Interactions of electrons with specimen -- 1.3 Comparison of TEM with other microscopy techniques -- References | |
505 | 8 | |a 2. Sample preparation -- 2.1 Material samples -- 2.1.1 TEM grids -- 2.1.2 Ion milling -- 2.1.3 Electropolishing -- 2.1.4 Focused ion beam -- 2.1.5 Microtomy -- 2.2 Biological samples -- 2.2.1 Particulate samples -- 2.2.2 Cells and tissue samples -- References | |
505 | 8 | |a 3. Instrumentation and operation -- 3.1 Construction -- 3.1.1 Electron gun -- 3.1.2 Electromagnetic lens -- 3.1.3 Condenser lenses and condenser apertures -- 3.1.4 Objective lens and objective aperture -- 3.1.5 Intermediate lens and diffraction aperture -- 3.1.6 Projector lens -- 3.1.7 Viewing screen and camera -- 3.2 Instrument imperfections, alignments, corrections, and calibrations -- 3.2.1 Beam shift and beam tilt -- 3.2.2 Spherical aberration -- 3.2.3 Chromatic aberration -- 3.2.4 Depth of field and depth of focus -- 3.2.5 Specimen height -- 3.2.6 Astigmatism -- 3.2.7 Aperture alignment -- 3.2.8 Magnification calibration -- 3.2.9 Camera length calibration -- 3.2.10 Magnetic rotation calibration -- 3.3 TEM operating procedures -- 3.3.1 Startup -- 3.3.2 Specimen loading and unloading -- 3.3.3 Alignments -- 3.3.4 Data recording -- 3.3.5 Finishing -- References | |
505 | 8 | |a 4. Electron diffraction I -- 4.1 Formation of electron diffraction -- 4.2 Reciprocal space -- 4.3 Indexing of electron diffraction patterns -- 4.3.1 Indexing of powder patterns -- 4.3.2 Indexing of single-crystal diffraction patterns -- 4.3.3 Indexing of compound patterns: twins -- 4.3.4 Indexing of compound patterns: multiple phases -- 4.3.5 Indexing of compound patterns: double diffraction -- 4.4 Experimental procedures -- 4.5 Simulation of diffraction patterns -- References | |
505 | 8 | |a 5. Imaging I -- 5.1 Imaging contrast -- 5.2 Imaging with mass-thickness contrast -- 5.3 Imaging with diffraction contrast -- 5.3.1 Formation of diffraction contrast -- 5.3.2 Central dark-field imaging -- 5.3.3 Two-beam condition -- 5.3.4 Bragg-diffracted beam intensity -- 5.3.5 Thickness fringes -- 5.3.6 Bend contours -- 5.3.7 Weak-beam dark-field imaging -- 5.3.8 Planar defects -- 5.3.9 Dislocations -- References | |
505 | 8 | |a Appendices -- Appendix I. SAED indexing table of primitive cubic structure -- Appendix II. SAED indexing table of body-centered cubic structure -- Appendix III. SAED indexing table of face-centered cubic structure -- Appendix IV. SAED indexing table of close-packed hexagonal structure -- Illustration credits -- Index. | |
520 | 3 | |a Transmission electron microscope (TEM) is a very powerful tool for characterizing various types of materials. Using a light microscope, the imaging resolution is at several hundred nanometers, and for a scanning electron microscope, SEM, at several nanometers. The imaging resolution of the TEM, however, can routinely reach several angstroms on a modem instrument. In addition, the TEM can also provide material structural information, since the electrons penetrate through the thin specimens, and chemical compositional information due to the strong electron-specimen atom interactions. Nowadays, TEM is widely applied in diverse areas in both physical sciences (chemistry, engineering, geosciences, materials science, and physics) and life sciences (agriculture, biology, and medicine), playing a key role in research or development for material design, synthesis, processing, or performance. This book provides a concise practical guide to the TEM user, starting from the beginner level, including upper-division undergraduates, graduates, researchers, and engineers, on how to learn TEM efficiently in a short period of time. It is written primarily for materials science and engineering or related disciplines, while some applications in life sciences are also included. It covers most of the areas using TEM, including the instrumentation, sample preparation, diffraction, imaging, analytical microscopy, and some newly developed advanced microscopy techniques. In each topic, a theoretical background is firstly briefly outlined, followed with step-by-step instructions in experimental operation or computation. Some technical tips are given in order to obtain the best results. The practical procedures to acquire, analyze, and interpret the TEM data are therefore provided. This book may serve as a textbook for a TEM course or workshop, or a reference book for the TEM user to improve their TEM skills. | |
650 | 0 | |a Transmission electron microscopy. |0 http://id.loc.gov/authorities/subjects/sh93001918 | |
650 | 6 | |a Microscopie électronique à transmission. | |
650 | 7 | |a SCIENCE |x General. |2 bisacsh | |
650 | 7 | |a Transmission electron microscopy |2 fast | |
653 | |a Analytical Electron Microscopy | ||
653 | |a Ceramics | ||
653 | |a Chemical Analysis | ||
653 | |a Chemistry | ||
653 | |a Composites | ||
653 | |a Crystallography | ||
653 | |a Electron Diffraction | ||
653 | |a Electron Energy- Loss Spectroscopy (EELS) | ||
653 | |a Forensic Science | ||
653 | |a Geosciences | ||
653 | |a Imaging | ||
653 | |a Industry | ||
653 | |a Life Sciences | ||
653 | |a Materials Science and Engineering | ||
653 | |a Metals and Alloys | ||
653 | |a Microstructure | ||
653 | |a Nanomaterials | ||
653 | |a Nanoscience | ||
653 | |a Nanotechnology | ||
653 | |a Physics | ||
653 | |a Scanning Transmission Electron Microscopy (STEM) | ||
653 | |a Polymer | ||
653 | |a Structure | ||
653 | |a Transmission Electron Microscopy (TEM) | ||
653 | |a X-ray Energy- Dispersive Spectroscopy (EDS) | ||
758 | |i has work: |a A practical guide to transmission electron microscopy (Text) |1 https://id.oclc.org/worldcat/entity/E39PCGT6pKBCQC4XtdfvPRqb3P |4 https://id.oclc.org/worldcat/ontology/hasWork | ||
776 | 0 | 8 | |i Print version: |z 9781606507049 |
830 | 0 | |a Materials characterization and analysis collection. |x 2377-4355 |0 http://id.loc.gov/authorities/names/no2018013025 | |
856 | 4 | 0 | |l FWS01 |p ZDB-4-EBA |q FWS_PDA_EBA |u https://search.ebscohost.com/login.aspx?direct=true&scope=site&db=nlebk&AN=1104642 |3 Volltext |
938 | |a EBSCOhost |b EBSC |n 1104642 | ||
938 | |a Momentum Press |b NYMP |n 9781606507032 | ||
938 | |a YBP Library Services |b YANK |n 12730093 | ||
994 | |a 92 |b GEBAY | ||
912 | |a ZDB-4-EBA | ||
049 | |a DE-863 |
Datensatz im Suchindex
DE-BY-FWS_katkey | ZDB-4-EBA-ocn936210003 |
---|---|
_version_ | 1816882337817821184 |
adam_text | |
any_adam_object | |
author | Luo, Zhiping |
author_facet | Luo, Zhiping |
author_role | aut |
author_sort | Luo, Zhiping |
author_variant | z l zl |
building | Verbundindex |
bvnumber | localFWS |
callnumber-first | Q - Science |
callnumber-label | QH212 |
callnumber-raw | QH212.T7 L866 2016 |
callnumber-search | QH212.T7 L866 2016 |
callnumber-sort | QH 3212 T7 L866 42016 |
callnumber-subject | QH - Natural History and Biology |
collection | ZDB-4-EBA |
contents | 1. Introduction -- 1.1 Microscope resolution -- 1.2 Interactions of electrons with specimen -- 1.3 Comparison of TEM with other microscopy techniques -- References 2. Sample preparation -- 2.1 Material samples -- 2.1.1 TEM grids -- 2.1.2 Ion milling -- 2.1.3 Electropolishing -- 2.1.4 Focused ion beam -- 2.1.5 Microtomy -- 2.2 Biological samples -- 2.2.1 Particulate samples -- 2.2.2 Cells and tissue samples -- References 3. Instrumentation and operation -- 3.1 Construction -- 3.1.1 Electron gun -- 3.1.2 Electromagnetic lens -- 3.1.3 Condenser lenses and condenser apertures -- 3.1.4 Objective lens and objective aperture -- 3.1.5 Intermediate lens and diffraction aperture -- 3.1.6 Projector lens -- 3.1.7 Viewing screen and camera -- 3.2 Instrument imperfections, alignments, corrections, and calibrations -- 3.2.1 Beam shift and beam tilt -- 3.2.2 Spherical aberration -- 3.2.3 Chromatic aberration -- 3.2.4 Depth of field and depth of focus -- 3.2.5 Specimen height -- 3.2.6 Astigmatism -- 3.2.7 Aperture alignment -- 3.2.8 Magnification calibration -- 3.2.9 Camera length calibration -- 3.2.10 Magnetic rotation calibration -- 3.3 TEM operating procedures -- 3.3.1 Startup -- 3.3.2 Specimen loading and unloading -- 3.3.3 Alignments -- 3.3.4 Data recording -- 3.3.5 Finishing -- References 4. Electron diffraction I -- 4.1 Formation of electron diffraction -- 4.2 Reciprocal space -- 4.3 Indexing of electron diffraction patterns -- 4.3.1 Indexing of powder patterns -- 4.3.2 Indexing of single-crystal diffraction patterns -- 4.3.3 Indexing of compound patterns: twins -- 4.3.4 Indexing of compound patterns: multiple phases -- 4.3.5 Indexing of compound patterns: double diffraction -- 4.4 Experimental procedures -- 4.5 Simulation of diffraction patterns -- References 5. Imaging I -- 5.1 Imaging contrast -- 5.2 Imaging with mass-thickness contrast -- 5.3 Imaging with diffraction contrast -- 5.3.1 Formation of diffraction contrast -- 5.3.2 Central dark-field imaging -- 5.3.3 Two-beam condition -- 5.3.4 Bragg-diffracted beam intensity -- 5.3.5 Thickness fringes -- 5.3.6 Bend contours -- 5.3.7 Weak-beam dark-field imaging -- 5.3.8 Planar defects -- 5.3.9 Dislocations -- References Appendices -- Appendix I. SAED indexing table of primitive cubic structure -- Appendix II. SAED indexing table of body-centered cubic structure -- Appendix III. SAED indexing table of face-centered cubic structure -- Appendix IV. SAED indexing table of close-packed hexagonal structure -- Illustration credits -- Index. |
ctrlnum | (OCoLC)936210003 |
dewey-full | 502.825 |
dewey-hundreds | 500 - Natural sciences and mathematics |
dewey-ones | 502 - Miscellany |
dewey-raw | 502.825 |
dewey-search | 502.825 |
dewey-sort | 3502.825 |
dewey-tens | 500 - Natural sciences and mathematics |
discipline | Allgemeine Naturwissenschaft |
edition | First edition. |
format | Electronic eBook |
fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>07908cam a2200901Mi 4500</leader><controlfield tag="001">ZDB-4-EBA-ocn936210003</controlfield><controlfield tag="003">OCoLC</controlfield><controlfield tag="005">20241004212047.0</controlfield><controlfield tag="006">m eo d </controlfield><controlfield tag="007">cr cn||||m|||a</controlfield><controlfield tag="008">151227s2016 nyua foab 001 0 eng d</controlfield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">NYMPP</subfield><subfield code="b">eng</subfield><subfield code="e">rda</subfield><subfield code="e">pn</subfield><subfield code="c">NYMPP</subfield><subfield code="d">OCLCO</subfield><subfield code="d">OCLCF</subfield><subfield code="d">YDXCP</subfield><subfield code="d">N$T</subfield><subfield code="d">NRC</subfield><subfield code="d">STF</subfield><subfield code="d">G3B</subfield><subfield code="d">IGB</subfield><subfield code="d">OCLCQ</subfield><subfield code="d">OCLCO</subfield><subfield code="d">OCLCQ</subfield><subfield code="d">OCLCO</subfield><subfield code="d">OCLCL</subfield></datafield><datafield tag="019" ind1=" " ind2=" "><subfield code="a">959328517</subfield><subfield code="a">962433050</subfield><subfield code="a">965415489</subfield><subfield code="a">1058498835</subfield><subfield code="a">1096237258</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9781606507032</subfield><subfield code="q">(electronic bk.)</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">1606507036</subfield><subfield code="q">(electronic bk.)</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9781606507049</subfield><subfield code="q">(electronic bk.)</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">1606507044</subfield><subfield code="q">(electronic bk.)</subfield></datafield><datafield tag="024" ind1="7" ind2=" "><subfield code="a">10.5643/9781606507049</subfield><subfield code="2">doi</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)936210003</subfield><subfield code="z">(OCoLC)959328517</subfield><subfield code="z">(OCoLC)962433050</subfield><subfield code="z">(OCoLC)965415489</subfield><subfield code="z">(OCoLC)1058498835</subfield><subfield code="z">(OCoLC)1096237258</subfield></datafield><datafield tag="050" ind1=" " ind2="4"><subfield code="a">QH212.T7</subfield><subfield code="b">L866 2016</subfield></datafield><datafield tag="072" ind1=" " ind2="7"><subfield code="a">SCI</subfield><subfield code="x">000000</subfield><subfield code="2">bisacsh</subfield></datafield><datafield tag="082" ind1="7" ind2=" "><subfield code="a">502.825</subfield><subfield code="2">23</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">MAIN</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Luo, Zhiping.,</subfield><subfield code="e">author.</subfield></datafield><datafield tag="245" ind1="1" ind2="2"><subfield code="a">A practical guide to transmission electron microscopy :</subfield><subfield code="b">fundamentals /</subfield><subfield code="c">Zhiping Luo.</subfield></datafield><datafield tag="250" ind1=" " ind2=" "><subfield code="a">First edition.</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">New York [New York] (222 East 46th Street, New York, NY 10017) :</subfield><subfield code="b">Momentum Press,</subfield><subfield code="c">2016.</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">1 online resource (1 PDF (xiv, 152 pages)) :</subfield><subfield code="b">illustrations</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="a">text</subfield><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="a">electronic</subfield><subfield code="2">isbdmedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="a">online resource</subfield><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="490" ind1="1" ind2=" "><subfield code="a">Materials characterization and analysis collection,</subfield><subfield code="x">2377-4355</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">Title from PDF title page (viewed on December 27, 2015).</subfield></datafield><datafield tag="504" ind1=" " ind2=" "><subfield code="a">Includes bibliographical references and index.</subfield></datafield><datafield tag="505" ind1="0" ind2=" "><subfield code="a">1. Introduction -- 1.1 Microscope resolution -- 1.2 Interactions of electrons with specimen -- 1.3 Comparison of TEM with other microscopy techniques -- References</subfield></datafield><datafield tag="505" ind1="8" ind2=" "><subfield code="a">2. Sample preparation -- 2.1 Material samples -- 2.1.1 TEM grids -- 2.1.2 Ion milling -- 2.1.3 Electropolishing -- 2.1.4 Focused ion beam -- 2.1.5 Microtomy -- 2.2 Biological samples -- 2.2.1 Particulate samples -- 2.2.2 Cells and tissue samples -- References</subfield></datafield><datafield tag="505" ind1="8" ind2=" "><subfield code="a">3. Instrumentation and operation -- 3.1 Construction -- 3.1.1 Electron gun -- 3.1.2 Electromagnetic lens -- 3.1.3 Condenser lenses and condenser apertures -- 3.1.4 Objective lens and objective aperture -- 3.1.5 Intermediate lens and diffraction aperture -- 3.1.6 Projector lens -- 3.1.7 Viewing screen and camera -- 3.2 Instrument imperfections, alignments, corrections, and calibrations -- 3.2.1 Beam shift and beam tilt -- 3.2.2 Spherical aberration -- 3.2.3 Chromatic aberration -- 3.2.4 Depth of field and depth of focus -- 3.2.5 Specimen height -- 3.2.6 Astigmatism -- 3.2.7 Aperture alignment -- 3.2.8 Magnification calibration -- 3.2.9 Camera length calibration -- 3.2.10 Magnetic rotation calibration -- 3.3 TEM operating procedures -- 3.3.1 Startup -- 3.3.2 Specimen loading and unloading -- 3.3.3 Alignments -- 3.3.4 Data recording -- 3.3.5 Finishing -- References</subfield></datafield><datafield tag="505" ind1="8" ind2=" "><subfield code="a">4. Electron diffraction I -- 4.1 Formation of electron diffraction -- 4.2 Reciprocal space -- 4.3 Indexing of electron diffraction patterns -- 4.3.1 Indexing of powder patterns -- 4.3.2 Indexing of single-crystal diffraction patterns -- 4.3.3 Indexing of compound patterns: twins -- 4.3.4 Indexing of compound patterns: multiple phases -- 4.3.5 Indexing of compound patterns: double diffraction -- 4.4 Experimental procedures -- 4.5 Simulation of diffraction patterns -- References</subfield></datafield><datafield tag="505" ind1="8" ind2=" "><subfield code="a">5. Imaging I -- 5.1 Imaging contrast -- 5.2 Imaging with mass-thickness contrast -- 5.3 Imaging with diffraction contrast -- 5.3.1 Formation of diffraction contrast -- 5.3.2 Central dark-field imaging -- 5.3.3 Two-beam condition -- 5.3.4 Bragg-diffracted beam intensity -- 5.3.5 Thickness fringes -- 5.3.6 Bend contours -- 5.3.7 Weak-beam dark-field imaging -- 5.3.8 Planar defects -- 5.3.9 Dislocations -- References</subfield></datafield><datafield tag="505" ind1="8" ind2=" "><subfield code="a">Appendices -- Appendix I. SAED indexing table of primitive cubic structure -- Appendix II. SAED indexing table of body-centered cubic structure -- Appendix III. SAED indexing table of face-centered cubic structure -- Appendix IV. SAED indexing table of close-packed hexagonal structure -- Illustration credits -- Index.</subfield></datafield><datafield tag="520" ind1="3" ind2=" "><subfield code="a">Transmission electron microscope (TEM) is a very powerful tool for characterizing various types of materials. Using a light microscope, the imaging resolution is at several hundred nanometers, and for a scanning electron microscope, SEM, at several nanometers. The imaging resolution of the TEM, however, can routinely reach several angstroms on a modem instrument. In addition, the TEM can also provide material structural information, since the electrons penetrate through the thin specimens, and chemical compositional information due to the strong electron-specimen atom interactions. Nowadays, TEM is widely applied in diverse areas in both physical sciences (chemistry, engineering, geosciences, materials science, and physics) and life sciences (agriculture, biology, and medicine), playing a key role in research or development for material design, synthesis, processing, or performance. This book provides a concise practical guide to the TEM user, starting from the beginner level, including upper-division undergraduates, graduates, researchers, and engineers, on how to learn TEM efficiently in a short period of time. It is written primarily for materials science and engineering or related disciplines, while some applications in life sciences are also included. It covers most of the areas using TEM, including the instrumentation, sample preparation, diffraction, imaging, analytical microscopy, and some newly developed advanced microscopy techniques. In each topic, a theoretical background is firstly briefly outlined, followed with step-by-step instructions in experimental operation or computation. Some technical tips are given in order to obtain the best results. The practical procedures to acquire, analyze, and interpret the TEM data are therefore provided. This book may serve as a textbook for a TEM course or workshop, or a reference book for the TEM user to improve their TEM skills.</subfield></datafield><datafield tag="650" ind1=" " ind2="0"><subfield code="a">Transmission electron microscopy.</subfield><subfield code="0">http://id.loc.gov/authorities/subjects/sh93001918</subfield></datafield><datafield tag="650" ind1=" " ind2="6"><subfield code="a">Microscopie électronique à transmission.</subfield></datafield><datafield tag="650" ind1=" " ind2="7"><subfield code="a">SCIENCE</subfield><subfield code="x">General.</subfield><subfield code="2">bisacsh</subfield></datafield><datafield tag="650" ind1=" " ind2="7"><subfield code="a">Transmission electron microscopy</subfield><subfield code="2">fast</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Analytical Electron Microscopy</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Ceramics</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Chemical Analysis</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Chemistry</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Composites</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Crystallography</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Electron Diffraction</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Electron Energy- Loss Spectroscopy (EELS)</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Forensic Science</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Geosciences</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Imaging</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Industry</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Life Sciences</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Materials Science and Engineering</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Metals and Alloys</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Microstructure</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Nanomaterials</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Nanoscience</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Nanotechnology</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Physics</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Scanning Transmission Electron Microscopy (STEM)</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Polymer</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Structure</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">Transmission Electron Microscopy (TEM)</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">X-ray Energy- Dispersive Spectroscopy (EDS)</subfield></datafield><datafield tag="758" ind1=" " ind2=" "><subfield code="i">has work:</subfield><subfield code="a">A practical guide to transmission electron microscopy (Text)</subfield><subfield code="1">https://id.oclc.org/worldcat/entity/E39PCGT6pKBCQC4XtdfvPRqb3P</subfield><subfield code="4">https://id.oclc.org/worldcat/ontology/hasWork</subfield></datafield><datafield tag="776" ind1="0" ind2="8"><subfield code="i">Print version:</subfield><subfield code="z">9781606507049</subfield></datafield><datafield tag="830" ind1=" " ind2="0"><subfield code="a">Materials characterization and analysis collection.</subfield><subfield code="x">2377-4355</subfield><subfield code="0">http://id.loc.gov/authorities/names/no2018013025</subfield></datafield><datafield tag="856" ind1="4" ind2="0"><subfield code="l">FWS01</subfield><subfield code="p">ZDB-4-EBA</subfield><subfield code="q">FWS_PDA_EBA</subfield><subfield code="u">https://search.ebscohost.com/login.aspx?direct=true&scope=site&db=nlebk&AN=1104642</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="938" ind1=" " ind2=" "><subfield code="a">EBSCOhost</subfield><subfield code="b">EBSC</subfield><subfield code="n">1104642</subfield></datafield><datafield tag="938" ind1=" " ind2=" "><subfield code="a">Momentum Press</subfield><subfield code="b">NYMP</subfield><subfield code="n">9781606507032</subfield></datafield><datafield tag="938" ind1=" " ind2=" "><subfield code="a">YBP Library Services</subfield><subfield code="b">YANK</subfield><subfield code="n">12730093</subfield></datafield><datafield tag="994" ind1=" " ind2=" "><subfield code="a">92</subfield><subfield code="b">GEBAY</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">ZDB-4-EBA</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-863</subfield></datafield></record></collection> |
id | ZDB-4-EBA-ocn936210003 |
illustrated | Illustrated |
indexdate | 2024-11-27T13:27:01Z |
institution | BVB |
isbn | 9781606507032 1606507036 9781606507049 1606507044 |
issn | 2377-4355 |
language | English |
oclc_num | 936210003 |
open_access_boolean | |
owner | MAIN DE-863 DE-BY-FWS |
owner_facet | MAIN DE-863 DE-BY-FWS |
physical | 1 online resource (1 PDF (xiv, 152 pages)) : illustrations |
psigel | ZDB-4-EBA |
publishDate | 2016 |
publishDateSearch | 2016 |
publishDateSort | 2016 |
publisher | Momentum Press, |
record_format | marc |
series | Materials characterization and analysis collection. |
series2 | Materials characterization and analysis collection, |
spelling | Luo, Zhiping., author. A practical guide to transmission electron microscopy : fundamentals / Zhiping Luo. First edition. New York [New York] (222 East 46th Street, New York, NY 10017) : Momentum Press, 2016. 1 online resource (1 PDF (xiv, 152 pages)) : illustrations text txt rdacontent electronic isbdmedia online resource cr rdacarrier Materials characterization and analysis collection, 2377-4355 Title from PDF title page (viewed on December 27, 2015). Includes bibliographical references and index. 1. Introduction -- 1.1 Microscope resolution -- 1.2 Interactions of electrons with specimen -- 1.3 Comparison of TEM with other microscopy techniques -- References 2. Sample preparation -- 2.1 Material samples -- 2.1.1 TEM grids -- 2.1.2 Ion milling -- 2.1.3 Electropolishing -- 2.1.4 Focused ion beam -- 2.1.5 Microtomy -- 2.2 Biological samples -- 2.2.1 Particulate samples -- 2.2.2 Cells and tissue samples -- References 3. Instrumentation and operation -- 3.1 Construction -- 3.1.1 Electron gun -- 3.1.2 Electromagnetic lens -- 3.1.3 Condenser lenses and condenser apertures -- 3.1.4 Objective lens and objective aperture -- 3.1.5 Intermediate lens and diffraction aperture -- 3.1.6 Projector lens -- 3.1.7 Viewing screen and camera -- 3.2 Instrument imperfections, alignments, corrections, and calibrations -- 3.2.1 Beam shift and beam tilt -- 3.2.2 Spherical aberration -- 3.2.3 Chromatic aberration -- 3.2.4 Depth of field and depth of focus -- 3.2.5 Specimen height -- 3.2.6 Astigmatism -- 3.2.7 Aperture alignment -- 3.2.8 Magnification calibration -- 3.2.9 Camera length calibration -- 3.2.10 Magnetic rotation calibration -- 3.3 TEM operating procedures -- 3.3.1 Startup -- 3.3.2 Specimen loading and unloading -- 3.3.3 Alignments -- 3.3.4 Data recording -- 3.3.5 Finishing -- References 4. Electron diffraction I -- 4.1 Formation of electron diffraction -- 4.2 Reciprocal space -- 4.3 Indexing of electron diffraction patterns -- 4.3.1 Indexing of powder patterns -- 4.3.2 Indexing of single-crystal diffraction patterns -- 4.3.3 Indexing of compound patterns: twins -- 4.3.4 Indexing of compound patterns: multiple phases -- 4.3.5 Indexing of compound patterns: double diffraction -- 4.4 Experimental procedures -- 4.5 Simulation of diffraction patterns -- References 5. Imaging I -- 5.1 Imaging contrast -- 5.2 Imaging with mass-thickness contrast -- 5.3 Imaging with diffraction contrast -- 5.3.1 Formation of diffraction contrast -- 5.3.2 Central dark-field imaging -- 5.3.3 Two-beam condition -- 5.3.4 Bragg-diffracted beam intensity -- 5.3.5 Thickness fringes -- 5.3.6 Bend contours -- 5.3.7 Weak-beam dark-field imaging -- 5.3.8 Planar defects -- 5.3.9 Dislocations -- References Appendices -- Appendix I. SAED indexing table of primitive cubic structure -- Appendix II. SAED indexing table of body-centered cubic structure -- Appendix III. SAED indexing table of face-centered cubic structure -- Appendix IV. SAED indexing table of close-packed hexagonal structure -- Illustration credits -- Index. Transmission electron microscope (TEM) is a very powerful tool for characterizing various types of materials. Using a light microscope, the imaging resolution is at several hundred nanometers, and for a scanning electron microscope, SEM, at several nanometers. The imaging resolution of the TEM, however, can routinely reach several angstroms on a modem instrument. In addition, the TEM can also provide material structural information, since the electrons penetrate through the thin specimens, and chemical compositional information due to the strong electron-specimen atom interactions. Nowadays, TEM is widely applied in diverse areas in both physical sciences (chemistry, engineering, geosciences, materials science, and physics) and life sciences (agriculture, biology, and medicine), playing a key role in research or development for material design, synthesis, processing, or performance. This book provides a concise practical guide to the TEM user, starting from the beginner level, including upper-division undergraduates, graduates, researchers, and engineers, on how to learn TEM efficiently in a short period of time. It is written primarily for materials science and engineering or related disciplines, while some applications in life sciences are also included. It covers most of the areas using TEM, including the instrumentation, sample preparation, diffraction, imaging, analytical microscopy, and some newly developed advanced microscopy techniques. In each topic, a theoretical background is firstly briefly outlined, followed with step-by-step instructions in experimental operation or computation. Some technical tips are given in order to obtain the best results. The practical procedures to acquire, analyze, and interpret the TEM data are therefore provided. This book may serve as a textbook for a TEM course or workshop, or a reference book for the TEM user to improve their TEM skills. Transmission electron microscopy. http://id.loc.gov/authorities/subjects/sh93001918 Microscopie électronique à transmission. SCIENCE General. bisacsh Transmission electron microscopy fast Analytical Electron Microscopy Ceramics Chemical Analysis Chemistry Composites Crystallography Electron Diffraction Electron Energy- Loss Spectroscopy (EELS) Forensic Science Geosciences Imaging Industry Life Sciences Materials Science and Engineering Metals and Alloys Microstructure Nanomaterials Nanoscience Nanotechnology Physics Scanning Transmission Electron Microscopy (STEM) Polymer Structure Transmission Electron Microscopy (TEM) X-ray Energy- Dispersive Spectroscopy (EDS) has work: A practical guide to transmission electron microscopy (Text) https://id.oclc.org/worldcat/entity/E39PCGT6pKBCQC4XtdfvPRqb3P https://id.oclc.org/worldcat/ontology/hasWork Print version: 9781606507049 Materials characterization and analysis collection. 2377-4355 http://id.loc.gov/authorities/names/no2018013025 FWS01 ZDB-4-EBA FWS_PDA_EBA https://search.ebscohost.com/login.aspx?direct=true&scope=site&db=nlebk&AN=1104642 Volltext |
spellingShingle | Luo, Zhiping A practical guide to transmission electron microscopy : fundamentals / Materials characterization and analysis collection. 1. Introduction -- 1.1 Microscope resolution -- 1.2 Interactions of electrons with specimen -- 1.3 Comparison of TEM with other microscopy techniques -- References 2. Sample preparation -- 2.1 Material samples -- 2.1.1 TEM grids -- 2.1.2 Ion milling -- 2.1.3 Electropolishing -- 2.1.4 Focused ion beam -- 2.1.5 Microtomy -- 2.2 Biological samples -- 2.2.1 Particulate samples -- 2.2.2 Cells and tissue samples -- References 3. Instrumentation and operation -- 3.1 Construction -- 3.1.1 Electron gun -- 3.1.2 Electromagnetic lens -- 3.1.3 Condenser lenses and condenser apertures -- 3.1.4 Objective lens and objective aperture -- 3.1.5 Intermediate lens and diffraction aperture -- 3.1.6 Projector lens -- 3.1.7 Viewing screen and camera -- 3.2 Instrument imperfections, alignments, corrections, and calibrations -- 3.2.1 Beam shift and beam tilt -- 3.2.2 Spherical aberration -- 3.2.3 Chromatic aberration -- 3.2.4 Depth of field and depth of focus -- 3.2.5 Specimen height -- 3.2.6 Astigmatism -- 3.2.7 Aperture alignment -- 3.2.8 Magnification calibration -- 3.2.9 Camera length calibration -- 3.2.10 Magnetic rotation calibration -- 3.3 TEM operating procedures -- 3.3.1 Startup -- 3.3.2 Specimen loading and unloading -- 3.3.3 Alignments -- 3.3.4 Data recording -- 3.3.5 Finishing -- References 4. Electron diffraction I -- 4.1 Formation of electron diffraction -- 4.2 Reciprocal space -- 4.3 Indexing of electron diffraction patterns -- 4.3.1 Indexing of powder patterns -- 4.3.2 Indexing of single-crystal diffraction patterns -- 4.3.3 Indexing of compound patterns: twins -- 4.3.4 Indexing of compound patterns: multiple phases -- 4.3.5 Indexing of compound patterns: double diffraction -- 4.4 Experimental procedures -- 4.5 Simulation of diffraction patterns -- References 5. Imaging I -- 5.1 Imaging contrast -- 5.2 Imaging with mass-thickness contrast -- 5.3 Imaging with diffraction contrast -- 5.3.1 Formation of diffraction contrast -- 5.3.2 Central dark-field imaging -- 5.3.3 Two-beam condition -- 5.3.4 Bragg-diffracted beam intensity -- 5.3.5 Thickness fringes -- 5.3.6 Bend contours -- 5.3.7 Weak-beam dark-field imaging -- 5.3.8 Planar defects -- 5.3.9 Dislocations -- References Appendices -- Appendix I. SAED indexing table of primitive cubic structure -- Appendix II. SAED indexing table of body-centered cubic structure -- Appendix III. SAED indexing table of face-centered cubic structure -- Appendix IV. SAED indexing table of close-packed hexagonal structure -- Illustration credits -- Index. Transmission electron microscopy. http://id.loc.gov/authorities/subjects/sh93001918 Microscopie électronique à transmission. SCIENCE General. bisacsh Transmission electron microscopy fast |
subject_GND | http://id.loc.gov/authorities/subjects/sh93001918 |
title | A practical guide to transmission electron microscopy : fundamentals / |
title_auth | A practical guide to transmission electron microscopy : fundamentals / |
title_exact_search | A practical guide to transmission electron microscopy : fundamentals / |
title_full | A practical guide to transmission electron microscopy : fundamentals / Zhiping Luo. |
title_fullStr | A practical guide to transmission electron microscopy : fundamentals / Zhiping Luo. |
title_full_unstemmed | A practical guide to transmission electron microscopy : fundamentals / Zhiping Luo. |
title_short | A practical guide to transmission electron microscopy : |
title_sort | practical guide to transmission electron microscopy fundamentals |
title_sub | fundamentals / |
topic | Transmission electron microscopy. http://id.loc.gov/authorities/subjects/sh93001918 Microscopie électronique à transmission. SCIENCE General. bisacsh Transmission electron microscopy fast |
topic_facet | Transmission electron microscopy. Microscopie électronique à transmission. SCIENCE General. Transmission electron microscopy |
url | https://search.ebscohost.com/login.aspx?direct=true&scope=site&db=nlebk&AN=1104642 |
work_keys_str_mv | AT luozhiping apracticalguidetotransmissionelectronmicroscopyfundamentals AT luozhiping practicalguidetotransmissionelectronmicroscopyfundamentals |