Essential practical NMR for organic chemistry:
Intro -- Essential Practical NMR for Organic Chemistry -- Contents -- Preface -- 1 Getting Started -- 1.1 The Technique -- 1.2 Instrumentation -- 1.2.1 CW Systems -- 1.2.2 FT Systems -- 1.2.3 Probes -- 1.2.4 Shims -- 1.3 Origin of the Chemical Shift -- 1.4 Origin of 'Splitting' -- 1.5 Inte...
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Elektronisch E-Book |
| Sprache: | English |
| Veröffentlicht: |
Hoboken, NJ ; Chichester, West Sussex
Wiley
2023
|
| Ausgabe: | Second edition |
| Schlagworte: | |
| Online-Zugang: | TUM01 |
| Zusammenfassung: | Intro -- Essential Practical NMR for Organic Chemistry -- Contents -- Preface -- 1 Getting Started -- 1.1 The Technique -- 1.2 Instrumentation -- 1.2.1 CW Systems -- 1.2.2 FT Systems -- 1.2.3 Probes -- 1.2.4 Shims -- 1.3 Origin of the Chemical Shift -- 1.4 Origin of 'Splitting' -- 1.5 Integration -- 2 Preparing the Sample -- 2.1 How Much Sample Do I Need? -- 2.2 Solvent Selection -- 2.2.1 Deutero Chloroform (CDCl3) -- 2.2.2 Deutero Dimethyl Sulfoxide (DMSO) -- 2.2.3 Deutero Methanol (CD3OD) -- 2.2.4 Deutero Water (D2O) -- 2.2.5 Deutero Benzene (C6D6) -- 2.2.6 Carbon Tetrachloride (CCl4) -- 2.2.7 Trifluoroacetic Acid (CF3COOH) -- 2.2.8 Using Mixed Solvents -- 2.3 Spectrum Referencing (Proton NMR) -- 2.4 Sample Preparation -- 2.4.1 Filtration -- 3 Spectrum Acquisition -- 3.1 Number of Transients -- 3.2 Number of Points -- 3.3 Spectral Width -- 3.4 Acquisition Time -- 3.5 Pulse Width/Pulse Angle -- 3.6 Relaxation Delay -- 3.7 Number of Increments -- 3.8 Non-Uniform Sampling (NUS) -- 3.9 Shimming -- 3.10 Tuning and Matching -- 3.11 Frequency Lock -- 3.11.1 Run Unlocked -- 3.11.2 Internal Lock -- 3.11.3 External Lock -- 3.12 To Spin or Not to Spin? -- 4 Processing -- 4.1 Introduction -- 4.2 Zero-Filling and Linear Prediction -- 4.3 Apodization -- 4.4 Fourier Transformation -- 4.5 Phase Correction -- 4.6 Baseline Correction -- 4.7 Integration -- 4.8 Referencing -- 4.9 Peak Picking -- 5 Interpreting Your Spectrum -- 5.1 Common Solvents and Impurities -- 5.2 Group 1 - Exchangeables and Aldehydes -- 5.3 Group 2 - Aromatic and Heterocyclic Protons -- 5.3.1 Monosubstituted Benzene Rings -- 5.3.2 Multi-substituted Benzene Rings -- 5.3.3 Heterocyclic Ring Systems (Unsaturated) and Polycyclic Aromatic Systems -- 5.4 Group 3 - Double and Triple Bonds -- 5.5 Group 4 - Alkyl Protons -- 6 Delving Deeper -- 6.1 Chiral Centres. |
| Beschreibung: | Description based on publisher supplied metadata and other sources |
| Beschreibung: | 1 Online-Ressource Illustrationen, Diagramme |
| ISBN: | 9781119844815 9781119844822 |
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| 520 | 3 | |a Intro -- Essential Practical NMR for Organic Chemistry -- Contents -- Preface -- 1 Getting Started -- 1.1 The Technique -- 1.2 Instrumentation -- 1.2.1 CW Systems -- 1.2.2 FT Systems -- 1.2.3 Probes -- 1.2.4 Shims -- 1.3 Origin of the Chemical Shift -- 1.4 Origin of 'Splitting' -- 1.5 Integration -- 2 Preparing the Sample -- 2.1 How Much Sample Do I Need? -- 2.2 Solvent Selection -- 2.2.1 Deutero Chloroform (CDCl3) -- 2.2.2 Deutero Dimethyl Sulfoxide (DMSO) -- 2.2.3 Deutero Methanol (CD3OD) -- 2.2.4 Deutero Water (D2O) -- 2.2.5 Deutero Benzene (C6D6) -- 2.2.6 Carbon Tetrachloride (CCl4) -- 2.2.7 Trifluoroacetic Acid (CF3COOH) -- 2.2.8 Using Mixed Solvents -- 2.3 Spectrum Referencing (Proton NMR) -- 2.4 Sample Preparation -- 2.4.1 Filtration -- 3 Spectrum Acquisition -- 3.1 Number of Transients -- 3.2 Number of Points -- 3.3 Spectral Width -- 3.4 Acquisition Time -- 3.5 Pulse Width/Pulse Angle -- 3.6 Relaxation Delay -- 3.7 Number of Increments -- 3.8 Non-Uniform Sampling (NUS) -- 3.9 Shimming -- 3.10 Tuning and Matching -- 3.11 Frequency Lock -- 3.11.1 Run Unlocked -- 3.11.2 Internal Lock -- 3.11.3 External Lock -- 3.12 To Spin or Not to Spin? -- 4 Processing -- 4.1 Introduction -- 4.2 Zero-Filling and Linear Prediction -- 4.3 Apodization -- 4.4 Fourier Transformation -- 4.5 Phase Correction -- 4.6 Baseline Correction -- 4.7 Integration -- 4.8 Referencing -- 4.9 Peak Picking -- 5 Interpreting Your Spectrum -- 5.1 Common Solvents and Impurities -- 5.2 Group 1 - Exchangeables and Aldehydes -- 5.3 Group 2 - Aromatic and Heterocyclic Protons -- 5.3.1 Monosubstituted Benzene Rings -- 5.3.2 Multi-substituted Benzene Rings -- 5.3.3 Heterocyclic Ring Systems (Unsaturated) and Polycyclic Aromatic Systems -- 5.4 Group 3 - Double and Triple Bonds -- 5.5 Group 4 - Alkyl Protons -- 6 Delving Deeper -- 6.1 Chiral Centres. | |
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Datensatz im Suchindex
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| isbn | 9781119844815 9781119844822 |
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| spelling | Richards, Stephen A. 1956- Verfasser (DE-588)143349295 aut Essential practical NMR for organic chemistry S.A. Richards and J.C. Hollerton Second edition Hoboken, NJ ; Chichester, West Sussex Wiley 2023 1 Online-Ressource Illustrationen, Diagramme txt rdacontent c rdamedia cr rdacarrier Description based on publisher supplied metadata and other sources Intro -- Essential Practical NMR for Organic Chemistry -- Contents -- Preface -- 1 Getting Started -- 1.1 The Technique -- 1.2 Instrumentation -- 1.2.1 CW Systems -- 1.2.2 FT Systems -- 1.2.3 Probes -- 1.2.4 Shims -- 1.3 Origin of the Chemical Shift -- 1.4 Origin of 'Splitting' -- 1.5 Integration -- 2 Preparing the Sample -- 2.1 How Much Sample Do I Need? -- 2.2 Solvent Selection -- 2.2.1 Deutero Chloroform (CDCl3) -- 2.2.2 Deutero Dimethyl Sulfoxide (DMSO) -- 2.2.3 Deutero Methanol (CD3OD) -- 2.2.4 Deutero Water (D2O) -- 2.2.5 Deutero Benzene (C6D6) -- 2.2.6 Carbon Tetrachloride (CCl4) -- 2.2.7 Trifluoroacetic Acid (CF3COOH) -- 2.2.8 Using Mixed Solvents -- 2.3 Spectrum Referencing (Proton NMR) -- 2.4 Sample Preparation -- 2.4.1 Filtration -- 3 Spectrum Acquisition -- 3.1 Number of Transients -- 3.2 Number of Points -- 3.3 Spectral Width -- 3.4 Acquisition Time -- 3.5 Pulse Width/Pulse Angle -- 3.6 Relaxation Delay -- 3.7 Number of Increments -- 3.8 Non-Uniform Sampling (NUS) -- 3.9 Shimming -- 3.10 Tuning and Matching -- 3.11 Frequency Lock -- 3.11.1 Run Unlocked -- 3.11.2 Internal Lock -- 3.11.3 External Lock -- 3.12 To Spin or Not to Spin? -- 4 Processing -- 4.1 Introduction -- 4.2 Zero-Filling and Linear Prediction -- 4.3 Apodization -- 4.4 Fourier Transformation -- 4.5 Phase Correction -- 4.6 Baseline Correction -- 4.7 Integration -- 4.8 Referencing -- 4.9 Peak Picking -- 5 Interpreting Your Spectrum -- 5.1 Common Solvents and Impurities -- 5.2 Group 1 - Exchangeables and Aldehydes -- 5.3 Group 2 - Aromatic and Heterocyclic Protons -- 5.3.1 Monosubstituted Benzene Rings -- 5.3.2 Multi-substituted Benzene Rings -- 5.3.3 Heterocyclic Ring Systems (Unsaturated) and Polycyclic Aromatic Systems -- 5.4 Group 3 - Double and Triple Bonds -- 5.5 Group 4 - Alkyl Protons -- 6 Delving Deeper -- 6.1 Chiral Centres. Strukturaufklärung (DE-588)4183788-5 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Organische Chemie (DE-588)4043793-0 gnd rswk-swf Electronic books NMR-Spektroskopie (DE-588)4075421-2 s Strukturaufklärung (DE-588)4183788-5 s Organische Chemie (DE-588)4043793-0 s DE-604 Hollerton, John C. 1959- Verfasser (DE-588)143349333 aut Erscheint auch als Druck-Ausgabe, Hardcover 978-1-119-84480-8 |
| spellingShingle | Richards, Stephen A. 1956- Hollerton, John C. 1959- Essential practical NMR for organic chemistry Strukturaufklärung (DE-588)4183788-5 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Organische Chemie (DE-588)4043793-0 gnd |
| subject_GND | (DE-588)4183788-5 (DE-588)4075421-2 (DE-588)4043793-0 |
| title | Essential practical NMR for organic chemistry |
| title_auth | Essential practical NMR for organic chemistry |
| title_exact_search | Essential practical NMR for organic chemistry |
| title_exact_search_txtP | Essential practical NMR for organic chemistry |
| title_full | Essential practical NMR for organic chemistry S.A. Richards and J.C. Hollerton |
| title_fullStr | Essential practical NMR for organic chemistry S.A. Richards and J.C. Hollerton |
| title_full_unstemmed | Essential practical NMR for organic chemistry S.A. Richards and J.C. Hollerton |
| title_short | Essential practical NMR for organic chemistry |
| title_sort | essential practical nmr for organic chemistry |
| topic | Strukturaufklärung (DE-588)4183788-5 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Organische Chemie (DE-588)4043793-0 gnd |
| topic_facet | Strukturaufklärung NMR-Spektroskopie Organische Chemie |
| work_keys_str_mv | AT richardsstephena essentialpracticalnmrfororganicchemistry AT hollertonjohnc essentialpracticalnmrfororganicchemistry |