Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials:
Gespeichert in:
1. Verfasser: | |
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Format: | Abschlussarbeit Buch |
Sprache: | English |
Veröffentlicht: |
Düren
Shaker Verlag
2022
|
Schriftenreihe: | Reports on measurement and sensor systems
|
Schlagworte: | |
Online-Zugang: | Inhaltsverzeichnis Inhaltsverzeichnis |
Beschreibung: | iii, 164 Seiten Illustrationen, Diagramme 21 cm x 14.8 cm, 260 g |
ISBN: | 9783844085174 3844085173 |
Internformat
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100 | 1 | |a Dong, Xingchen |e Verfasser |0 (DE-588)1258793369 |4 aut | |
245 | 1 | 0 | |a Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials |c Xingchen Dong |
264 | 1 | |a Düren |b Shaker Verlag |c 2022 | |
300 | |a iii, 164 Seiten |b Illustrationen, Diagramme |c 21 cm x 14.8 cm, 260 g | ||
336 | |b txt |2 rdacontent | ||
337 | |b n |2 rdamedia | ||
338 | |b nc |2 rdacarrier | ||
490 | 0 | |a Reports on measurement and sensor systems | |
502 | |b Dissertation |c Technische Universität München |d 2021 | ||
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650 | 0 | 7 | |a Schwarzer Phosphor |0 (DE-588)1189763842 |2 gnd |9 rswk-swf |
650 | 0 | 7 | |a Hyperspektraler Sensor |0 (DE-588)1078791082 |2 gnd |9 rswk-swf |
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650 | 0 | 7 | |8 5\p |a Materials |0 (DLC)sh85082065 |0 http://id.loc.gov/authorities/subjects/sh85082065 |2 lcsh |
653 | |a layer thickness | ||
653 | |a two-dimensional materials | ||
653 | |a microscopy | ||
653 | |a hyperspectral imaging | ||
653 | |a multivariate analysis | ||
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710 | 2 | |a Shaker Verlag |0 (DE-588)1064118135 |4 pbl | |
776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe |a Dong, Xingchen |t Hyperspectral Imaging Microscopy for Atomic Layer Mapping of Two-Dimensional Materials |b 1. Auflage |d Düren : Shaker, 2022 |h Online-Ressource, 173 Seiten, 60 Illustrationen |
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Datensatz im Suchindex
_version_ | 1804184535157440512 |
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adam_text | CONTENTS
1
INTRODUCTION
1
1.1
MOTIVATION
...........................................................................................................
2
1.2
OBJECTIVE
...........................................................................................................
4
1.3
THESIS
ORGANIZATION
............................................................................................
4
2
FUNDAMENTALS
AND
STATE
OF
THE
ART
7
2.1
MICROSCALE
HYPERSPECTRAL
IMAGING
...................................................................
7
2.2
2D
MATERIALS
AND
APPLICATIONS
.........................................................................
11
2.3
MICROSCALE
SPECTRAL
IMAGING
OF
2D
MATERIALS
.................................................
15
2.3.1
SPECTRAL
IMAGING
TECHNIQUES
FOR
2D
MEASUREMENTS
..........................
16
2.3.2
SPECTROSCOPIC
IMAGING
OF
GRAPHENE
.....................................................
21
2.3.3
SPECTROSCOPIC
IMAGING
OF
TMDS
...........................................................
24
2.3.4
SPECTROSCOPIC
IMAGING
OF
BLACK
PHOSPHORUS
.........................................
26
2.4
DISCUSSION
...........................................................................................................
29
2.5
SUMMARY
...........................................................................................................
30
3
HYPERSPECTRAL
SYSTEM
AND
DATA
ANALYSIS
METHODS
31
3.1
HYPERSPECTRAL
SYSTEM
.........................................................................................
31
3.1.1
HYPERSPECTRAL
DATA
ACQUISITION
MODES
..................................................
31
3.1.2
LINE-SCAN
HYPERSPECTRAL
REFLECTION
MICROSCOPY
......................................
33
3.1.3
SYSTEM
CALIBRATION
................................................................................
37
3.2
HYPERSPECTRAL
DATA
ACQUISITION
......................................................................
37
3.3
HYPERSPECTRAL
DATA
ANALYSIS
............................................................................
40
3.3.1
CONVENTIONAL
ANALYSIS
METHODS
..............................................................
40
3.3.2
MACHINE
LEARNING
METHODS
................................................................
44
3.4
SUMMARY
...........................................................................................................
48
4
PIXELWISE
HYPERSPECTRAL
DATA
INTERPRETATION
AND
CLASSIFICATION
51
4.1
WORKFLOW
OF
SPECTRAL
UNMIXING
AND
PEAK
POSITION
MAPPING
..........................
51
II
CONTENTS
4.2
HYPERSPECTRAL
REFLECTION
MEASUREMENTS
..............................................................
53
4.3
FEATURE
EXTRACTION
AND
PIXELWISE
CLASSIFICATION
...............................................
54
4.3.1
THICKNESS
MAPPING
WITH
SPECTRAL
UNMIXING
.........................................
54
4.3.2
THICKNESS
MAPPING
WITH
PEAK
POSITIONS
...............................................
56
4.4
SUMMARY
................................................................................................................
59
5
HYPERSPECTRAL-FINGERPRINTS-BASED
ATOMIC
LAYER
MAPPING
61
5.1
LAYER
MAPPING
OF
MONO-AND
FEW-LAYER
M0S2
...................................................
61
5.1.1
SPECTRAL
UNMIXING
FOR
ATOMIC
LAYER
MAPPING
......................................
61
5.1.2
HYPERSPECTRAL
MEASUREMENT
AND
THICKNESS
MAP
RECONSTRUCTION
.
.
62
5.2
LAYER
MAPPING
OF
MULTI-LAYER
HBN
....................................................................
66
5.2.1
HYPERSPECTRAL
MEASUREMENT
AND
THICKNESS
MAP
RECONSTRUCTION
.
.
66
5.2.2
HYPERSPECTRAL
CHARACTERIZATION
OF
AN
UNKNOWN
REGION
......................
67
5.3
IDENTIFICATION
ACCURACY
EVALUATION
USING
CVD
MOS
2
......................................
71
5.3.1
HYPERSPECTRAL
FINGERPRINTS
AND
MAP
RECONSTRUCTION
OF
MONO
AND
BI-LAYER
FLAKES
..........................................................................................
71
5.3.2
CROSS-VALIDATION
AND
GENERALIZABILITY
ANALYSIS
......................................
75
5.3.3
ANALYSIS
OF
HYPERSPECTRAL
DIMENSION
REDUCTION
...................................
77
5.4
DUAL-ILLUMINATION
HYPERSPECTRAL
MICROSCOPY
AND
PERFORMANCE
EVALUATION
.
79
5.5
SUMMARY
................................................................................................................
82
6
DEEP-LEARNING-ENABLED
IMAGES
FUSION
FOR
ATOMIC
LAYER
MAPPING
85
6.1
PRINCIPLE
OF
THE
DEEP
FUSION
METHOD
.................................................................
85
6.2
DATA
PRE-PROCESSING
AND
POST-PROCESSING
...........................................................
87
6.2.1
REGISTRATION
OF
RGB
AND
HYPERSPECTRAL
IMAGES
...................................
87
6.2.2
DATA
NORMALIZATION
....................................................................................
88
6.2.3
DATA
LABELING
.............................................................................................
89
6.2.4
DATA
AUGMENTATION
....................................................................................
92
6.2.5
DATA
POST-PROCESSING
.................................................................................
92
6.3
NETWORK
ARCHITECTURE,
TRAINING,
AND
TESTING
.....................................................
93
6.3.1
NETWORK
ARCHITECTURE
.................................................................................
93
6.3.2
BATCH
NORMALIZATION
.................................................................................
95
6.3.3
TRAINING
AND
TESTING
.................................................................................
96
6.4
PREDICTION
PERFORMANCES
AND
QUANTITATIVE
EVALUATION
......................................
97
6.4.1
PREDICTION
RESULTS
....................................................................................
97
6.4.2
QUANTITATIVE
EVALUATION
.........................................................................
102
6.4.3
MODEL
GENERALIZABILITY
ANALYSIS
..............................................................
105
6.5
SUMMARY
..............................................................................................................
106
CONTENTS
HI
7
CONCLUSION
AND
OUTLOOK
109
7.1
CONCLUSION
.............................................................................................................
109
7.2
OUTLOOK
................................................................................................................
110
APPENDIX
A
113
A.L
LIST
OF
SYMBOLS
...................................................................................................
113
A.2
LIST
OF
ABBREVIATIONS
..........................................................................................
115
A.3
LIST
OF
FIGURES
......................................................................................................
118
A.4
LIST
OF
TABLES
......................................................................................................
125
ACKNOWLEDGMENT
127
BIBLIOGRAPHY
129
PATENTS
AND
PUBLICATIONS
159
SUPERVISED
STUDENT
THESES
163
|
adam_txt |
CONTENTS
1
INTRODUCTION
1
1.1
MOTIVATION
.
2
1.2
OBJECTIVE
.
4
1.3
THESIS
ORGANIZATION
.
4
2
FUNDAMENTALS
AND
STATE
OF
THE
ART
7
2.1
MICROSCALE
HYPERSPECTRAL
IMAGING
.
7
2.2
2D
MATERIALS
AND
APPLICATIONS
.
11
2.3
MICROSCALE
SPECTRAL
IMAGING
OF
2D
MATERIALS
.
15
2.3.1
SPECTRAL
IMAGING
TECHNIQUES
FOR
2D
MEASUREMENTS
.
16
2.3.2
SPECTROSCOPIC
IMAGING
OF
GRAPHENE
.
21
2.3.3
SPECTROSCOPIC
IMAGING
OF
TMDS
.
24
2.3.4
SPECTROSCOPIC
IMAGING
OF
BLACK
PHOSPHORUS
.
26
2.4
DISCUSSION
.
29
2.5
SUMMARY
.
30
3
HYPERSPECTRAL
SYSTEM
AND
DATA
ANALYSIS
METHODS
31
3.1
HYPERSPECTRAL
SYSTEM
.
31
3.1.1
HYPERSPECTRAL
DATA
ACQUISITION
MODES
.
31
3.1.2
LINE-SCAN
HYPERSPECTRAL
REFLECTION
MICROSCOPY
.
33
3.1.3
SYSTEM
CALIBRATION
.
37
3.2
HYPERSPECTRAL
DATA
ACQUISITION
.
37
3.3
HYPERSPECTRAL
DATA
ANALYSIS
.
40
3.3.1
CONVENTIONAL
ANALYSIS
METHODS
.
40
3.3.2
MACHINE
LEARNING
METHODS
.
44
3.4
SUMMARY
.
48
4
PIXELWISE
HYPERSPECTRAL
DATA
INTERPRETATION
AND
CLASSIFICATION
51
4.1
WORKFLOW
OF
SPECTRAL
UNMIXING
AND
PEAK
POSITION
MAPPING
.
51
II
CONTENTS
4.2
HYPERSPECTRAL
REFLECTION
MEASUREMENTS
.
53
4.3
FEATURE
EXTRACTION
AND
PIXELWISE
CLASSIFICATION
.
54
4.3.1
THICKNESS
MAPPING
WITH
SPECTRAL
UNMIXING
.
54
4.3.2
THICKNESS
MAPPING
WITH
PEAK
POSITIONS
.
56
4.4
SUMMARY
.
59
5
HYPERSPECTRAL-FINGERPRINTS-BASED
ATOMIC
LAYER
MAPPING
61
5.1
LAYER
MAPPING
OF
MONO-AND
FEW-LAYER
M0S2
.
61
5.1.1
SPECTRAL
UNMIXING
FOR
ATOMIC
LAYER
MAPPING
.
61
5.1.2
HYPERSPECTRAL
MEASUREMENT
AND
THICKNESS
MAP
RECONSTRUCTION
.
.
62
5.2
LAYER
MAPPING
OF
MULTI-LAYER
HBN
.
66
5.2.1
HYPERSPECTRAL
MEASUREMENT
AND
THICKNESS
MAP
RECONSTRUCTION
.
.
66
5.2.2
HYPERSPECTRAL
CHARACTERIZATION
OF
AN
UNKNOWN
REGION
.
67
5.3
IDENTIFICATION
ACCURACY
EVALUATION
USING
CVD
MOS
2
.
71
5.3.1
HYPERSPECTRAL
FINGERPRINTS
AND
MAP
RECONSTRUCTION
OF
MONO
AND
BI-LAYER
FLAKES
.
71
5.3.2
CROSS-VALIDATION
AND
GENERALIZABILITY
ANALYSIS
.
75
5.3.3
ANALYSIS
OF
HYPERSPECTRAL
DIMENSION
REDUCTION
.
77
5.4
DUAL-ILLUMINATION
HYPERSPECTRAL
MICROSCOPY
AND
PERFORMANCE
EVALUATION
.
79
5.5
SUMMARY
.
82
6
DEEP-LEARNING-ENABLED
IMAGES
FUSION
FOR
ATOMIC
LAYER
MAPPING
85
6.1
PRINCIPLE
OF
THE
DEEP
FUSION
METHOD
.
85
6.2
DATA
PRE-PROCESSING
AND
POST-PROCESSING
.
87
6.2.1
REGISTRATION
OF
RGB
AND
HYPERSPECTRAL
IMAGES
.
87
6.2.2
DATA
NORMALIZATION
.
88
6.2.3
DATA
LABELING
.
89
6.2.4
DATA
AUGMENTATION
.
92
6.2.5
DATA
POST-PROCESSING
.
92
6.3
NETWORK
ARCHITECTURE,
TRAINING,
AND
TESTING
.
93
6.3.1
NETWORK
ARCHITECTURE
.
93
6.3.2
BATCH
NORMALIZATION
.
95
6.3.3
TRAINING
AND
TESTING
.
96
6.4
PREDICTION
PERFORMANCES
AND
QUANTITATIVE
EVALUATION
.
97
6.4.1
PREDICTION
RESULTS
.
97
6.4.2
QUANTITATIVE
EVALUATION
.
102
6.4.3
MODEL
GENERALIZABILITY
ANALYSIS
.
105
6.5
SUMMARY
.
106
CONTENTS
HI
7
CONCLUSION
AND
OUTLOOK
109
7.1
CONCLUSION
.
109
7.2
OUTLOOK
.
110
APPENDIX
A
113
A.L
LIST
OF
SYMBOLS
.
113
A.2
LIST
OF
ABBREVIATIONS
.
115
A.3
LIST
OF
FIGURES
.
118
A.4
LIST
OF
TABLES
.
125
ACKNOWLEDGMENT
127
BIBLIOGRAPHY
129
PATENTS
AND
PUBLICATIONS
159
SUPERVISED
STUDENT
THESES
163 |
any_adam_object | 1 |
any_adam_object_boolean | 1 |
author | Dong, Xingchen |
author_GND | (DE-588)1258793369 |
author_facet | Dong, Xingchen |
author_role | aut |
author_sort | Dong, Xingchen |
author_variant | x d xd |
building | Verbundindex |
bvnumber | BV048537141 |
classification_rvk | ZM 3100 ZM 7605 |
ctrlnum | (OCoLC)1352872889 (DE-599)DNB1252479123 |
dewey-full | 621.367 620.1127 |
dewey-hundreds | 600 - Technology (Applied sciences) |
dewey-ones | 621 - Applied physics 620 - Engineering and allied operations |
dewey-raw | 621.367 620.1127 |
dewey-search | 621.367 620.1127 |
dewey-sort | 3621.367 |
dewey-tens | 620 - Engineering and allied operations |
discipline | Elektrotechnik / Elektronik / Nachrichtentechnik Werkstoffwissenschaften / Fertigungstechnik |
discipline_str_mv | Elektrotechnik / Elektronik / Nachrichtentechnik Werkstoffwissenschaften / Fertigungstechnik |
format | Thesis Book |
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genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
genre_facet | Hochschulschrift |
id | DE-604.BV048537141 |
illustrated | Illustrated |
index_date | 2024-07-03T20:54:18Z |
indexdate | 2024-07-10T09:40:53Z |
institution | BVB |
institution_GND | (DE-588)1064118135 |
isbn | 9783844085174 3844085173 |
language | English |
oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-033913731 |
oclc_num | 1352872889 |
open_access_boolean | |
owner | DE-83 |
owner_facet | DE-83 |
physical | iii, 164 Seiten Illustrationen, Diagramme 21 cm x 14.8 cm, 260 g |
publishDate | 2022 |
publishDateSearch | 2022 |
publishDateSort | 2022 |
publisher | Shaker Verlag |
record_format | marc |
series2 | Reports on measurement and sensor systems |
spelling | Dong, Xingchen Verfasser (DE-588)1258793369 aut Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials Xingchen Dong Düren Shaker Verlag 2022 iii, 164 Seiten Illustrationen, Diagramme 21 cm x 14.8 cm, 260 g txt rdacontent n rdamedia nc rdacarrier Reports on measurement and sensor systems Dissertation Technische Universität München 2021 Mikroskopie (DE-588)4039238-7 gnd rswk-swf Bildverarbeitung (DE-588)4006684-8 gnd rswk-swf Übergangsmetalldichalkogenide (DE-588)4481165-2 gnd rswk-swf Schwarzer Phosphor (DE-588)1189763842 gnd rswk-swf Hyperspektraler Sensor (DE-588)1078791082 gnd rswk-swf Graphen (DE-588)7591667-8 gnd rswk-swf 5\p Materials (DLC)sh85082065 http://id.loc.gov/authorities/subjects/sh85082065 lcsh layer thickness two-dimensional materials microscopy hyperspectral imaging multivariate analysis (DE-588)4113937-9 Hochschulschrift gnd-content Graphen (DE-588)7591667-8 s Übergangsmetalldichalkogenide (DE-588)4481165-2 s Schwarzer Phosphor (DE-588)1189763842 s Mikroskopie (DE-588)4039238-7 s Hyperspektraler Sensor (DE-588)1078791082 s Bildverarbeitung (DE-588)4006684-8 s DE-604 Shaker Verlag (DE-588)1064118135 pbl Erscheint auch als Online-Ausgabe Dong, Xingchen Hyperspectral Imaging Microscopy for Atomic Layer Mapping of Two-Dimensional Materials 1. Auflage Düren : Shaker, 2022 Online-Ressource, 173 Seiten, 60 Illustrationen B:DE-101 application/pdf https://d-nb.info/1252479123/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033913731&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p aepkn-pa 0,88103 20220516 DE-101 https://d-nb.info/provenance/plan#aepkn-pa 2\p dnb 20220907 DE-101 https://d-nb.info/provenance/plan#dnb 3\p dnb 20220907 DE-101 https://d-nb.info/provenance/plan#dnb 4\p dnb 20220907 DE-101 https://d-nb.info/provenance/plan#dnb 5\p aeplcsh-pa 0,07143 20220516 DE-101 https://d-nb.info/provenance/plan#aeplcsh-pa |
spellingShingle | Dong, Xingchen Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials Mikroskopie (DE-588)4039238-7 gnd Bildverarbeitung (DE-588)4006684-8 gnd Übergangsmetalldichalkogenide (DE-588)4481165-2 gnd Schwarzer Phosphor (DE-588)1189763842 gnd Hyperspektraler Sensor (DE-588)1078791082 gnd Graphen (DE-588)7591667-8 gnd 5\p Materials (DLC)sh85082065 http://id.loc.gov/authorities/subjects/sh85082065 lcsh |
subject_GND | (DE-588)4039238-7 (DE-588)4006684-8 (DE-588)4481165-2 (DE-588)1189763842 (DE-588)1078791082 (DE-588)7591667-8 (DLC)sh85082065 http://id.loc.gov/authorities/subjects/sh85082065 (DE-588)4113937-9 |
title | Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials |
title_auth | Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials |
title_exact_search | Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials |
title_exact_search_txtP | Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials |
title_full | Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials Xingchen Dong |
title_fullStr | Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials Xingchen Dong |
title_full_unstemmed | Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials Xingchen Dong |
title_short | Hyperspectral imaging microscopy for atomic layer mapping of two-dimensional materials |
title_sort | hyperspectral imaging microscopy for atomic layer mapping of two dimensional materials |
topic | Mikroskopie (DE-588)4039238-7 gnd Bildverarbeitung (DE-588)4006684-8 gnd Übergangsmetalldichalkogenide (DE-588)4481165-2 gnd Schwarzer Phosphor (DE-588)1189763842 gnd Hyperspektraler Sensor (DE-588)1078791082 gnd Graphen (DE-588)7591667-8 gnd 5\p Materials (DLC)sh85082065 http://id.loc.gov/authorities/subjects/sh85082065 lcsh |
topic_facet | Mikroskopie Bildverarbeitung Übergangsmetalldichalkogenide Schwarzer Phosphor Hyperspektraler Sensor Graphen Materials Hochschulschrift |
url | https://d-nb.info/1252479123/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033913731&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
work_keys_str_mv | AT dongxingchen hyperspectralimagingmicroscopyforatomiclayermappingoftwodimensionalmaterials AT shakerverlag hyperspectralimagingmicroscopyforatomiclayermappingoftwodimensionalmaterials |
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