Colloidal synthesis and ligand exchange of germanium nanoparticles:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin
[2021?]
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Beschreibung: | Tag der mündlichen Prüfung: 04.10.2021 nicht identisch mit anders gebundenem Pflichtexemplar (unterschiedliche Seitenzählung) |
| Beschreibung: | xiii, 108 Seiten Illustrationen, Diagramme (teilweise farbig) |
Internformat
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| 300 | |a xiii, 108 Seiten |b Illustrationen, Diagramme (teilweise farbig) | ||
| 336 | |b txt |2 rdacontent | ||
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Datensatz im Suchindex
| _version_ | 1818737905024106496 |
|---|---|
| adam_text |
CONTENTS
ABSTRACT
IV
ACKNOWLEDGEMENTS
V
LIST
OF
FIGURES
VIII
LIST
OF
TABLES
X
LIST
OF
ABBREVIATIONS
XII
1
INTRODUCTION
1
1.1
INTRODUCTION
.
1
1.2
SCOPE
OF
THE
THESIS
.
7
2
THEORY
9
2.1
NANOPARTICLE
FORMATION
.
9
2.1.1
THERMODYNAMICS
OF
THE
PHASE
TRANSITION
.
10
2.1.2
CLASSICAL
NUCLEATION
THEORY
.
12
2.1.3
HETEROGENEOUS
NUCLEATION
.
14
2.1.4
NUCLEATION
RATE
.
16
2.1.5
CRYSTALLIZATION
BY
PARTICLE
ATTACHMENT
.
17
2.2
SURFACE
CHEMISTRY
.
20
2.2.1
CAPPING
AGENTS
.
20
2.2.2
LIGAND
EXCHANGE
.
22
3
METHODS
AND
MATERIALS
26
3.1
AIR-FREE
TECHNIQUES
.
26
3.1.1
SCHLENK
APPARATUS
.
26
3.2
MATERIALS
AND
METHODS
FOR
THE
NANOPARTICLE
SYNTHESIS
IN
CHAP
TER
4
.
27
3.2.1
MATERIALS
.
28
3.2.2
HOT
INJECTION
SYNTHESIS
.
28
3.3
MATERIALS
AND
METHODS
FOR
THE
CONTROL
OF
GE
NANOPARTICLE
SUR
FACE
CHEMISTRY
IN
CHAPTER
5
.
31
3.3.1
MATERIALS
.
31
3.3.2
SYNTHESIS
OF
OLEYLAMINE-CAPPED
C-GE
NANOPARTICLES
.
.
31
3.3.3
LIGAND
EXCHANGES
.
32
VII
4
NANOPARTICLE
SYNTHESIS
34
4.1
RESULTS
.
34
4.1.1
SOLVENT
SCREENING
.
34
4.1.2
GERMANIUM
TO
SULFUR
RATIO
[GE
:
S]
.
36
4.1.3
PRECURSOR
EFFECT
ON
THE
REACTION
KINETICS
.
38
4.1.4
PARTICLE
SIZE
DISTRIBUTION
.
38
4.1.5
NUCLEAR
MAGNETIC
RESONANCE
INVESTIGATION
.
44
4.2
DISCUSSION
.
47
4.2.1
REACTION
MECHANISM
.
47
4.2.2
DISCREPANCY
BETWEEN
HEXADECYLAMINE
AND
OLEYLAMINE
49
4.3
SUMMARY
AND
CONCLUSION
OF
THE
NANOPARTICLE
SYNTHESIS
.
51
5
SURFACE
CHEMISTRY
CONTROL
OF
GE
NANOPARTICLES
52
5.1
RESULTS
.
56
5.1.1
PRELIMINARY
MORPHOLOGICAL
ASSESSMENT
.
56
5.1.2
THERMAL
EXCHANGE
.
58
5.1.3
CATALYZED
EXCHANGE
.
64
5.2
DISCUSSION
.
69
5.3
SUMMARY
AND
CONCLUSION
OF
THE
SURFACE
CHEMISTRY
CONTROL
OF
GE
NANOPARTICLES
.
71
6
FUTURE
WORK
AND
CONCLUSION
73
6.1
FUTURE
WORK
.
73
6.2
CONCLUSION
.
74
6.3
LIST
OF
PUBLICATIONS
.
76
A
APPENDIX
77
A.L
STATE
OF
THE
ART
OF
THE
GE
NANOPARTICLE
SYNTHESES
.
77
A.
1.1
PHYSICAL
METHODS
OF
SYNTHESIS
.
77
SPUTTERING
AND
EVAPORATION
.
77
PLASMA
SYNTHESIS
AND
LASER
ABLATION
.
78
A.
1.2
CHEMICAL
METHODS
OF
SYNTHESIS
.
78
METATHESIS
.
78
INVERSE
MICELLE
.
79
REDUCTION
OF
GE
HALIDES
WITH
HIGH
BOILING
POINT
SOLVENTS
79
A.2
YIELD
DETERMINATION
OF
THE
GERMANIUM
NANOPARTICLES
SYNTHE
SIZED
IN
OLEYLAMINE
.
80
A.
3
SUPPORTING
INFORMATION
FOR
THE
SURFACE
CHARACTERIZATION
.
82
B
PERMISSIONS
89
B.
L
COPYRIGHTS
.
89
BIBLIOGRAPHY
90
DECLARATION
OF
AUTHORSHIP
108 |
| adam_txt |
CONTENTS
ABSTRACT
IV
ACKNOWLEDGEMENTS
V
LIST
OF
FIGURES
VIII
LIST
OF
TABLES
X
LIST
OF
ABBREVIATIONS
XII
1
INTRODUCTION
1
1.1
INTRODUCTION
.
1
1.2
SCOPE
OF
THE
THESIS
.
7
2
THEORY
9
2.1
NANOPARTICLE
FORMATION
.
9
2.1.1
THERMODYNAMICS
OF
THE
PHASE
TRANSITION
.
10
2.1.2
CLASSICAL
NUCLEATION
THEORY
.
12
2.1.3
HETEROGENEOUS
NUCLEATION
.
14
2.1.4
NUCLEATION
RATE
.
16
2.1.5
CRYSTALLIZATION
BY
PARTICLE
ATTACHMENT
.
17
2.2
SURFACE
CHEMISTRY
.
20
2.2.1
CAPPING
AGENTS
.
20
2.2.2
LIGAND
EXCHANGE
.
22
3
METHODS
AND
MATERIALS
26
3.1
AIR-FREE
TECHNIQUES
.
26
3.1.1
SCHLENK
APPARATUS
.
26
3.2
MATERIALS
AND
METHODS
FOR
THE
NANOPARTICLE
SYNTHESIS
IN
CHAP
TER
4
.
27
3.2.1
MATERIALS
.
28
3.2.2
HOT
INJECTION
SYNTHESIS
.
28
3.3
MATERIALS
AND
METHODS
FOR
THE
CONTROL
OF
GE
NANOPARTICLE
SUR
FACE
CHEMISTRY
IN
CHAPTER
5
.
31
3.3.1
MATERIALS
.
31
3.3.2
SYNTHESIS
OF
OLEYLAMINE-CAPPED
C-GE
NANOPARTICLES
.
.
31
3.3.3
LIGAND
EXCHANGES
.
32
VII
4
NANOPARTICLE
SYNTHESIS
34
4.1
RESULTS
.
34
4.1.1
SOLVENT
SCREENING
.
34
4.1.2
GERMANIUM
TO
SULFUR
RATIO
[GE
:
S]
.
36
4.1.3
PRECURSOR
EFFECT
ON
THE
REACTION
KINETICS
.
38
4.1.4
PARTICLE
SIZE
DISTRIBUTION
.
38
4.1.5
NUCLEAR
MAGNETIC
RESONANCE
INVESTIGATION
.
44
4.2
DISCUSSION
.
47
4.2.1
REACTION
MECHANISM
.
47
4.2.2
DISCREPANCY
BETWEEN
HEXADECYLAMINE
AND
OLEYLAMINE
49
4.3
SUMMARY
AND
CONCLUSION
OF
THE
NANOPARTICLE
SYNTHESIS
.
51
5
SURFACE
CHEMISTRY
CONTROL
OF
GE
NANOPARTICLES
52
5.1
RESULTS
.
56
5.1.1
PRELIMINARY
MORPHOLOGICAL
ASSESSMENT
.
56
5.1.2
THERMAL
EXCHANGE
.
58
5.1.3
CATALYZED
EXCHANGE
.
64
5.2
DISCUSSION
.
69
5.3
SUMMARY
AND
CONCLUSION
OF
THE
SURFACE
CHEMISTRY
CONTROL
OF
GE
NANOPARTICLES
.
71
6
FUTURE
WORK
AND
CONCLUSION
73
6.1
FUTURE
WORK
.
73
6.2
CONCLUSION
.
74
6.3
LIST
OF
PUBLICATIONS
.
76
A
APPENDIX
77
A.L
STATE
OF
THE
ART
OF
THE
GE
NANOPARTICLE
SYNTHESES
.
77
A.
1.1
PHYSICAL
METHODS
OF
SYNTHESIS
.
77
SPUTTERING
AND
EVAPORATION
.
77
PLASMA
SYNTHESIS
AND
LASER
ABLATION
.
78
A.
1.2
CHEMICAL
METHODS
OF
SYNTHESIS
.
78
METATHESIS
.
78
INVERSE
MICELLE
.
79
REDUCTION
OF
GE
HALIDES
WITH
HIGH
BOILING
POINT
SOLVENTS
79
A.2
YIELD
DETERMINATION
OF
THE
GERMANIUM
NANOPARTICLES
SYNTHE
SIZED
IN
OLEYLAMINE
.
80
A.
3
SUPPORTING
INFORMATION
FOR
THE
SURFACE
CHARACTERIZATION
.
82
B
PERMISSIONS
89
B.
L
COPYRIGHTS
.
89
BIBLIOGRAPHY
90
DECLARATION
OF
AUTHORSHIP
108 |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV048321511 |
| illustrated | Illustrated |
| index_date | 2024-07-03T20:12:12Z |
| indexdate | 2024-12-18T01:00:27Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-033700843 |
| open_access_boolean | |
| owner | DE-11 DE-706 |
| owner_facet | DE-11 DE-706 |
| physical | xiii, 108 Seiten Illustrationen, Diagramme (teilweise farbig) |
| publishDate | 2021 |
| publishDateSearch | 2021 |
| publishDateSort | 2021 |
| record_format | marc |
| spelling | Pescara, Bruno Verfasser (DE-588)1262258189 aut Colloidal synthesis and ligand exchange of germanium nanoparticles von M. Sc., Pescara, Bruno Berlin [2021?] xiii, 108 Seiten Illustrationen, Diagramme (teilweise farbig) txt rdacontent n rdamedia nc rdacarrier Tag der mündlichen Prüfung: 04.10.2021 nicht identisch mit anders gebundenem Pflichtexemplar (unterschiedliche Seitenzählung) Germanium (DE-588)4135644-5 gnd rswk-swf Nanopartikel (DE-588)4333369-2 gnd rswk-swf Kolloid (DE-588)4164695-2 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Germanium (DE-588)4135644-5 s Nanopartikel (DE-588)4333369-2 s Kolloid (DE-588)4164695-2 s DE-604 B:DE-101 application/pdf https://d-nb.info/1254189564/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033700843&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Pescara, Bruno Colloidal synthesis and ligand exchange of germanium nanoparticles Germanium (DE-588)4135644-5 gnd Nanopartikel (DE-588)4333369-2 gnd Kolloid (DE-588)4164695-2 gnd |
| subject_GND | (DE-588)4135644-5 (DE-588)4333369-2 (DE-588)4164695-2 (DE-588)4113937-9 |
| title | Colloidal synthesis and ligand exchange of germanium nanoparticles |
| title_auth | Colloidal synthesis and ligand exchange of germanium nanoparticles |
| title_exact_search | Colloidal synthesis and ligand exchange of germanium nanoparticles |
| title_exact_search_txtP | Colloidal synthesis and ligand exchange of germanium nanoparticles |
| title_full | Colloidal synthesis and ligand exchange of germanium nanoparticles von M. Sc., Pescara, Bruno |
| title_fullStr | Colloidal synthesis and ligand exchange of germanium nanoparticles von M. Sc., Pescara, Bruno |
| title_full_unstemmed | Colloidal synthesis and ligand exchange of germanium nanoparticles von M. Sc., Pescara, Bruno |
| title_short | Colloidal synthesis and ligand exchange of germanium nanoparticles |
| title_sort | colloidal synthesis and ligand exchange of germanium nanoparticles |
| topic | Germanium (DE-588)4135644-5 gnd Nanopartikel (DE-588)4333369-2 gnd Kolloid (DE-588)4164695-2 gnd |
| topic_facet | Germanium Nanopartikel Kolloid Hochschulschrift |
| url | https://d-nb.info/1254189564/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033700843&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT pescarabruno colloidalsynthesisandligandexchangeofgermaniumnanoparticles |
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