Porphyrin and Redox Active Ligands-Based Metal Complexes: Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Stuttgart
[2021]
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Beschreibung: | XIX, 288 Seiten Illustrationen, Diagramme 21 cm |
Internformat
MARC
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| 100 | 1 | |a Chandra, Shubhadeep |d 1994- |e Verfasser |0 (DE-588)1253531838 |4 aut | |
| 245 | 1 | 0 | |a Porphyrin and Redox Active Ligands-Based Metal Complexes |b Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds |c vorgelegt von Shubhadeep Chandra ; Hauptberichter: Prof. Biprajit Sarkar |
| 264 | 1 | |a Stuttgart |c [2021] | |
| 300 | |a XIX, 288 Seiten |b Illustrationen, Diagramme |c 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c Universität Stuttgart |d 2021 | ||
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 700 | 1 | |a Sarkar, Biprajit |d 1977- |0 (DE-588)130379549 |4 dgs | |
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Datensatz im Suchindex
| _version_ | 1804184143258451968 |
|---|---|
| adam_text | CONTENTS
LIST
OF
ABBREVIATIONS
VII
RESEARCH
SUMMARY
IX
CHAPTER
1.
INTRODUCTION
1.1.
MESO-MESO
LINKED
AND
FUSED
PORPHYRIN
DIMER
1
1.1.1.
SYNTHESIS
3
1.1.1.1.
SOLUTION-BASED
METHODS
3
1.1.1.2.
ELECTROCHEMICAL
TECHNIQUES
5
1.1.2.
OPTICAL
PROPERTIES
6
1.1.3.
ELECTROCHEMISTRY
8
1.1.4.
MAGNETIC
PROPERTIES
10
1.2.
ELECTROCATALYSIS
11
1.2.1.
OVERPOTENTIAL
(7)
13
1.2.2.
CALCULATION
OF
OBSERVED
RATE-CONSTANT
14
1.2.3.
FOOT-OF-THE-WAVE
ANALYSIS
15
1.2.4.
CATALYTIC
TAFEL
PLOTS
16
1.2.5.
FARADIC
EFFICIENCY
17
1.3.
HYDROGEN
EVOLUTION
REACTION
(HER)
18
1.3.1.
INTRODUCTION
18
1.3.2.
CO(LL)
PORPHYRINS
20
1.3.3.
FE(III)
PORPHYRINS
22
1.3.4.
NI(II)
PORPHYRINS
23
1.3.5.
CU(II)
PORPHYRINS
24
1.4.
DIRADICALS
25
1.4.1.
INTRODUCTION
25
1.4.2.
KEKULE
TYPE
DIRADICALS
28
1.4.3.
APPLICATIONS
OF
DIRADICALS
32
1.5.
AZOCARBOXAMIDE
LIGAND
33
1.6.
TRANSFER
HYDROGENATION
34
1.6.1.
INTRODUCTION
34
1.6.2.
IR
CATALYSTS
CONTAINING
NHC
LIGANDS
35
1.6.3.
IRIDIUM
CYCLOMETALATED
COMPLEXES
(IRIDACYCLES)
36
1.6.4.
IR
CATALYSTS
CONTAINING
TRIAZOLYLIDENE
(TRZ)
LIGANDS
38
IV
1.7.
REFERENCES
39
1.8.
MOTIVATION
52
CHAPTER
2.
REMARKABLE
ENHANCEMENT
OF
CATALYTIC
ACTIVITY
OF
CU-COMPLEXES
TOWARDS
ELECTROCHEMICAL
HYDROGEN
EVOLUTION
REACTION
(HER)
BY
USING
TRIPLY-FUSED
PORPHYRIN:
COMPARATIVE
ANALYSIS
WITH
THE
MONOMERIC
ANALOGUE
2.1.
INTRODUCTION
54
2.2.
RESULTS
AND
DISCUSSION
55
2.2.1.
SYNTHESIS
55
2.2.2.
ELECTROCHEMISTRY
57
2.2.3.
EPR
SPECTROSCOPY
AND
MAGNETIC
PROPERTIES
59
2.2.4.
UV-VIS-NIR
SPECTROELECTROCHEMISTRY
62
2.2.5.
ELECTROCATALYTIC
HER
STUDIES
64
2.2.6.
MECHANISTIC
STUDIES
74
2.3.
CONCLUSION
78
2.4.
EXPERIMENTAL
SECTION
79
2.5.
REFERENCES
85
CHAPTER
3.
INFLUENCE
OF
BULKY
SUBSTITUENT
ON
THE
ENHANCEMENT
OF
ELECTROCHEMICAL
HER
ACTIVITY
OF
BIMETALLIC
NI-CONTAINING
FUSED
PORPHYRIN
ANALOGUES
3.1.
INTRODUCTION
89
3.2.
RESULTS
AND
DISCUSSION
92
3.2.1.
SYNTHESIS
AND
CHARACTERIZATION
92
3.2.2.
ELECTROCHEMISTRY
93
3.2.3.
UV-VIS-NIR
SPECTROSCOPY
95
3.2.4.
ELECTROCATALYSIS
97
3.2.5.
MECHANISTIC
STUDIES
103
3.3.
CONCLUSION
106
3.4.
EXPERIMENTAL
SECTION
107
3.5.
REFERENCES
117
CHAPTER
4.
ELECTRONIC
AND
MAGNETIC
INTERACTION
IN
A
MESO-MESO
LINKED
AG(II)/AG(II)
,
CU(II)/CU(II)
AND
AU(II)/AU(II)
PORPHYRIN
DIMERS
UPON
STEPWISE
OXIDATION
4.1.
INTRODUCTION
121
4.2.
RESULTS
AND
DISCUSSION
123
4.2.1.
SYNTHESIS
AND
X-RAY
CRYSTALLOGRAPHY
123
4.2.2.
CYCLIC
VOLTAMMETRY
125
V
4.2.3.
UV-VIS
AND
UV-VIS
SEC
129
4.2.4.
MAGNETIC
MEASUREMENTS
134
4.2.5.
EPR
SPECTROSCOPY
135
4.3.
CONCLUSION
142
4.4.
EXPERIMENTAL
SECTION
143
4.5.
REFERENCES
151
CHAPTER
5.
ACYCLIC
DIAMINOCARBENE-BASED
THIELE,
CHICHIBABIN
AND
MULLER
HYDROCARBONS
5.1.
INTRODUCTION
155
5.2.
RESULTS
AND
DISCUSSION
156
5.3.
CONCLUSION
168
5.4.
EXPERIMENTAL
SECTION
169
5.5.
REFERENCES
179
CHAPTER
6.
IRIDIUM
AZOCARBOXAMIDE
COMPLEXES:
VARIABLE
COORDINATION
MODES,
C-H
ACTIVATION,
TRANSFER
HYDROGENATION
CATALYSIS
AND
MECHANISTIC
INSIGHTS
6.1.
INTRODUCTION
182
6.2.
RESULTS
AND
DISCUSSION
184
6.2.1.
SYNTHESIS
AND
CHARACTERIZATION
184
6.2.2.
X-RAY
DIFFRACTION
187
6.2.3.
ELECTROCHEMISTRY
AND
TRANSFER
HYDROGENATION
190
6.3.
CONCLUSION
197
6.4.
EXPERIMENTAL
SECTION
198
6.5.
REFERENCES
201
7
APPENDIX
205
CURRICULUM
VITAE
286
VI
|
| adam_txt |
CONTENTS
LIST
OF
ABBREVIATIONS
VII
RESEARCH
SUMMARY
IX
CHAPTER
1.
INTRODUCTION
1.1.
MESO-MESO
LINKED
AND
FUSED
PORPHYRIN
DIMER
1
1.1.1.
SYNTHESIS
3
1.1.1.1.
SOLUTION-BASED
METHODS
3
1.1.1.2.
ELECTROCHEMICAL
TECHNIQUES
5
1.1.2.
OPTICAL
PROPERTIES
6
1.1.3.
ELECTROCHEMISTRY
8
1.1.4.
MAGNETIC
PROPERTIES
10
1.2.
ELECTROCATALYSIS
11
1.2.1.
OVERPOTENTIAL
(7)
13
1.2.2.
CALCULATION
OF
OBSERVED
RATE-CONSTANT
14
1.2.3.
FOOT-OF-THE-WAVE
ANALYSIS
15
1.2.4.
CATALYTIC
TAFEL
PLOTS
16
1.2.5.
FARADIC
EFFICIENCY
17
1.3.
HYDROGEN
EVOLUTION
REACTION
(HER)
18
1.3.1.
INTRODUCTION
18
1.3.2.
CO(LL)
PORPHYRINS
20
1.3.3.
FE(III)
PORPHYRINS
22
1.3.4.
NI(II)
PORPHYRINS
23
1.3.5.
CU(II)
PORPHYRINS
24
1.4.
DIRADICALS
25
1.4.1.
INTRODUCTION
25
1.4.2.
KEKULE
TYPE
DIRADICALS
28
1.4.3.
APPLICATIONS
OF
DIRADICALS
32
1.5.
AZOCARBOXAMIDE
LIGAND
33
1.6.
TRANSFER
HYDROGENATION
34
1.6.1.
INTRODUCTION
34
1.6.2.
IR
CATALYSTS
CONTAINING
NHC
LIGANDS
35
1.6.3.
IRIDIUM
CYCLOMETALATED
COMPLEXES
(IRIDACYCLES)
36
1.6.4.
IR
CATALYSTS
CONTAINING
TRIAZOLYLIDENE
(TRZ)
LIGANDS
38
IV
1.7.
REFERENCES
39
1.8.
MOTIVATION
52
CHAPTER
2.
REMARKABLE
ENHANCEMENT
OF
CATALYTIC
ACTIVITY
OF
CU-COMPLEXES
TOWARDS
ELECTROCHEMICAL
HYDROGEN
EVOLUTION
REACTION
(HER)
BY
USING
TRIPLY-FUSED
PORPHYRIN:
COMPARATIVE
ANALYSIS
WITH
THE
MONOMERIC
ANALOGUE
2.1.
INTRODUCTION
54
2.2.
RESULTS
AND
DISCUSSION
55
2.2.1.
SYNTHESIS
55
2.2.2.
ELECTROCHEMISTRY
57
2.2.3.
EPR
SPECTROSCOPY
AND
MAGNETIC
PROPERTIES
59
2.2.4.
UV-VIS-NIR
SPECTROELECTROCHEMISTRY
62
2.2.5.
ELECTROCATALYTIC
HER
STUDIES
64
2.2.6.
MECHANISTIC
STUDIES
74
2.3.
CONCLUSION
78
2.4.
EXPERIMENTAL
SECTION
79
2.5.
REFERENCES
85
CHAPTER
3.
INFLUENCE
OF
BULKY
SUBSTITUENT
ON
THE
ENHANCEMENT
OF
ELECTROCHEMICAL
HER
ACTIVITY
OF
BIMETALLIC
NI-CONTAINING
FUSED
PORPHYRIN
ANALOGUES
3.1.
INTRODUCTION
89
3.2.
RESULTS
AND
DISCUSSION
92
3.2.1.
SYNTHESIS
AND
CHARACTERIZATION
92
3.2.2.
ELECTROCHEMISTRY
93
3.2.3.
UV-VIS-NIR
SPECTROSCOPY
95
3.2.4.
ELECTROCATALYSIS
97
3.2.5.
MECHANISTIC
STUDIES
103
3.3.
CONCLUSION
106
3.4.
EXPERIMENTAL
SECTION
107
3.5.
REFERENCES
117
CHAPTER
4.
ELECTRONIC
AND
MAGNETIC
INTERACTION
IN
A
MESO-MESO
LINKED
AG(II)/AG(II)
,
CU(II)/CU(II)
AND
AU(II)/AU(II)
PORPHYRIN
DIMERS
UPON
STEPWISE
OXIDATION
4.1.
INTRODUCTION
121
4.2.
RESULTS
AND
DISCUSSION
123
4.2.1.
SYNTHESIS
AND
X-RAY
CRYSTALLOGRAPHY
123
4.2.2.
CYCLIC
VOLTAMMETRY
125
V
4.2.3.
UV-VIS
AND
UV-VIS
SEC
129
4.2.4.
MAGNETIC
MEASUREMENTS
134
4.2.5.
EPR
SPECTROSCOPY
135
4.3.
CONCLUSION
142
4.4.
EXPERIMENTAL
SECTION
143
4.5.
REFERENCES
151
CHAPTER
5.
ACYCLIC
DIAMINOCARBENE-BASED
THIELE,
CHICHIBABIN
AND
MULLER
HYDROCARBONS
5.1.
INTRODUCTION
155
5.2.
RESULTS
AND
DISCUSSION
156
5.3.
CONCLUSION
168
5.4.
EXPERIMENTAL
SECTION
169
5.5.
REFERENCES
179
CHAPTER
6.
IRIDIUM
AZOCARBOXAMIDE
COMPLEXES:
VARIABLE
COORDINATION
MODES,
C-H
ACTIVATION,
TRANSFER
HYDROGENATION
CATALYSIS
AND
MECHANISTIC
INSIGHTS
6.1.
INTRODUCTION
182
6.2.
RESULTS
AND
DISCUSSION
184
6.2.1.
SYNTHESIS
AND
CHARACTERIZATION
184
6.2.2.
X-RAY
DIFFRACTION
187
6.2.3.
ELECTROCHEMISTRY
AND
TRANSFER
HYDROGENATION
190
6.3.
CONCLUSION
197
6.4.
EXPERIMENTAL
SECTION
198
6.5.
REFERENCES
201
7
APPENDIX
205
CURRICULUM
VITAE
286
VI |
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| author | Chandra, Shubhadeep 1994- |
| author_GND | (DE-588)1253531838 (DE-588)130379549 |
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| illustrated | Illustrated |
| index_date | 2024-07-03T20:06:31Z |
| indexdate | 2024-07-10T09:34:39Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-033680846 |
| oclc_num | 1334028753 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR |
| owner_facet | DE-355 DE-BY-UBR |
| physical | XIX, 288 Seiten Illustrationen, Diagramme 21 cm |
| publishDate | 2021 |
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| spelling | Chandra, Shubhadeep 1994- Verfasser (DE-588)1253531838 aut Porphyrin and Redox Active Ligands-Based Metal Complexes Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds vorgelegt von Shubhadeep Chandra ; Hauptberichter: Prof. Biprajit Sarkar Stuttgart [2021] XIX, 288 Seiten Illustrationen, Diagramme 21 cm txt rdacontent n rdamedia nc rdacarrier Dissertation Universität Stuttgart 2021 (DE-588)4113937-9 Hochschulschrift gnd-content Sarkar, Biprajit 1977- (DE-588)130379549 dgs B:DE-101 application/pdf https://d-nb.info/1255032960/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033680846&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p dnb 20220428 DE-101 https://d-nb.info/provenance/plan#dnb |
| spellingShingle | Chandra, Shubhadeep 1994- Porphyrin and Redox Active Ligands-Based Metal Complexes Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds |
| subject_GND | (DE-588)4113937-9 |
| title | Porphyrin and Redox Active Ligands-Based Metal Complexes Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds |
| title_auth | Porphyrin and Redox Active Ligands-Based Metal Complexes Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds |
| title_exact_search | Porphyrin and Redox Active Ligands-Based Metal Complexes Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds |
| title_exact_search_txtP | Porphyrin and Redox Active Ligands-Based Metal Complexes Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds |
| title_full | Porphyrin and Redox Active Ligands-Based Metal Complexes Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds vorgelegt von Shubhadeep Chandra ; Hauptberichter: Prof. Biprajit Sarkar |
| title_fullStr | Porphyrin and Redox Active Ligands-Based Metal Complexes Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds vorgelegt von Shubhadeep Chandra ; Hauptberichter: Prof. Biprajit Sarkar |
| title_full_unstemmed | Porphyrin and Redox Active Ligands-Based Metal Complexes Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds vorgelegt von Shubhadeep Chandra ; Hauptberichter: Prof. Biprajit Sarkar |
| title_short | Porphyrin and Redox Active Ligands-Based Metal Complexes |
| title_sort | porphyrin and redox active ligands based metal complexes studies on electrocatalytic activity and electronic structure of redox active compounds |
| title_sub | Studies on Electrocatalytic Activity and Electronic Structure of Redox-Active Compounds |
| topic_facet | Hochschulschrift |
| url | https://d-nb.info/1255032960/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033680846&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT chandrashubhadeep porphyrinandredoxactiveligandsbasedmetalcomplexesstudiesonelectrocatalyticactivityandelectronicstructureofredoxactivecompounds AT sarkarbiprajit porphyrinandredoxactiveligandsbasedmetalcomplexesstudiesonelectrocatalyticactivityandelectronicstructureofredoxactivecompounds |
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