Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Hamburg
2021
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Physical Description: | 103 Seiten Illustrationen, Diagramme 21 cm |
Staff View
MARC
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|---|---|---|---|
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| 100 | 1 | |a Pelzer, Tristan |e Verfasser |0 (DE-588)1234592010 |4 aut | |
| 245 | 1 | 0 | |a Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates |c submitted by Tristan Pelzer |
| 264 | 1 | |a Hamburg |c 2021 | |
| 300 | |a 103 Seiten |b Illustrationen, Diagramme |c 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c University of Hamburg |d 2021 | ||
| 650 | 0 | 7 | |a Kunststoffherstellung |0 (DE-588)4300399-0 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Oxazolidinone |0 (DE-588)4136163-5 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Oxazolidinone |0 (DE-588)4136163-5 |D s |
| 689 | 0 | 1 | |a Kunststoffherstellung |0 (DE-588)4300399-0 |D s |
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Record in the Search Index
| _version_ | 1804183146727473152 |
|---|---|
| adam_text | II.
TABLE
OF
CONTENT
1.
KURZZUSAMMENFASSUNG
...........................................................................................................
1
2.
ABSTRACT
...................................................................................................................................
3
3.
INTRODUCTION
............................................................................................................................
5
4.
STATE
OF
THE
ART
.......................................................................................................................
9
4.1.
PATHWAYS
OF
OXAZOLIDINONE
SYNTHESIS
..........................................................................
9
4.1.1.
COMBINATION
REACTIONS
............................................................................................
9
4.1.2.
CYCLIZATION
REACTIONS
............................................................................................
12
4.1.3.
CONVERSION
REACTIONS
............................................................................................
13
4.2.
LITERATURE
KNOWN
CATALYSTS
FOR
THE
REACTION
OF
EPOXIDE
WITH
ISOCYANATE
TOWARDS
OXAZOLIDINONE
...........................................................................................................................
14
5.
MOTIVATION
AND
OBJECTIVES
...................................................................................................
17
6.
RESULTS
AND
DISCUSSION
.......................................................................................................
19
6.1.
GENERAL
REMARKS
ON
CHEMICALS
AND
ANALYTICAL
TECHNIQUES
USED
...............................
20
6.1.1.
CHEMICALS
AND
MODEL
SYSTEM
..............................................................................20
6.1.2.
ANALYTICAL
TECHNIQUES
............................................................................................
21
6.1.2.1.
INFRARED
SPECTROSCOPY
..........................................................................................
21
6.1.2.2.
NUCLEAR
MAGNETIC
RESONANCE
SPECTROSCOPY
.......................................................
25
6.2.
TETRABUTYL
AMMONIUM
HALIDES
AND
TRIHALIDES
BY
ADDITION
OF
IODINE
...........................27
6.2.1.
STUDY
ON
THE
SYNTHESIS
OF
OXAZOLIDINONES
CATALYZED
BY
TETRA-N-BUTYL
AMMONIUM
HALIDES
...............................................................................................................................
27
6.2.2.
STUDY
ON
THE
SYNTHESIS
OF
OXAZOLIDINONES
CATALYZED
BY
TETRABUTYL
AMMONIUM
HALIDES
WITH
ADDITION
OF
IODINE
.............................................................................................
36
6.2.3.
INTERIM
CONCLUDING
SUMMARY
ON
TBAX
AND
TBAX/I
2
CATALYSIS
...........................
41
6.3.
POLYMER
SHEET
SYNTHESIS
..............................................................................................
43
6.3.1.
EXPERIMENTAL
SETUP
...............................................................................................
43
6.3.2.
RESULTS
AND
DISCUSSION
ON
POLYMER
SHEET
SYNTHESIS
.........................................
44
6.3.3.
MECHANICAL
AND
THERMAL
PROPERTIES
OF
THE
POLYOXAZOLIDINONE
MATERIALS
...........
54
6.3.4. INTERIM
CONCLUDING
SUMMARY
ON
TBAX/I2
POLYMER
SHEET
SYNTHESIS
....................
58
6.4.
TRIPHENYLANTIMONY
AND
IODINE
......................................................................................60
6.4.1.
RESULTS
AND
DISCUSSION
ON
EXPERIMENTS
PERFORMED
.............................................
60
6.4.2.
INTERIM
CONCLUDING
SUMMARY
ON
PH
3
SB/L2
CATALYSIS
.............................................
66
7.
SUMMARY
...............................................................................................................................
67
8.
EXPERIMENTAL
SECTION
............................................................................................................
73
8.1.
MATERIALS
AND
METHODS
.................................................................................................
73
8.1.1.
MATERIALS
................................................................................................................
73
8.1.2.
INSTRUMENTS
AND
DATA
TREATMENT
...........................................................................
73
8.2.
GENERAL
REACTIONS
PROCEDURES
AND
INSTRUCTIONS
............................................................
74
8.2.1.
OCGE
AND
MDI
COUPLING
REACTIONS
.......................................................................
74
8.2.1.1.
EPOXIDE
MDI
COUPLING
REACTIONS
USING
TETRA-N-BUTYL
AMMONIUM
HALIDES
(CL,
BR,
I)
............................................................................................................................
74
8.2.1.2.
EPOXIDE
MDI
COUPLING
REACTIONS
USING
TETRA-N-BUTYL
AMMONIUM
HALIDES
(CL,
BR,
I)
WITH
IODINE
..........................................................................................................................
75
8.2.2.
BADGE
AND
MDI
POLYMER
SHEET
SYNTHESIS
.........................................................
76
8.2.2.1.
PREPARATION
OF
THE
CATALYST
MIXTURE
TBAX+K
...................................................
76
8.2.2.2.
SYNTHESIS
OF
OXAZOLIDINONE
ISOCYANURATE
POLYMER
SHEETS
FROM
BADGE
AND
MDI
CATALYZED
BY
TBAX
+
L
2
................................................................................................
77
8.2.3.
TRIPHENYLANTIMONY
IODINE
......................................................................................
79
8.2.3.1.
GENERAL
REACTION
PROCEDURE
6:
OCGE
MDI
COUPLING
REACTIONS
CATALYZED
BY
TRIPHENYLANTIMONY
AND
IODINE
...............................................................................................
79
9.
LITERATURE
...............................................................................................................................
81
10.
APPENDIX
...............................................................................................................................
87
10.1.
REACTION
DETAILS
FROM
DFT
LEVEL
CALCULATIONS
ON
TRIPHENYLANTIMONY
AND
IODINE
...87
10.1.
HAZARDOUS
MATERIAL
...................................................................................................
92
10.2.
LIST
OF
FIGURES
.............................................................................................................
95
10.3.
LIST
OF
SCHEMES
.........................................................................................................
97
10.4.
LIST
OF
TABLES
.............................................................................................................
98
11.
DANKSAGUNG
........................................................................................................................
101
12.
EIDESSTATTLICHE
VERSICHERUNG
.............................................................................................
103
|
| adam_txt |
II.
TABLE
OF
CONTENT
1.
KURZZUSAMMENFASSUNG
.
1
2.
ABSTRACT
.
3
3.
INTRODUCTION
.
5
4.
STATE
OF
THE
ART
.
9
4.1.
PATHWAYS
OF
OXAZOLIDINONE
SYNTHESIS
.
9
4.1.1.
COMBINATION
REACTIONS
.
9
4.1.2.
CYCLIZATION
REACTIONS
.
12
4.1.3.
CONVERSION
REACTIONS
.
13
4.2.
LITERATURE
KNOWN
CATALYSTS
FOR
THE
REACTION
OF
EPOXIDE
WITH
ISOCYANATE
TOWARDS
OXAZOLIDINONE
.
14
5.
MOTIVATION
AND
OBJECTIVES
.
17
6.
RESULTS
AND
DISCUSSION
.
19
6.1.
GENERAL
REMARKS
ON
CHEMICALS
AND
ANALYTICAL
TECHNIQUES
USED
.
20
6.1.1.
CHEMICALS
AND
MODEL
SYSTEM
.20
6.1.2.
ANALYTICAL
TECHNIQUES
.
21
6.1.2.1.
INFRARED
SPECTROSCOPY
.
21
6.1.2.2.
NUCLEAR
MAGNETIC
RESONANCE
SPECTROSCOPY
.
25
6.2.
TETRABUTYL
AMMONIUM
HALIDES
AND
TRIHALIDES
BY
ADDITION
OF
IODINE
.27
6.2.1.
STUDY
ON
THE
SYNTHESIS
OF
OXAZOLIDINONES
CATALYZED
BY
TETRA-N-BUTYL
AMMONIUM
HALIDES
.
27
6.2.2.
STUDY
ON
THE
SYNTHESIS
OF
OXAZOLIDINONES
CATALYZED
BY
TETRABUTYL
AMMONIUM
HALIDES
WITH
ADDITION
OF
IODINE
.
36
6.2.3.
INTERIM
CONCLUDING
SUMMARY
ON
TBAX
AND
TBAX/I
2
CATALYSIS
.
41
6.3.
POLYMER
SHEET
SYNTHESIS
.
43
6.3.1.
EXPERIMENTAL
SETUP
.
43
6.3.2.
RESULTS
AND
DISCUSSION
ON
POLYMER
SHEET
SYNTHESIS
.
44
6.3.3.
MECHANICAL
AND
THERMAL
PROPERTIES
OF
THE
POLYOXAZOLIDINONE
MATERIALS
.
54
6.3.4. INTERIM
CONCLUDING
SUMMARY
ON
TBAX/I2
POLYMER
SHEET
SYNTHESIS
.
58
6.4.
TRIPHENYLANTIMONY
AND
IODINE
.60
6.4.1.
RESULTS
AND
DISCUSSION
ON
EXPERIMENTS
PERFORMED
.
60
6.4.2.
INTERIM
CONCLUDING
SUMMARY
ON
PH
3
SB/L2
CATALYSIS
.
66
7.
SUMMARY
.
67
8.
EXPERIMENTAL
SECTION
.
73
8.1.
MATERIALS
AND
METHODS
.
73
8.1.1.
MATERIALS
.
73
8.1.2.
INSTRUMENTS
AND
DATA
TREATMENT
.
73
8.2.
GENERAL
REACTIONS
PROCEDURES
AND
INSTRUCTIONS
.
74
8.2.1.
OCGE
AND
MDI
COUPLING
REACTIONS
.
74
8.2.1.1.
EPOXIDE
MDI
COUPLING
REACTIONS
USING
TETRA-N-BUTYL
AMMONIUM
HALIDES
(CL,
BR,
I)
.
74
8.2.1.2.
EPOXIDE
MDI
COUPLING
REACTIONS
USING
TETRA-N-BUTYL
AMMONIUM
HALIDES
(CL,
BR,
I)
WITH
IODINE
.
75
8.2.2.
BADGE
AND
MDI
POLYMER
SHEET
SYNTHESIS
.
76
8.2.2.1.
PREPARATION
OF
THE
CATALYST
MIXTURE
TBAX+K
.
76
8.2.2.2.
SYNTHESIS
OF
OXAZOLIDINONE
ISOCYANURATE
POLYMER
SHEETS
FROM
BADGE
AND
MDI
CATALYZED
BY
TBAX
+
L
2
.
77
8.2.3.
TRIPHENYLANTIMONY
IODINE
.
79
8.2.3.1.
GENERAL
REACTION
PROCEDURE
6:
OCGE
MDI
COUPLING
REACTIONS
CATALYZED
BY
TRIPHENYLANTIMONY
AND
IODINE
.
79
9.
LITERATURE
.
81
10.
APPENDIX
.
87
10.1.
REACTION
DETAILS
FROM
DFT
LEVEL
CALCULATIONS
ON
TRIPHENYLANTIMONY
AND
IODINE
.87
10.1.
HAZARDOUS
MATERIAL
.
92
10.2.
LIST
OF
FIGURES
.
95
10.3.
LIST
OF
SCHEMES
.
97
10.4.
LIST
OF
TABLES
.
98
11.
DANKSAGUNG
.
101
12.
EIDESSTATTLICHE
VERSICHERUNG
.
103 |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
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| id | DE-604.BV047668801 |
| illustrated | Illustrated |
| index_date | 2024-07-03T18:54:40Z |
| indexdate | 2024-07-10T09:18:49Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-033053493 |
| oclc_num | 1262745436 |
| open_access_boolean | |
| owner | DE-29T DE-83 |
| owner_facet | DE-29T DE-83 |
| physical | 103 Seiten Illustrationen, Diagramme 21 cm |
| publishDate | 2021 |
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| record_format | marc |
| spelling | Pelzer, Tristan Verfasser (DE-588)1234592010 aut Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates submitted by Tristan Pelzer Hamburg 2021 103 Seiten Illustrationen, Diagramme 21 cm txt rdacontent n rdamedia nc rdacarrier Dissertation University of Hamburg 2021 Kunststoffherstellung (DE-588)4300399-0 gnd rswk-swf Oxazolidinone (DE-588)4136163-5 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Oxazolidinone (DE-588)4136163-5 s Kunststoffherstellung (DE-588)4300399-0 s DE-604 B:DE-101 application/pdf https://d-nb.info/1233824112/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033053493&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p dnb 20210715 DE-101 https://d-nb.info/provenance/plan#dnb |
| spellingShingle | Pelzer, Tristan Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates Kunststoffherstellung (DE-588)4300399-0 gnd Oxazolidinone (DE-588)4136163-5 gnd |
| subject_GND | (DE-588)4300399-0 (DE-588)4136163-5 (DE-588)4113937-9 |
| title | Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates |
| title_auth | Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates |
| title_exact_search | Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates |
| title_exact_search_txtP | Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates |
| title_full | Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates submitted by Tristan Pelzer |
| title_fullStr | Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates submitted by Tristan Pelzer |
| title_full_unstemmed | Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates submitted by Tristan Pelzer |
| title_short | Catalytic synthesis and characterization of oxazolidin-2-one based polymers from epoxides and isocyanates |
| title_sort | catalytic synthesis and characterization of oxazolidin 2 one based polymers from epoxides and isocyanates |
| topic | Kunststoffherstellung (DE-588)4300399-0 gnd Oxazolidinone (DE-588)4136163-5 gnd |
| topic_facet | Kunststoffherstellung Oxazolidinone Hochschulschrift |
| url | https://d-nb.info/1233824112/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033053493&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT pelzertristan catalyticsynthesisandcharacterizationofoxazolidin2onebasedpolymersfromepoxidesandisocyanates |
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