Analytical chemistry: principles and practice
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin ; Boston
De Gruyter
[2022]
|
| Schriftenreihe: | De Gruyter graduate
|
| Schlagworte: | |
| Online-Zugang: | https://www.degruyter.com/isbn/9783110721195 Inhaltsverzeichnis |
| Beschreibung: | XII, 302 Seiten Illustrationen, Diagramme |
| ISBN: | 9783110721195 |
Internformat
MARC
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| 015 | |a 21,N24 |2 dnb | ||
| 016 | 7 | |a 1235281701 |2 DE-101 | |
| 020 | |a 9783110721195 |c pbk. |9 978-3-11-072119-5 | ||
| 035 | |a (OCoLC)1294507256 | ||
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| 100 | 1 | |a Soffiantini, Vic |e Verfasser |0 (DE-588)1250015405 |4 aut | |
| 245 | 1 | 0 | |a Analytical chemistry |b principles and practice |c Vic Soffiantini |
| 264 | 1 | |a Berlin ; Boston |b De Gruyter |c [2022] | |
| 264 | 4 | |c © 2022 | |
| 300 | |a XII, 302 Seiten |b Illustrationen, Diagramme | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a De Gruyter graduate | |
| 650 | 0 | 7 | |a Analytische Chemie |0 (DE-588)4129906-1 |2 gnd |9 rswk-swf |
| 653 | |a Chemische Analyse | ||
| 653 | |a Instrumentelle Analyse | ||
| 653 | |a Analytik | ||
| 689 | 0 | 0 | |a Analytische Chemie |0 (DE-588)4129906-1 |D s |
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| 710 | 2 | |a Walter de Gruyter GmbH & Co. KG |0 (DE-588)10095502-2 |4 pbl | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, EPUB |z 978-3-11-072121-8 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, PDF |z 978-3-11-072120-1 |
| 856 | 4 | 2 | |m X:MVB |u https://www.degruyter.com/isbn/9783110721195 |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033034429&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-033034429 | ||
Datensatz im Suchindex
| _version_ | 1804183114194354176 |
|---|---|
| adam_text | CONTENTS
PREFACE
-
V
INTRODUCTION
-
1
CHAPTER
1
ANALYTICAL
CHEMISTRY
----
3
CHAPTER
2
LABORATORY
OPERATIONS
----
7
CHAPTER
3
PLANNING
THE
ANALYSIS
-
31
CHAPTER 4
SAMPLING
----
35
INSTRUMENTAL
ANALYSIS
CHAPTER
5
CALORIMETRY
-
51
CHAPTER 6
CHROMATOGRAPHY
----
55
6.1
COLUMN
CHROMATOGRAPHY
----
57
6.2
GAS-LIQUID
CHROMATOGRAPHY
----
57
6.3
HIGH-PERFORMANCE
LIQUID
CHROMATOGRAPHY
----
63
6.4
ION
CHROMATOGRAPHY
----
65
6.5
PAPER
CHROMATOGRAPHY
----
66
6.6
THIN-LAYER
CHROMATOGRAPHY
----
67
CHAPTER
7
CONDUCTOMETRY
-
71
CHAPTER 8
COULOMETRIC
ANALYSIS
-
79
CHAPTER
9
POTENTIOMETRY
----
83
VIII
-
CONTENTS
CHAPTER
10
POLARIMETRY
----
89
CHAPTER
11
TURBIDIMETRY
AND
NEPHELOMETRY
----
95
CHAPTER
12
POLAROGRAPHY
(VOLTAMMETRY)
-
97
CHAPTER
13
REFRACTOMETRY
-
99
CHAPTER
14
SPECTROPHOTOMETRY
----
103
14.1
COLORIMETRY
----
107
14.2
COLOUR
SCALES
----
108
14.3
ULTRAVIOLET
AND
VISIBLE
SPECTROPHOTOMETRY
-----109
14.4
INFRARED
SPECTROPHOTOMETRY
----
114
14.5
FTIR
SPECTROPHOTOMETRY
----
114
14.6
NEAR-INFRARED
SPECTROPHOTOMETRY
----
117
14.7
RAMAN
SPECTROPHOTOMETRY
----
118
14.8
MASS
SPECTROPHOTOMETRY
----
118
14.9
ATOMIC
ABSORPTION
SPECTROPHOTOMETRY
----
119
14.10
INDUCTIVELY
COUPLED
SPECTROPHOTOMETRY
----
125
14.11
REFLECTANCE
SPECTROPHOTOMETRY
----
127
14.12
FLUORESCENCE
SPECTROSCOPY
----
128
14.12.1
PHYSICAL
MEASUREMENTS
-----129
PHYSICAL
MEASUREMENTS
CHAPTER
15
VISCOSITY
----
133
CHAPTER
16
DENSITY
-
139
16.1
HYDROMETERS
----
141
CHAPTER
17
PARTICLE
ANALYSIS
-
147
17.1
GEL
PERMEATION
CHROMATOGRAPHY
-
147
17.2
TEST
SIEVE
ANALYSIS
----
148
CONTENTS
-
IX
17.3
PARTICLE
COUNTERS
----
151
17.4
IMAGING
----
151
CHAPTER
18
SURFACE
TENSION
-
153
18.1
CHEMICAL
ANALYSIS
----
154
CHAPTER
19
CHEMICAL
ANALYSIS
-
157
19.1
ELECTROCHEMICAL
SERIES
----
157
19.2
NOMENCLATURE
OF
ACIDS
-
158
19.3
VALENCIES
----
158
19.4
CHEMICAL
REAGENTS
-----160
19.4.1
PREPARATION
OF
SOME
COMMON
LABORATORY
SOLUTIONS
OR
REAGENTS
-----163
19.4.2
DILUTION
FORMULA
----
164
19.4.3
PREPARATION
OF
AAS
STANDARD
AQUEOUS
SOLUTIONS
----
164
CHAPTER
20
GRAVIMETRIC
ANALYSIS
-
167
20.1
CO-PRECIPITATION
----
168
20.2
POST-PRECIPITATION
---169
CHAPTER
21
VOLUMETRIC
ANALYSIS
(TITRIMETRIC)
-
171
21.1
TITRATIONS
----
172
21.2
INDICATORS
-
175
21.3
COULOMETRIC
TITRATIONS
-----
176
21.4
ARGENTOMETRIC
TITRATIONS
-
177
21.5
NEUTRALISATION
TITRATIONS
(ACIDS
AND
BASES)
-
178
21.6
NEUTRALISATION
TITRATIONS
(ACIDS
AND
BASES)
-
180
21.7
REDOX
(REDUCTION-OXIDATION)
TITRATIONS
-
181
21.8
PRECIPITATION
TITRATIONS
-
182
21.9
COMPLEXOMETRIC
TITRATIONS
-
183
CHAPTER
22
REACTIONS
WITH
IODINE
-
185
22.1
LODIMETRY
-----
185
22.2
IODOMETRY
----
185
X
-
CONTENTS
CHAPTER
23
QUALITATIVE
CHEMICAL
ANALYSIS
-
187
DATA
CHAPTER
24
DATA
INTERPRETATION
-
197
24.1
THE
T-TEST:
(AKA
STUDENT
S
T-TEST)
----
199
24.2
THE
Q-TEST
(OR
GRUBBS
TEST)
----
199
24.3
THE
F-TEST
----
200
24.4
GANTT
CHARTS
----
200
24.5
CONTROL
CHARTS
----
200
24.6
REGRESSION
ANALYSIS
----
201
24.7
CALIBRATION
OF
INSTRUMENTATION
-----
202
24.8
VALIDATION
OF
ANALYTICAL
TEST
METHODS
----
203
24.9
MEASUREMENT
OF
ERRORS
----
207
CHAPTER
25
LABORATORY
REPORTS
-
215
25.1
WHAT
ARE
SIGNIFICANT
FIGURES?
----
215
25.2
THE
REPORT
----
217
APPENDICES
APPENDIX
I
LABORATORY
SAFETY
AND
CHECKLISTS
-
223
APPENDIX
II
INTERNATIONALLY
ACCEPTED
LABORATORY
PROCEDURES
AND
TEST
METHODS
-
233
APPENDIX
III
STRENGTHS
OF
COMMON
CONCENTRATED
ACIDS
-
235
APPENDIX
IV
UNITS
OF
MEASUREMENT
AND
CONCENTRATION
-
237
APPENDIX
V
INTERNATIONAL
SYSTEM
(SI)
OF
UNITS
-
241
APPENDIX
VI
METRIC
(SI)
PREFIXES
AND
DECIMAL
UNIT
MULTIPLES
-
243
CONTENTS
-
-
XI
APPENDIX
VII
TEMPERATURE
SCALES
AND
CONVERSIONS
-
245
APPENDIX
VIII
VACUUM
UNITS
-
247
APPENDIX
IX
PRESSURE
UNITS
-
249
APPENDIX
X
AUTOCLAVE
STEAM
PRESSURE
AND
TEMPERATURE
-
251
APPENDIX
XI
DRYING
AGENTS
-
DESICCANTS
-
253
APPENDIX
XII
CONSTANT
HUMIDITY
SOLUTIONS
-
255
APPENDIX
XIII
FREEZING
MIXTURES
-
257
APPENDIX
XIV
RATE
OF
FLOW
UNITS
----
259
APPENDIX
XV
DETECTION
LIMITS
IN
ATOMIC
SPECTROSCOPY
-
261
APPENDIX
XVI
OXIDATION
STATES
-
265
APPENDIX
XVII
COMMODITY
PROPERTIES
----
267
APPENDIX
XVIII
PROPERTIES
OF
METALS
AND
ALLOYS
-
269
APPENDIX
XIX
CARE
OF
PLATINUM
APPARATUS
-
271
APPENDIX
XX
PERIODIC
TABLE
-
273
XII
-
CONTENTS
GLOSSARY
OF
TERMS
----
275
QUIZ
----
287
QUESTIONS
----
287
ANSWERS
----
289
INDEX
----
295
|
| adam_txt |
CONTENTS
PREFACE
-
V
INTRODUCTION
-
1
CHAPTER
1
ANALYTICAL
CHEMISTRY
----
3
CHAPTER
2
LABORATORY
OPERATIONS
----
7
CHAPTER
3
PLANNING
THE
ANALYSIS
-
31
CHAPTER 4
SAMPLING
----
35
INSTRUMENTAL
ANALYSIS
CHAPTER
5
CALORIMETRY
-
51
CHAPTER 6
CHROMATOGRAPHY
----
55
6.1
COLUMN
CHROMATOGRAPHY
----
57
6.2
GAS-LIQUID
CHROMATOGRAPHY
----
57
6.3
HIGH-PERFORMANCE
LIQUID
CHROMATOGRAPHY
----
63
6.4
ION
CHROMATOGRAPHY
----
65
6.5
PAPER
CHROMATOGRAPHY
----
66
6.6
THIN-LAYER
CHROMATOGRAPHY
----
67
CHAPTER
7
CONDUCTOMETRY
-
71
CHAPTER 8
COULOMETRIC
ANALYSIS
-
79
CHAPTER
9
POTENTIOMETRY
----
83
VIII
-
CONTENTS
CHAPTER
10
POLARIMETRY
----
89
CHAPTER
11
TURBIDIMETRY
AND
NEPHELOMETRY
----
95
CHAPTER
12
POLAROGRAPHY
(VOLTAMMETRY)
-
97
CHAPTER
13
REFRACTOMETRY
-
99
CHAPTER
14
SPECTROPHOTOMETRY
----
103
14.1
COLORIMETRY
----
107
14.2
COLOUR
SCALES
----
108
14.3
ULTRAVIOLET
AND
VISIBLE
SPECTROPHOTOMETRY
-----109
14.4
INFRARED
SPECTROPHOTOMETRY
----
114
14.5
FTIR
SPECTROPHOTOMETRY
----
114
14.6
NEAR-INFRARED
SPECTROPHOTOMETRY
----
117
14.7
RAMAN
SPECTROPHOTOMETRY
----
118
14.8
MASS
SPECTROPHOTOMETRY
----
118
14.9
ATOMIC
ABSORPTION
SPECTROPHOTOMETRY
----
119
14.10
INDUCTIVELY
COUPLED
SPECTROPHOTOMETRY
----
125
14.11
REFLECTANCE
SPECTROPHOTOMETRY
----
127
14.12
FLUORESCENCE
SPECTROSCOPY
----
128
14.12.1
PHYSICAL
MEASUREMENTS
-----129
PHYSICAL
MEASUREMENTS
CHAPTER
15
VISCOSITY
----
133
CHAPTER
16
DENSITY
-
139
16.1
HYDROMETERS
----
141
CHAPTER
17
PARTICLE
ANALYSIS
-
147
17.1
GEL
PERMEATION
CHROMATOGRAPHY
-
147
17.2
TEST
SIEVE
ANALYSIS
----
148
CONTENTS
-
IX
17.3
PARTICLE
COUNTERS
----
151
17.4
IMAGING
----
151
CHAPTER
18
SURFACE
TENSION
-
153
18.1
CHEMICAL
ANALYSIS
----
154
CHAPTER
19
CHEMICAL
ANALYSIS
-
157
19.1
ELECTROCHEMICAL
SERIES
----
157
19.2
NOMENCLATURE
OF
ACIDS
-
158
19.3
VALENCIES
----
158
19.4
CHEMICAL
REAGENTS
-----160
19.4.1
PREPARATION
OF
SOME
COMMON
LABORATORY
SOLUTIONS
OR
REAGENTS
-----163
19.4.2
DILUTION
FORMULA
----
164
19.4.3
PREPARATION
OF
AAS
STANDARD
AQUEOUS
SOLUTIONS
----
164
CHAPTER
20
GRAVIMETRIC
ANALYSIS
-
167
20.1
CO-PRECIPITATION
----
168
20.2
POST-PRECIPITATION
---169
CHAPTER
21
VOLUMETRIC
ANALYSIS
(TITRIMETRIC)
-
171
21.1
TITRATIONS
----
172
21.2
INDICATORS
-
175
21.3
COULOMETRIC
TITRATIONS
-----
176
21.4
ARGENTOMETRIC
TITRATIONS
-
177
21.5
NEUTRALISATION
TITRATIONS
(ACIDS
AND
BASES)
-
178
21.6
NEUTRALISATION
TITRATIONS
(ACIDS
AND
BASES)
-
180
21.7
REDOX
(REDUCTION-OXIDATION)
TITRATIONS
-
181
21.8
PRECIPITATION
TITRATIONS
-
182
21.9
COMPLEXOMETRIC
TITRATIONS
-
183
CHAPTER
22
REACTIONS
WITH
IODINE
-
185
22.1
LODIMETRY
-----
185
22.2
IODOMETRY
----
185
X
-
CONTENTS
CHAPTER
23
QUALITATIVE
CHEMICAL
ANALYSIS
-
187
DATA
CHAPTER
24
DATA
INTERPRETATION
-
197
24.1
THE
T-TEST:
(AKA
STUDENT
'
S
T-TEST)
----
199
24.2
THE
Q-TEST
(OR
GRUBBS
'
TEST)
----
199
24.3
THE
F-TEST
----
200
24.4
GANTT
CHARTS
----
200
24.5
CONTROL
CHARTS
----
200
24.6
REGRESSION
ANALYSIS
----
201
24.7
CALIBRATION
OF
INSTRUMENTATION
-----
202
24.8
VALIDATION
OF
ANALYTICAL
TEST
METHODS
----
203
24.9
MEASUREMENT
OF
ERRORS
----
207
CHAPTER
25
LABORATORY
REPORTS
-
215
25.1
WHAT
ARE
SIGNIFICANT
FIGURES?
----
215
25.2
THE
REPORT
----
217
APPENDICES
APPENDIX
I
LABORATORY
SAFETY
AND
CHECKLISTS
-
223
APPENDIX
II
INTERNATIONALLY
ACCEPTED
LABORATORY
PROCEDURES
AND
TEST
METHODS
-
233
APPENDIX
III
STRENGTHS
OF
COMMON
CONCENTRATED
ACIDS
-
235
APPENDIX
IV
UNITS
OF
MEASUREMENT
AND
CONCENTRATION
-
237
APPENDIX
V
INTERNATIONAL
SYSTEM
(SI)
OF
UNITS
-
241
APPENDIX
VI
METRIC
(SI)
PREFIXES
AND
DECIMAL
UNIT
MULTIPLES
-
243
CONTENTS
-
-
XI
APPENDIX
VII
TEMPERATURE
SCALES
AND
CONVERSIONS
-
245
APPENDIX
VIII
VACUUM
UNITS
-
247
APPENDIX
IX
PRESSURE
UNITS
-
249
APPENDIX
X
AUTOCLAVE
STEAM
PRESSURE
AND
TEMPERATURE
-
251
APPENDIX
XI
DRYING
AGENTS
-
DESICCANTS
-
253
APPENDIX
XII
CONSTANT
HUMIDITY
SOLUTIONS
-
255
APPENDIX
XIII
FREEZING
MIXTURES
-
257
APPENDIX
XIV
RATE
OF
FLOW
UNITS
----
259
APPENDIX
XV
DETECTION
LIMITS
IN
ATOMIC
SPECTROSCOPY
-
261
APPENDIX
XVI
OXIDATION
STATES
-
265
APPENDIX
XVII
COMMODITY
PROPERTIES
----
267
APPENDIX
XVIII
PROPERTIES
OF
METALS
AND
ALLOYS
-
269
APPENDIX
XIX
CARE
OF
PLATINUM
APPARATUS
-
271
APPENDIX
XX
PERIODIC
TABLE
-
273
XII
-
CONTENTS
GLOSSARY
OF
TERMS
----
275
QUIZ
----
287
QUESTIONS
----
287
ANSWERS
----
289
INDEX
----
295 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Soffiantini, Vic |
| author_GND | (DE-588)1250015405 |
| author_facet | Soffiantini, Vic |
| author_role | aut |
| author_sort | Soffiantini, Vic |
| author_variant | v s vs |
| building | Verbundindex |
| bvnumber | BV047650358 |
| classification_rvk | VG 5010 |
| ctrlnum | (OCoLC)1294507256 (DE-599)DNB1235281701 |
| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV047650358 |
| illustrated | Illustrated |
| index_date | 2024-07-03T18:49:51Z |
| indexdate | 2024-07-10T09:18:18Z |
| institution | BVB |
| institution_GND | (DE-588)10095502-2 |
| isbn | 9783110721195 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-033034429 |
| oclc_num | 1294507256 |
| open_access_boolean | |
| owner | DE-11 DE-20 DE-1102 DE-19 DE-BY-UBM |
| owner_facet | DE-11 DE-20 DE-1102 DE-19 DE-BY-UBM |
| physical | XII, 302 Seiten Illustrationen, Diagramme |
| publishDate | 2022 |
| publishDateSearch | 2022 |
| publishDateSort | 2022 |
| publisher | De Gruyter |
| record_format | marc |
| series2 | De Gruyter graduate |
| spelling | Soffiantini, Vic Verfasser (DE-588)1250015405 aut Analytical chemistry principles and practice Vic Soffiantini Berlin ; Boston De Gruyter [2022] © 2022 XII, 302 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier De Gruyter graduate Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Chemische Analyse Instrumentelle Analyse Analytik Analytische Chemie (DE-588)4129906-1 s DE-604 Walter de Gruyter GmbH & Co. KG (DE-588)10095502-2 pbl Erscheint auch als Online-Ausgabe, EPUB 978-3-11-072121-8 Erscheint auch als Online-Ausgabe, PDF 978-3-11-072120-1 X:MVB https://www.degruyter.com/isbn/9783110721195 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033034429&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Soffiantini, Vic Analytical chemistry principles and practice Analytische Chemie (DE-588)4129906-1 gnd |
| subject_GND | (DE-588)4129906-1 |
| title | Analytical chemistry principles and practice |
| title_auth | Analytical chemistry principles and practice |
| title_exact_search | Analytical chemistry principles and practice |
| title_exact_search_txtP | Analytical chemistry principles and practice |
| title_full | Analytical chemistry principles and practice Vic Soffiantini |
| title_fullStr | Analytical chemistry principles and practice Vic Soffiantini |
| title_full_unstemmed | Analytical chemistry principles and practice Vic Soffiantini |
| title_short | Analytical chemistry |
| title_sort | analytical chemistry principles and practice |
| title_sub | principles and practice |
| topic | Analytische Chemie (DE-588)4129906-1 gnd |
| topic_facet | Analytische Chemie |
| url | https://www.degruyter.com/isbn/9783110721195 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033034429&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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