In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids: = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Erlangen
FAU University Press
2021
|
| Schlagworte: | |
| Online-Zugang: | Volltext Volltext Volltext Volltext Inhaltsverzeichnis |
| Beschreibung: | xv, 209 Seiten Illustrationen, Diagramme 24 cm x 17 cm, 564 g |
| ISBN: | 9783961474493 9783961474509 |
| DOI: | 10.25593/978-3-96147-450-9 |
Internformat
MARC
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| 020 | |a 9783961474509 |c OnlineAusgabe |9 978-3-96147-450-9 | ||
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| 100 | 1 | |a Paula, Carolin |0 (DE-588)1245314947 |4 aut | |
| 245 | 1 | 0 | |a In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids |b = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen |c Carolin Paula |
| 246 | 1 | 1 | |a In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen |
| 264 | 1 | |a Erlangen |b FAU University Press |c 2021 | |
| 300 | |a xv, 209 Seiten |b Illustrationen, Diagramme |c 24 cm x 17 cm, 564 g | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c Friedrich-Alexander-Universität Erlangen-Nürnberg |d 2020 | ||
| 650 | 0 | 7 | |a Phasenumwandlung |0 (DE-588)4132140-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a NMR-Spektroskopie |0 (DE-588)4075421-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Kristalliner Stoff |0 (DE-588)4165762-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Röntgendiffraktometrie |0 (DE-588)4336833-5 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Poröser Stoff |0 (DE-588)4046811-2 |2 gnd |9 rswk-swf |
| 653 | |a MIL-53 | ||
| 653 | |a In-Situ MAS NMR spectroscopy | ||
| 653 | |a crystalline porous solids | ||
| 653 | |a solid-solid transformation | ||
| 653 | |a VPI-5 | ||
| 653 | |a breathing behaviour | ||
| 653 | |a In-situ X-ray diffractometry | ||
| 653 | |a breathing behavior | ||
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Kristalliner Stoff |0 (DE-588)4165762-7 |D s |
| 689 | 0 | 1 | |a Poröser Stoff |0 (DE-588)4046811-2 |D s |
| 689 | 0 | 2 | |a NMR-Spektroskopie |0 (DE-588)4075421-2 |D s |
| 689 | 0 | 3 | |a Röntgendiffraktometrie |0 (DE-588)4336833-5 |D s |
| 689 | 0 | 4 | |a Phasenumwandlung |0 (DE-588)4132140-6 |D s |
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| 710 | 2 | |a FAU University Press ein Imprint der Universität Erlangen-Nürnberg |b Universitätsbibliothek |0 (DE-588)1068111240 |4 pbl | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe |t In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids |d Erlangen : FAU University Press, 2021 |h Online-Ressource |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe |o 10.25593/978-3-96147-450-9 |o urn:nbn:de:bvb:29-opus4-174146 |
| 856 | 4 | 1 | |u https://open.fau.de/handle/openfau/17414 |x Verlag |z kostenfrei |3 Volltext |
| 856 | 4 | 1 | |u https://doi.org/10.25593/978-3-96147-450-9 |x Resolving-System |z kostenfrei |3 Volltext |
| 856 | 4 | 1 | |u https://nbn-resolving.org/urn:nbn:de:bvb:29-opus4-174146 |x Resolving-System |z kostenfrei |3 Volltext |
| 856 | 4 | 1 | |u https://d-nb.info/124448931X/34 |x Langzeitarchivierung Nationalbibliothek |z kostenfrei |3 Volltext |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032962149&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
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Datensatz im Suchindex
| _version_ | 1804182926653390848 |
|---|---|
| adam_text | TABLE
OF
CONTENTS
ABSTRACT
...............................................................................................................V
LIST
OF
ABBREVIATIONS
AND
SYMBOLS
.................................................................
XI
1
MOTIVATION
...................................................................................................
I
2
THEORETICAL
BACKGROUND
............................................................................
5
2.1
IN
SITU
MEASUREMENT
TECHNIQUES
IN
HETEROGENEOUS
CATALYSIS
...........
5
2.2
PRINCIPLE
OF
X-RAY
DIFFRACTOMETRY
........................................................
9
2.3
PRINCIPLE
OF
NMR
SPECTROSCOPY
.........................................................
12
2.3.1
TYPES
OF
INTERACTION
........................................................................
17
2.3.1.1
ZEEMAN
INTERACTION
..............................................................
19
2.3.1.2
RADIOFREQUENCY
FIELD
...........................................................
20
2.3.1.3
CHEMICAL
SHIFT
......................................................................
20
2.3.1.4
DIRECT
DIPOLAR
COUPLING
......................................................
24
2.3.1.5
INDIRECT
DIPOLAR
COUPLING
...................................................
25
2.3.1.6
ELECTRIC
QUADRUPOLAR
COUPLING
...........................................
26
2.4
BASICS
OF
SOLID-STATE
NMR
SPECTROSCOPY
...........................................
30
2.4.1
MAGIC-ANGLE
SPINNING
....................................................................
31
2.4.2
DIPOLAR
DECOUPLING
........................................................................
32
2.5
PULSE
SEQUENCES
IN
HIGH-RESOLUTION
SOLID-STATE
NMR
......................
33
2.5.1
SINGLE
PULSE
SEQUENCE
....................................................................
34
2.5.2
CROSS
POLARIZATION
..........................................................................
34
2.5.3
TOTAL
SUPPRESSION
OF
SPINNING
SIDEBANDS
....................................
36
2.6
STATE
OF
THE
ART
OF
IN
SITU
SOLID-STATE
NMR
SPECTROSCOPY
UNDER
CONTINUOUS
FLOW
CONDITIONS
................................................................
38
2.7
MATERIALS
STUDIED
IN
THIS
WORK
..........................................................
42
2.7.1
THE
ALUMINOPHOSPHATES
VPI-5
AND
AIPO4-8
..............................
42
2.7.2
METAL-ORGANIC
FRAMEWORKS
...........................................................
45
2.7.2.1
MIL-53
....................................................................................
51
2.7.2.2
MIL-53-ADP
.........................................................................
54
2.7.2.3
MIL-53-FA
.............................................................................
54
3
SCOPE
OF
THE
WORK
...................................................................................
57
4
EXPERIMENTAL
SECTION
...............................................................................
61
VII
4-I
SYNTHESIS
OF
THE
STUDIED
MATERIALS
....................................................
61
4.1.1
VPI-5
................................................................................................
61
4.1.2
MIL-53
..............................................................................................
61
4.1.3
MIL-53-ADP.....................................................................................
61
4.1.4
MIL-53-FA
.......................................................................................
62
4.2
PHYSICOCHEMICAL
CHARACTERIZATION
...................................................
62
4.3
EX
SITU
SOLID-STATE
NMR
ADSORPTION
STUDIES
.....................................
65
4.4
IN
SITU
PXRD
STUDIES
OF
STRUCTURAL
TRANSFORMATIONS
........................
66
4.4.1
TRANSFORMATION
OF
VPI-5
TO
AIPO4-8
...........................................66
4.4.2
WATER
AD
AND
DESORPTION
ON
MIL-53-TYPE
MOFS
......................
67
4.4.3
AD
AND
DESORPTION
OF
CO
2
ON
MIL-53-ADP
AND
MIL-53-FA....69
4.5
IN
SITU
SOLID-STATE
NMR
SPECTROSCOPY
UNDER
CONTINUOUS
FLOW
CONDITIONS
............................................................................................
70
4.5.1
PROBE
ELECTRONICS
.............................................................................
71
4.5.2
ROTOR
DESIGN
AND
FLOW
PROFILE
.......................................................
72
4.5.3
LASER
SPECIFICATIONS
FOR
HEATING
...................................................
74
4.5.4
MEASUREMENT
SET-UP
......................................................................
76
4.5.5
TRANSFORMATION
OF
VPI-5
TO
AIPO4-8
..........................................
78
4.5.6
WATER
ADSORPTION
ON
MIL-53-TYPE
MOFS
....................................
79
4.6
ANALYSIS
OF
THE
RECRYSTALLIZATION
KINETICS
..........................................80
5
RESULTS
AND
DISCUSSION
............................................................................
83
5.1
CHARACTERIZATION
OF
THE
SYNTHESIZED
MATERIALS
................................
83
5.1.1
VPI-5
...............................................................................................
83
5.1.2
MIL-53
.............................................................................................
86
5.1.3
MIL-53-ADP....................................................................................
90
5.1.4
MIL-53-FA
.......................................................................................
93
5.2
IN
SITU
SOLID-STATE
NMR
SPECTROSCOPY
UNDER
CONTINUOUS
FLOW
CONDITIONS
...........................................................................................
97
5.2.1
CALIBRATION
OF
THE
FLOW
PROBE
......................................................
97
5.2.2
TEMPERATURE
CALIBRATION
OF
THE
SAMPLE
IN
THE
ROTOR
.................
99
5.3
STRUCTURAL
TRANSFORMATION
OF
VPI-5
TO
AIPO4-8
..............................
103
5.3.1
IN
SITU
NMR
STUDY
OF
THE
STRUCTURAL
TRANSFORMATION
...............
103
5.3.2
IN
SITU
XRD
STUDY
OF
THE
STRUCTURAL
TRANSFORMATION
................
108
VIII
5.4
BREATHING
BEHAVIOR
OF
ISORETICULAR
MOFS
WITH
MIL-53-TYPE
TOPOLOGY
114
5.4.1
EX
SITU
SOLID-STATE
NMR
SPECTROSCOPY
OF
CO
2
ADSORBED
ON
SAMPLES
WITH
MIL-53-TYPE
TOPOLOGY
115
5.4.2
IN
SITU
INVESTIGATIONS
OF
THE
MIL-53
BREATHING
BEHAVIOR
118
5.4.2.1
IN
SITU
SOLID-STATE
NMR
OF
THE
MIL-53
HYDRATION
119
5.4.2.2
IN
SITU
XRD
STUDY
OF
THE
MIL-53
HYDRATION
120
5.4.3
STRUCTURAL
TRANSFORMATION
OF
MIL-53-ADP
ON
SORPTION
OF
WATER
AND
C0
2
128
5.4.3.1
IN
SITU
SOLID-STATE
NMR
OF
THE
DE
AND
REHYDRATION
OF
MIL-53-ADP
128
5.43.2
IN
SITU
XRD
STUDY
OF
THE
SORPTION
OF
WATER
ON
MIL-53
ADP
132
5.4.33
IN
SITU
XRD
STUDY
OF
THE
SORPTION
OF
CO
2
ON
MIL-53-ADP
142
5.4.4
BEHAVIOR
OF
MIL-53-FA
UPON
ADSORPTION
OF
WATER
AND
CO
2
....148
5.4.4.1
IN
SITU
SOLID-STATE
NMR
SPECTROSCOPY
OF
THE
BREATHING
BEHAVIOR
OF
MIL-53-FA
148
5.4.4.2
IN
SITU
XRD
STUDY
OF
THE
SORPTION
OF
WATER
IN
MIL-53-FA
152
5.4.43
IN
SITU
XRD
STUDY
OF
THE
ADSORPTION
OF
CO
2
IN
MIL-53-FA
157
5.4.5
COMPARISON
OF
THE
BREATHING
BEHAVIOR
OF
THE
THREE
ISORETICULAR
MOFS
.............................................................................................
160
5.5
VALUATION
OF
THE
IN
SITU
NMR
PROBE
163
6
SUMMARY
167
7
PERSPECTIVES
173
8
ZUSAMMENFASSUNG
175
LIST
OF
REFERENCES
183
APPENDIX
201
|
| adam_txt |
TABLE
OF
CONTENTS
ABSTRACT
.V
LIST
OF
ABBREVIATIONS
AND
SYMBOLS
.
XI
1
MOTIVATION
.
I
2
THEORETICAL
BACKGROUND
.
5
2.1
IN
SITU
MEASUREMENT
TECHNIQUES
IN
HETEROGENEOUS
CATALYSIS
.
5
2.2
PRINCIPLE
OF
X-RAY
DIFFRACTOMETRY
.
9
2.3
PRINCIPLE
OF
NMR
SPECTROSCOPY
.
12
2.3.1
TYPES
OF
INTERACTION
.
17
2.3.1.1
ZEEMAN
INTERACTION
.
19
2.3.1.2
RADIOFREQUENCY
FIELD
.
20
2.3.1.3
CHEMICAL
SHIFT
.
20
2.3.1.4
DIRECT
DIPOLAR
COUPLING
.
24
2.3.1.5
INDIRECT
DIPOLAR
COUPLING
.
25
2.3.1.6
ELECTRIC
QUADRUPOLAR
COUPLING
.
26
2.4
BASICS
OF
SOLID-STATE
NMR
SPECTROSCOPY
.
30
2.4.1
MAGIC-ANGLE
SPINNING
.
31
2.4.2
DIPOLAR
DECOUPLING
.
32
2.5
PULSE
SEQUENCES
IN
HIGH-RESOLUTION
SOLID-STATE
NMR
.
33
2.5.1
SINGLE
PULSE
SEQUENCE
.
34
2.5.2
CROSS
POLARIZATION
.
34
2.5.3
TOTAL
SUPPRESSION
OF
SPINNING
SIDEBANDS
.
36
2.6
STATE
OF
THE
ART
OF
IN
SITU
SOLID-STATE
NMR
SPECTROSCOPY
UNDER
CONTINUOUS
FLOW
CONDITIONS
.
38
2.7
MATERIALS
STUDIED
IN
THIS
WORK
.
42
2.7.1
THE
ALUMINOPHOSPHATES
VPI-5
AND
AIPO4-8
.
42
2.7.2
METAL-ORGANIC
FRAMEWORKS
.
45
2.7.2.1
MIL-53
.
51
2.7.2.2
MIL-53-ADP
.
54
2.7.2.3
MIL-53-FA
.
54
3
SCOPE
OF
THE
WORK
.
57
4
EXPERIMENTAL
SECTION
.
61
VII
4-I
SYNTHESIS
OF
THE
STUDIED
MATERIALS
.
61
4.1.1
VPI-5
.
61
4.1.2
MIL-53
.
61
4.1.3
MIL-53-ADP.
61
4.1.4
MIL-53-FA
.
62
4.2
PHYSICOCHEMICAL
CHARACTERIZATION
.
62
4.3
EX
SITU
SOLID-STATE
NMR
ADSORPTION
STUDIES
.
65
4.4
IN
SITU
PXRD
STUDIES
OF
STRUCTURAL
TRANSFORMATIONS
.
66
4.4.1
TRANSFORMATION
OF
VPI-5
TO
AIPO4-8
.66
4.4.2
WATER
AD
AND
DESORPTION
ON
MIL-53-TYPE
MOFS
.
67
4.4.3
AD
AND
DESORPTION
OF
CO
2
ON
MIL-53-ADP
AND
MIL-53-FA.69
4.5
IN
SITU
SOLID-STATE
NMR
SPECTROSCOPY
UNDER
CONTINUOUS
FLOW
CONDITIONS
.
70
4.5.1
PROBE
ELECTRONICS
.
71
4.5.2
ROTOR
DESIGN
AND
FLOW
PROFILE
.
72
4.5.3
LASER
SPECIFICATIONS
FOR
HEATING
.
74
4.5.4
MEASUREMENT
SET-UP
.
76
4.5.5
TRANSFORMATION
OF
VPI-5
TO
AIPO4-8
.
78
4.5.6
WATER
ADSORPTION
ON
MIL-53-TYPE
MOFS
.
79
4.6
ANALYSIS
OF
THE
RECRYSTALLIZATION
KINETICS
.80
5
RESULTS
AND
DISCUSSION
.
83
5.1
CHARACTERIZATION
OF
THE
SYNTHESIZED
MATERIALS
.
83
5.1.1
VPI-5
.
83
5.1.2
MIL-53
.
86
5.1.3
MIL-53-ADP.
90
5.1.4
MIL-53-FA
.
93
5.2
IN
SITU
SOLID-STATE
NMR
SPECTROSCOPY
UNDER
CONTINUOUS
FLOW
CONDITIONS
.
97
5.2.1
CALIBRATION
OF
THE
FLOW
PROBE
.
97
5.2.2
TEMPERATURE
CALIBRATION
OF
THE
SAMPLE
IN
THE
ROTOR
.
99
5.3
STRUCTURAL
TRANSFORMATION
OF
VPI-5
TO
AIPO4-8
.
103
5.3.1
IN
SITU
NMR
STUDY
OF
THE
STRUCTURAL
TRANSFORMATION
.
103
5.3.2
IN
SITU
XRD
STUDY
OF
THE
STRUCTURAL
TRANSFORMATION
.
108
VIII
5.4
BREATHING
BEHAVIOR
OF
ISORETICULAR
MOFS
WITH
MIL-53-TYPE
TOPOLOGY
114
5.4.1
EX
SITU
SOLID-STATE
NMR
SPECTROSCOPY
OF
CO
2
ADSORBED
ON
SAMPLES
WITH
MIL-53-TYPE
TOPOLOGY
115
5.4.2
IN
SITU
INVESTIGATIONS
OF
THE
MIL-53
BREATHING
BEHAVIOR
118
5.4.2.1
IN
SITU
SOLID-STATE
NMR
OF
THE
MIL-53
HYDRATION
119
5.4.2.2
IN
SITU
XRD
STUDY
OF
THE
MIL-53
HYDRATION
120
5.4.3
STRUCTURAL
TRANSFORMATION
OF
MIL-53-ADP
ON
SORPTION
OF
WATER
AND
C0
2
128
5.4.3.1
IN
SITU
SOLID-STATE
NMR
OF
THE
DE
AND
REHYDRATION
OF
MIL-53-ADP
128
5.43.2
IN
SITU
XRD
STUDY
OF
THE
SORPTION
OF
WATER
ON
MIL-53
ADP
132
5.4.33
IN
SITU
XRD
STUDY
OF
THE
SORPTION
OF
CO
2
ON
MIL-53-ADP
142
5.4.4
BEHAVIOR
OF
MIL-53-FA
UPON
ADSORPTION
OF
WATER
AND
CO
2
.148
5.4.4.1
IN
SITU
SOLID-STATE
NMR
SPECTROSCOPY
OF
THE
BREATHING
BEHAVIOR
OF
MIL-53-FA
148
5.4.4.2
IN
SITU
XRD
STUDY
OF
THE
SORPTION
OF
WATER
IN
MIL-53-FA
152
5.4.43
IN
SITU
XRD
STUDY
OF
THE
ADSORPTION
OF
CO
2
IN
MIL-53-FA
157
5.4.5
COMPARISON
OF
THE
BREATHING
BEHAVIOR
OF
THE
THREE
ISORETICULAR
MOFS
.
160
5.5
VALUATION
OF
THE
IN
SITU
NMR
PROBE
163
6
SUMMARY
167
7
PERSPECTIVES
173
8
ZUSAMMENFASSUNG
175
LIST
OF
REFERENCES
183
APPENDIX
201 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Paula, Carolin |
| author_GND | (DE-588)1245314947 |
| author_facet | Paula, Carolin |
| author_role | aut |
| author_sort | Paula, Carolin |
| author_variant | c p cp |
| building | Verbundindex |
| bvnumber | BV047576670 |
| classification_tum | MTA 510 |
| collection | ebook |
| ctrlnum | (OCoLC)1282186184 (DE-599)DNB1244530743 |
| discipline | Physik |
| discipline_str_mv | Physik |
| doi_str_mv | 10.25593/978-3-96147-450-9 |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV047576670 |
| illustrated | Illustrated |
| index_date | 2024-07-03T18:32:12Z |
| indexdate | 2024-07-10T09:15:19Z |
| institution | BVB |
| institution_GND | (DE-588)1068111240 |
| isbn | 9783961474493 9783961474509 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032962149 |
| oclc_num | 1282186184 |
| open_access_boolean | 1 |
| owner | DE-29 DE-12 DE-91 DE-BY-TUM DE-29T |
| owner_facet | DE-29 DE-12 DE-91 DE-BY-TUM DE-29T |
| physical | xv, 209 Seiten Illustrationen, Diagramme 24 cm x 17 cm, 564 g |
| psigel | ebook |
| publishDate | 2021 |
| publishDateSearch | 2021 |
| publishDateSort | 2021 |
| publisher | FAU University Press |
| record_format | marc |
| spelling | Paula, Carolin (DE-588)1245314947 aut In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen Carolin Paula In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen Erlangen FAU University Press 2021 xv, 209 Seiten Illustrationen, Diagramme 24 cm x 17 cm, 564 g txt rdacontent n rdamedia nc rdacarrier Dissertation Friedrich-Alexander-Universität Erlangen-Nürnberg 2020 Phasenumwandlung (DE-588)4132140-6 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Kristalliner Stoff (DE-588)4165762-7 gnd rswk-swf Röntgendiffraktometrie (DE-588)4336833-5 gnd rswk-swf Poröser Stoff (DE-588)4046811-2 gnd rswk-swf MIL-53 In-Situ MAS NMR spectroscopy crystalline porous solids solid-solid transformation VPI-5 breathing behaviour In-situ X-ray diffractometry breathing behavior (DE-588)4113937-9 Hochschulschrift gnd-content Kristalliner Stoff (DE-588)4165762-7 s Poröser Stoff (DE-588)4046811-2 s NMR-Spektroskopie (DE-588)4075421-2 s Röntgendiffraktometrie (DE-588)4336833-5 s Phasenumwandlung (DE-588)4132140-6 s DE-604 FAU University Press ein Imprint der Universität Erlangen-Nürnberg Universitätsbibliothek (DE-588)1068111240 pbl Erscheint auch als Online-Ausgabe In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids Erlangen : FAU University Press, 2021 Online-Ressource Erscheint auch als Online-Ausgabe 10.25593/978-3-96147-450-9 urn:nbn:de:bvb:29-opus4-174146 https://open.fau.de/handle/openfau/17414 Verlag kostenfrei Volltext https://doi.org/10.25593/978-3-96147-450-9 Resolving-System kostenfrei Volltext https://nbn-resolving.org/urn:nbn:de:bvb:29-opus4-174146 Resolving-System kostenfrei Volltext https://d-nb.info/124448931X/34 Langzeitarchivierung Nationalbibliothek kostenfrei Volltext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032962149&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p vlb 20211026 DE-101 https://d-nb.info/provenance/plan#vlb |
| spellingShingle | Paula, Carolin In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen Phasenumwandlung (DE-588)4132140-6 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Kristalliner Stoff (DE-588)4165762-7 gnd Röntgendiffraktometrie (DE-588)4336833-5 gnd Poröser Stoff (DE-588)4046811-2 gnd |
| subject_GND | (DE-588)4132140-6 (DE-588)4075421-2 (DE-588)4165762-7 (DE-588)4336833-5 (DE-588)4046811-2 (DE-588)4113937-9 |
| title | In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen |
| title_alt | In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen |
| title_auth | In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen |
| title_exact_search | In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen |
| title_exact_search_txtP | In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen |
| title_full | In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen Carolin Paula |
| title_fullStr | In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen Carolin Paula |
| title_full_unstemmed | In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen Carolin Paula |
| title_short | In situ solid-state NMR and XRD investigations of structural transformations in crystalline porous solids |
| title_sort | in situ solid state nmr and xrd investigations of structural transformations in crystalline porous solids in situ feststoff nmr und xrd untersuchungen von strukturumwandlungen in kristallinen porosen feststoffen |
| title_sub | = In-situ Feststoff-NMR- und XRD-Untersuchungen von Strukturumwandlungen in kristallinen porösen Feststoffen |
| topic | Phasenumwandlung (DE-588)4132140-6 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Kristalliner Stoff (DE-588)4165762-7 gnd Röntgendiffraktometrie (DE-588)4336833-5 gnd Poröser Stoff (DE-588)4046811-2 gnd |
| topic_facet | Phasenumwandlung NMR-Spektroskopie Kristalliner Stoff Röntgendiffraktometrie Poröser Stoff Hochschulschrift |
| url | https://open.fau.de/handle/openfau/17414 https://doi.org/10.25593/978-3-96147-450-9 https://nbn-resolving.org/urn:nbn:de:bvb:29-opus4-174146 https://d-nb.info/124448931X/34 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032962149&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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