Experimental and numerical study of aromatic species formation in counterflow diffusion flames:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Düren
Shaker
2021
|
| Schriftenreihe: | Berichte aus der Energietechnik
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | xvii, 178 Seiten Illustrationen, Diagramme 21 cm x 14.8 cm, 293 g |
| ISBN: | 9783844081404 3844081402 |
Internformat
MARC
| LEADER | 00000nam a22000008c 4500 | ||
|---|---|---|---|
| 001 | BV047564700 | ||
| 003 | DE-604 | ||
| 005 | 20220209 | ||
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| 020 | |a 9783844081404 |c : EUR 48.80 (DE), EUR 48.80 (AT), CHF 61.10 (freier Preis) |9 978-3-8440-8140-4 | ||
| 020 | |a 3844081402 |9 3-8440-8140-2 | ||
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| 100 | 1 | |a Baroncelli, Martina |e Verfasser |0 (DE-588)1242603913 |4 aut | |
| 245 | 1 | 0 | |a Experimental and numerical study of aromatic species formation in counterflow diffusion flames |c Martina Baroncelli |
| 264 | 1 | |a Düren |b Shaker |c 2021 | |
| 300 | |a xvii, 178 Seiten |b Illustrationen, Diagramme |c 21 cm x 14.8 cm, 293 g | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Berichte aus der Energietechnik | |
| 502 | |b Dissertation |c RWTH Aachen University |d 2021 | ||
| 650 | 0 | 7 | |a Verbrennung |0 (DE-588)4062656-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Gegenstromprinzip |0 (DE-588)4329194-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Diffusionsflamme |0 (DE-588)4149814-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Verbrennungsprodukt |0 (DE-588)4187589-8 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Polycyclische Aromaten |0 (DE-588)4175141-3 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Oxyfuel-Verfahren |0 (DE-588)7628163-2 |2 gnd |9 rswk-swf |
| 653 | |a combustion | ||
| 653 | |a chemical models | ||
| 653 | |a aromatics | ||
| 653 | |a pyrolysis | ||
| 653 | |a soot | ||
| 653 | |a pollution | ||
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
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| 689 | 0 | 2 | |a Gegenstromprinzip |0 (DE-588)4329194-6 |D s |
| 689 | 0 | 3 | |a Diffusionsflamme |0 (DE-588)4149814-8 |D s |
| 689 | 0 | 4 | |a Polycyclische Aromaten |0 (DE-588)4175141-3 |D s |
| 689 | 0 | 5 | |a Verbrennungsprodukt |0 (DE-588)4187589-8 |D s |
| 689 | 0 | |5 DE-604 | |
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| 999 | |a oai:aleph.bib-bvb.de:BVB01-032940077 | ||
| 883 | 1 | |8 1\p |a vlb |d 20210706 |q DE-101 |u https://d-nb.info/provenance/plan#vlb | |
Datensatz im Suchindex
| _version_ | 1804182893484834816 |
|---|---|
| adam_text | CONTENTS
PUBLICATION
LIST
IX
1.
INTRODUCTION
1
2.
EXPERIMENTAL
SETUP
5
2.1.
EXPERIMENTS
IN
THE
COUNTERFLOW
REACTOR
...................................
6
2.1.1.
THEORETICAL
BACKGROUND
OF
LAMINAR
COUNTERFLOW
FLAMES
6
2.1.2.
TECHNICAL
DETAILS
..........................................................
12
2.1.3.
BURNER
CONTROL
AND
EXPERIMENTAL
PROCEDURES
................
13
2.1.4.
UNCERTAINTY
QUANTIFICATION
...........................................
15
2.1.5.
VERIFICATION
...................................................................
18
2.2.
MASS
SPECTROMETRY
...................................................................
21
2.2.1.
SAMPLING
......................................................................
21
2.2.2.
ELECTRON
IMPACT
IONIZATION
............................................
24
2.2.3.
SEPARATION
AND
DETECTION
...........................................
27
2.2.4.
DETECTION
EFFICIENCY
AND
OPTIMIZATION
..........................
28
2.2.5.
SATURATION
AND
DOUBLE
EVENTS
......................................
31
2.2.6.
DATA
QUANTIFICATION
.......................................................
32
2.3.
TEMPERATURE
MEASUREMENTS
....................................................
41
2.4.
NUMERICAL
SIMULATIONS
.............................................................
44
3.
INVESTIGATING
THE
EFFECT
OF
OXY-FUEL
COMBUSTION
AND
LIGHT
COAL
VOLATILES
INTERACTION:
A
MASS
SPECTROMETRIC
STUDY
49
3.1.
NUMERICAL
AND
EXPERIMENTAL
PROCEDURES
................................
50
3.2.
RESULTS
AND
ANALYSIS
................................................................
51
3.2.1.
MAIN
SPECIES
................................................................
51
3.2.2.
SMALL
INTERMEDIATES
....................................................
54
3.2.3.
SOOT
PRECURSORS
.............................................................
60
3.3.
CHAPTER
SUMMARY
...................................................................
66
4.
ROLE
OF
RING-ENLARGEMENT
REACTIONS
IN
THE
FORMATION
OF
ARO
MATIC
HYDROCARBONS
69
4.1.
EXPERIMENTAL
SETUP
AND
DATA
REDUCTION
...............................
71
CONTENTS
4.2.
THEORETICAL
CALCULATIONS
AND
KINETIC
MODELING
.......................
73
4.2.1.
HYDROGEN
ABSTRACTION
REACTIONS
FROM
C-,H(,
...............
73
4.2.2.
MODELING
OF
THE
RING-ENLARGEMENT
REACTIONS
...............
74
4.2.3.
FIRST
INSPECTION
OF
THE
MASS
SPECTRUM
.......................
76
4.3.
INITIAL
FUEL
DECOMPOSITION
STEPS
...............................................
78
4.3.1.
SMALL
HYDROCARBONS
.....................................................
79
4.3.2.
CONSEQUENCES
UPON
METHANE
ADDITION
.......................
82
4.4.
RING-ENLARGEMENT
REACTIONS
.....................................................
89
4.4.1.
FIRST
RING-ENLARGEMENT
ROUTE:
C5H5+CH3
-
C
B
H6-|-2H
AND
ANALOGOUS
..............................................................
89
4.4.2.
ADDITIONAL
ENLARGEMENT
ROUTES:
C5H5+C2/C3
-
TCY/CG
95
4.5.
CHAPTER
SUMMARY
...................................................................
99
5.
EFFECTS
OF
C!-C
3
HYDROCARBON
BLENDING
ON
AROMATICS
FOR
MATION
IN
1-BUTENE
COUNTERFLOW
FLAMES
101
5.1.
EXPERIMENTAL
APPROACH
..............................................................
103
5.2.
COMPUTATIONAL
MODELING
...........................................................
104
5.3.
EXPERIMENTAL
RESULTS
................................................................
105
5.4.
CI
TO
C5
CHEMISTRY
...................................................................
107
5.4.1.
EARLY
FUEL
DECOMPOSITION
STEPS
OF
1-BUTENE
..................
107
5.4.2.
EFFECT
OF
FUEL-SPECIFIC
CHEMISTRY
ON
C1-C5
INTERMEDIATES
................................................................
112
5.5.
ANALYSIS
ON
AROMATIC
SPECIES
..................................................
114
5.5.1.
CGHF,
AND
C
B
H
IQ
:
THE
ROLE
OF
THE
C3
RADICAL
POOL
.
.
.
115
5.5.2.
BENZENE-DRIVEN
PATHWAYS
............................................
118
5.5.3.
ACETYLENE-DRIVEN
PATHWAYS
.........................................
119
5.5.4.
NAPHTHALENE
.................................................................
122
5.6.
NEW
REACTION
RATES
...................................................................
125
5.7.
BEYOND
NAPHTHALENE
AND
TOWARDS
SOOT
...................................
130
5.8.
CHAPTER
SUMMARY
...................................................................
132
6.
CONCLUDING
REMARKS
135
A.
SUPPORTING
MATERIAL
ABOUT
THE
TEST
FACILITY
AND
MEASURE
MENT
PROCEDURE
139
A.
L.
DERIVATION
OF
THE
R-MOMENTUM
EQUATION
FOR
THE
COUNTERFLOW
FLAME
..................................................
139
A.
2.
TECHNICAL
INFORMATION
AND
TEMPERATURE
MEASUREMENTS
....
141
CONTENTS
B.
SUPPORTING
MATERIAL
FOR
THE
STUDY
PRESENTED
IN
CH.
3
142
B.
L.
CALIBRATION
...............................................................................
142
B.
2.
ADDITIONAL
EXPERIMENTAL
RESULTS
..............................................
144
C.
SUPPORTING
MATERIAL
FOR
THE
STUDY
PRESENTED
IN
CH.
4
146
C.
L.
ADDITIONAL
INFORMATION
ABOUT
THE
THEORETICAL
CALCULATIONS
.
.
146
C.
2.
SUMMARY
OF
THE
MODIFIED
REACTIONS
.........................................
147
C.3.
ADDITIONAL
COMPARISONS
..........................................................
149
C.
4.
FURTHER
INTERMEDIATES
.............................................................
152
D.
SUPPORTING
MATERIAL
FOR
THE
STUDY
PRESENTED
IN
CH.
5
156
D.
L.
ADDITIONAL
INFORMATION
ON
CALIBRATION
...................................
156
D.
2.
CALIBRATION
OF
CSHG,
CGHG,
AND
C5H40
...................................
157
D.3.
ADDITIONAL
NUMERICAL
AND
EXPERIMENTAL
DATA
..........................
158
D.4.
ROP
FOR
PROPARGYL
...................................................................
160
BIBLIOGRAPHY
161
|
| adam_txt |
CONTENTS
PUBLICATION
LIST
IX
1.
INTRODUCTION
1
2.
EXPERIMENTAL
SETUP
5
2.1.
EXPERIMENTS
IN
THE
COUNTERFLOW
REACTOR
.
6
2.1.1.
THEORETICAL
BACKGROUND
OF
LAMINAR
COUNTERFLOW
FLAMES
6
2.1.2.
TECHNICAL
DETAILS
.
12
2.1.3.
BURNER
CONTROL
AND
EXPERIMENTAL
PROCEDURES
.
13
2.1.4.
UNCERTAINTY
QUANTIFICATION
.
15
2.1.5.
VERIFICATION
.
18
2.2.
MASS
SPECTROMETRY
.
21
2.2.1.
SAMPLING
.
21
2.2.2.
ELECTRON
IMPACT
IONIZATION
.
24
2.2.3.
SEPARATION
AND
DETECTION
.
27
2.2.4.
DETECTION
EFFICIENCY
AND
OPTIMIZATION
.
28
2.2.5.
SATURATION
AND
DOUBLE
EVENTS
.
31
2.2.6.
DATA
QUANTIFICATION
.
32
2.3.
TEMPERATURE
MEASUREMENTS
.
41
2.4.
NUMERICAL
SIMULATIONS
.
44
3.
INVESTIGATING
THE
EFFECT
OF
OXY-FUEL
COMBUSTION
AND
LIGHT
COAL
VOLATILES
INTERACTION:
A
MASS
SPECTROMETRIC
STUDY
49
3.1.
NUMERICAL
AND
EXPERIMENTAL
PROCEDURES
.
50
3.2.
RESULTS
AND
ANALYSIS
.
51
3.2.1.
MAIN
SPECIES
.
51
3.2.2.
SMALL
INTERMEDIATES
.
54
3.2.3.
SOOT
PRECURSORS
.
60
3.3.
CHAPTER
SUMMARY
.
66
4.
ROLE
OF
RING-ENLARGEMENT
REACTIONS
IN
THE
FORMATION
OF
ARO
MATIC
HYDROCARBONS
69
4.1.
EXPERIMENTAL
SETUP
AND
DATA
REDUCTION
.
71
CONTENTS
4.2.
THEORETICAL
CALCULATIONS
AND
KINETIC
MODELING
.
73
4.2.1.
HYDROGEN
ABSTRACTION
REACTIONS
FROM
C-,H(,
.
73
4.2.2.
MODELING
OF
THE
RING-ENLARGEMENT
REACTIONS
.
74
4.2.3.
FIRST
INSPECTION
OF
THE
MASS
SPECTRUM
.
76
4.3.
INITIAL
FUEL
DECOMPOSITION
STEPS
.
78
4.3.1.
SMALL
HYDROCARBONS
.
79
4.3.2.
CONSEQUENCES
UPON
METHANE
ADDITION
.
82
4.4.
RING-ENLARGEMENT
REACTIONS
.
89
4.4.1.
FIRST
RING-ENLARGEMENT
ROUTE:
C5H5+CH3
-
C
B
H6-|-2H
AND
ANALOGOUS
.
89
4.4.2.
ADDITIONAL
ENLARGEMENT
ROUTES:
C5H5+C2/C3
-
TCY/CG
95
4.5.
CHAPTER
SUMMARY
.
99
5.
EFFECTS
OF
C!-C
3
HYDROCARBON
BLENDING
ON
AROMATICS
FOR
MATION
IN
1-BUTENE
COUNTERFLOW
FLAMES
101
5.1.
EXPERIMENTAL
APPROACH
.
103
5.2.
COMPUTATIONAL
MODELING
.
104
5.3.
EXPERIMENTAL
RESULTS
.
105
5.4.
CI
TO
C5
CHEMISTRY
.
107
5.4.1.
EARLY
FUEL
DECOMPOSITION
STEPS
OF
1-BUTENE
.
107
5.4.2.
EFFECT
OF
FUEL-SPECIFIC
CHEMISTRY
ON
C1-C5
INTERMEDIATES
.
112
5.5.
ANALYSIS
ON
AROMATIC
SPECIES
.
114
5.5.1.
CGHF,
AND
C
B
H
IQ
:
THE
ROLE
OF
THE
C3
RADICAL
POOL
.
.
.
115
5.5.2.
BENZENE-DRIVEN
PATHWAYS
.
118
5.5.3.
ACETYLENE-DRIVEN
PATHWAYS
.
119
5.5.4.
NAPHTHALENE
.
122
5.6.
NEW
REACTION
RATES
.
125
5.7.
BEYOND
NAPHTHALENE
AND
TOWARDS
SOOT
.
130
5.8.
CHAPTER
SUMMARY
.
132
6.
CONCLUDING
REMARKS
135
A.
SUPPORTING
MATERIAL
ABOUT
THE
TEST
FACILITY
AND
MEASURE
MENT
PROCEDURE
139
A.
L.
DERIVATION
OF
THE
R-MOMENTUM
EQUATION
FOR
THE
COUNTERFLOW
FLAME
.
139
A.
2.
TECHNICAL
INFORMATION
AND
TEMPERATURE
MEASUREMENTS
.
141
CONTENTS
B.
SUPPORTING
MATERIAL
FOR
THE
STUDY
PRESENTED
IN
CH.
3
142
B.
L.
CALIBRATION
.
142
B.
2.
ADDITIONAL
EXPERIMENTAL
RESULTS
.
144
C.
SUPPORTING
MATERIAL
FOR
THE
STUDY
PRESENTED
IN
CH.
4
146
C.
L.
ADDITIONAL
INFORMATION
ABOUT
THE
THEORETICAL
CALCULATIONS
.
.
146
C.
2.
SUMMARY
OF
THE
MODIFIED
REACTIONS
.
147
C.3.
ADDITIONAL
COMPARISONS
.
149
C.
4.
FURTHER
INTERMEDIATES
.
152
D.
SUPPORTING
MATERIAL
FOR
THE
STUDY
PRESENTED
IN
CH.
5
156
D.
L.
ADDITIONAL
INFORMATION
ON
CALIBRATION
.
156
D.
2.
CALIBRATION
OF
CSHG,
CGHG,
AND
C5H40
.
157
D.3.
ADDITIONAL
NUMERICAL
AND
EXPERIMENTAL
DATA
.
158
D.4.
ROP
FOR
PROPARGYL
.
160
BIBLIOGRAPHY
161 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Baroncelli, Martina |
| author_GND | (DE-588)1242603913 |
| author_facet | Baroncelli, Martina |
| author_role | aut |
| author_sort | Baroncelli, Martina |
| author_variant | m b mb |
| building | Verbundindex |
| bvnumber | BV047564700 |
| classification_rvk | VN 5477 |
| classification_tum | CIT 590 |
| ctrlnum | (OCoLC)1292600037 (DE-599)DNB1236587448 |
| discipline | Chemie / Pharmazie Chemie-Ingenieurwesen |
| discipline_str_mv | Chemie / Pharmazie Chemie-Ingenieurwesen |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV047564700 |
| illustrated | Illustrated |
| index_date | 2024-07-03T18:28:15Z |
| indexdate | 2024-07-10T09:14:47Z |
| institution | BVB |
| isbn | 9783844081404 3844081402 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032940077 |
| oclc_num | 1292600037 |
| open_access_boolean | |
| owner | DE-83 DE-91G DE-BY-TUM |
| owner_facet | DE-83 DE-91G DE-BY-TUM |
| physical | xvii, 178 Seiten Illustrationen, Diagramme 21 cm x 14.8 cm, 293 g |
| publishDate | 2021 |
| publishDateSearch | 2021 |
| publishDateSort | 2021 |
| publisher | Shaker |
| record_format | marc |
| series2 | Berichte aus der Energietechnik |
| spelling | Baroncelli, Martina Verfasser (DE-588)1242603913 aut Experimental and numerical study of aromatic species formation in counterflow diffusion flames Martina Baroncelli Düren Shaker 2021 xvii, 178 Seiten Illustrationen, Diagramme 21 cm x 14.8 cm, 293 g txt rdacontent n rdamedia nc rdacarrier Berichte aus der Energietechnik Dissertation RWTH Aachen University 2021 Verbrennung (DE-588)4062656-8 gnd rswk-swf Gegenstromprinzip (DE-588)4329194-6 gnd rswk-swf Diffusionsflamme (DE-588)4149814-8 gnd rswk-swf Verbrennungsprodukt (DE-588)4187589-8 gnd rswk-swf Polycyclische Aromaten (DE-588)4175141-3 gnd rswk-swf Oxyfuel-Verfahren (DE-588)7628163-2 gnd rswk-swf combustion chemical models aromatics pyrolysis soot pollution (DE-588)4113937-9 Hochschulschrift gnd-content Verbrennung (DE-588)4062656-8 s Oxyfuel-Verfahren (DE-588)7628163-2 s Gegenstromprinzip (DE-588)4329194-6 s Diffusionsflamme (DE-588)4149814-8 s Polycyclische Aromaten (DE-588)4175141-3 s Verbrennungsprodukt (DE-588)4187589-8 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032940077&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p vlb 20210706 DE-101 https://d-nb.info/provenance/plan#vlb |
| spellingShingle | Baroncelli, Martina Experimental and numerical study of aromatic species formation in counterflow diffusion flames Verbrennung (DE-588)4062656-8 gnd Gegenstromprinzip (DE-588)4329194-6 gnd Diffusionsflamme (DE-588)4149814-8 gnd Verbrennungsprodukt (DE-588)4187589-8 gnd Polycyclische Aromaten (DE-588)4175141-3 gnd Oxyfuel-Verfahren (DE-588)7628163-2 gnd |
| subject_GND | (DE-588)4062656-8 (DE-588)4329194-6 (DE-588)4149814-8 (DE-588)4187589-8 (DE-588)4175141-3 (DE-588)7628163-2 (DE-588)4113937-9 |
| title | Experimental and numerical study of aromatic species formation in counterflow diffusion flames |
| title_auth | Experimental and numerical study of aromatic species formation in counterflow diffusion flames |
| title_exact_search | Experimental and numerical study of aromatic species formation in counterflow diffusion flames |
| title_exact_search_txtP | Experimental and numerical study of aromatic species formation in counterflow diffusion flames |
| title_full | Experimental and numerical study of aromatic species formation in counterflow diffusion flames Martina Baroncelli |
| title_fullStr | Experimental and numerical study of aromatic species formation in counterflow diffusion flames Martina Baroncelli |
| title_full_unstemmed | Experimental and numerical study of aromatic species formation in counterflow diffusion flames Martina Baroncelli |
| title_short | Experimental and numerical study of aromatic species formation in counterflow diffusion flames |
| title_sort | experimental and numerical study of aromatic species formation in counterflow diffusion flames |
| topic | Verbrennung (DE-588)4062656-8 gnd Gegenstromprinzip (DE-588)4329194-6 gnd Diffusionsflamme (DE-588)4149814-8 gnd Verbrennungsprodukt (DE-588)4187589-8 gnd Polycyclische Aromaten (DE-588)4175141-3 gnd Oxyfuel-Verfahren (DE-588)7628163-2 gnd |
| topic_facet | Verbrennung Gegenstromprinzip Diffusionsflamme Verbrennungsprodukt Polycyclische Aromaten Oxyfuel-Verfahren Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032940077&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT baroncellimartina experimentalandnumericalstudyofaromaticspeciesformationincounterflowdiffusionflames |