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adam_text | TABLE
OF
CONTENTS
INTRODUCTION
.................................................................
12
1
SCOPE
OF
APPLICATION
................................................................................................................
14
*2
GENERAL..........................................
__________________________________________
16
3
HAZARD
ASSESSMENT
AND
SUBSTITUTION
CHECK
............................................................................
18
3.1
PROCEDURE
........................................................................................................................
18
3.2
OBTAINING
INFORMATION
...................................................................................................
24
3.3
DETERMINING
LEVELS
OF
EXPOSURE
.....................................................................................
25
3.3.1
GENERAL
................................................................................................................
25
3.3.2
QUALIFICATION
OF
LABORATORY
PERSONNEL
................................................................
25
3.3.3
STANDARD
LABORATORY
CONDITIONS
..........................................................................
26
3.3.4
USE
OF
LARGER
QUANTITIES
......................................................................................
27
3.4
SPECIAL
FEATURES
OF
LABORATORIES
.....................................................................................
27
3.4.1
EMERGENCIES
AND
FAULTS
......................................................................................
27
3.4.2
INCORPORATION
OF
HAZARDOUS
MATERIALS
DUE
TO
INJURIES
........................................
28
3.4.3
THIRD-PARTY
ACTIVITIES
IN
LABORATORIES
...................................................................
28
3.4.4
TAKING
SPECIAL
ACTIVITIES
INTO
ACCOUNT
.................................................................
28
3.4.5
ACCOMMODATING
PERSONS
WITH
DISABILITIES
IN
THE
LABORATORY
..............................
29
3.4.5.1
BACKGROUND
..........................................................................................
29
3.4.5.2
TECHNICAL
AND
STRUCTURAL
MEASURES
......................................................
30
3.4.5.3
ORGANISATIONAL
MEASURES
.....................................................................
31
3.4.5.4
PERSONAL
PROTECTIVE
MEASURES
............................................................
32
3.5
TAKING
THE
COURSE
OF
THE
REACTION
AND
NEW
MATERIALS
INTO
ACCOUNT
................................
33
3.6
SUBSTITUTING
HAZARDOUS
MATERIALS
..................................................................................
34
3.7
EMPLOYMENT
RESTRICTIONS
................................................................................................
36
3.8
DOCUMENTATION
...............................................................................................................
36
4
GENERALLY
VALID
OPERATING
INSTRUCTIONS.....................
...........
38
4.1
OPERATING
INSTRUCTIONS
...................................................................................................
38
4.2
INSTRUCTION
......................................................................................................................
39
4.3
GENERAL
PRINCIPLES
FOR
WORKING
IN
LABORATORIES
...............................................................
41
4.3.1
AVOIDING
HAZARDS
.................................................................................................
41
4.3.2
ASSIGNING
WORK
...................................................................................................
41
4.3.3
WORKING
ALONE
.....................................................................................................
42
4.3.4
REPORTING
DEFECTS
................................................................................................
42
4.3.5
MONITORING
AND
SAFEGUARDS
...............................................................................
43
4.3.6
EFFECTIVENESS
OF
PROTECTIVE
MEASURES
..................................................................
43
4.3.7
TWO-WAY
INFORMATION
.........................................................................................
44
4
4.3.8
NOTIFYING
SUPERIORS
OF
DAMAGE
TO
HEALTH
...........................................................44
4.3.9
EMERGENCY
MEASURES
.........................................................................................44
4.4
CLOTHING
AND
FOOTWEAR
...................................................................................................
45
4.4.1
WORK
CLOTHES
AND
PROTECTIVE
CLOTHING
.................................................................
45
4.4.2
FOOTWEAR
.............................................................................................................
46
4.5
PERSONAL
PROTECTIVE
EQUIPMENT
......................................................................................
47
4.5.1
GENERAL
...............................................................................................................
47
4.5.2
EYE
PROTECTION
.....................................................................................................
47
4.5.3
HAND
PROTECTION
.................................................................................................
49
4.5.4
RESPIRATORY
DEVICES.............................................................................................
50
4.5.5
PROTECTIVE
CLOTHING
.............................................................................................
50
4.6
HYGIENE
...........................................................................................................................
51
4.6.1
GENERAL
MEASURES
...............................................................................................
51
4.6.2
FOOD,
BEVERAGES
AND
COSMETICS
...........................................................................
51
4.6.3
SKIN
PROTECTION
....................................................................................................
52
4.6.4
STORING
WORK
CLOTHES
AND
PROTECTIVE
CLOTHING
....................................................
52
4.6.5
CLEANING
WORK
CLOTHES
AND
PROTECTIVE
CLOTHING
.................................................
52
4.6.6
RESPIRATORY
DEVICE
HYGIENE
.................................................................................
53
4.7
FIRST
AID
AND
OCCUPATIONAL
MEDICINE
...............................................................................
53
4.7.1
FIRST
AID
...............................................................................................................
53
4.7.1.1
GENERAL
................................................................................................
53
4.7.1.2
OBLIGATION
TO
PROVIDE
INFORMATION
.......................................................
54
4.7.1.3
FIRST
AID
EQUIPMENT
.............................................................................
54
4.7.1.4
MEASURES.............................................................................................
55
4.7.2
OCCUPATIONAL
MEDICINE
.......................................................................................
56
4.8
FIRE
PROTECTION
................................................................................................................
57
4.8.1
FIRE
EXTINGUISHING
FACILITIES
................................................................................
57
4.8.2
EXTINGUISHING
DRILLS
............................................................................................
59
4.8.3
CONDUCT
IN
THE
EVENT
OF
A
FIRE
.............................................................................
59
4.8.4
FIRE-FIGHTING
........................................................................................................
59
4.8.5
COMPRESSED-GAS
CYLINDERS
IN
THE
EVENT
OF
A
FIRE
.................................................
60
4.9
STORAGE
AND
AVAILABILITY
OF
HAZARDOUS
MATERIALS
............................................................
60
4.9.1
GENERAL
SPECIFICATIONS
........................................................................................
60
4.9.2
SETTING
DOWN
SAFELY
...........................................................................................
62
4.9.3
ACCESS
.................................................................................................................
63
4.9.4
INVENTORY
CHECKING
.............................................................................................
64
4.10
TRANSFERRING
AND
TRANSPORTING
HAZARDOUS
MATERIALS
......................................................
64
4.10.1
TRANSFER...............................................................................................................
64
4.10.2
EMPTYING
AT
OVERPRESSURE..................................................................................
65
4.10.3
TRANSPORT
............................................................................................................
65
4.11
RELEASE
OF
GASES,
VAPORS
OR
SUSPENDED
MATTER
..............................................................
66
4.11.1
WORK
IN
FUME
HOODS
..........................................................................................
66
4.11.2
UNINTENTIONAL
RELEASE
OF
MATERIALS
AND
ACCIDENTS
.............................................
68
4.12
WORK
WITH
FLAMMABLE
MATERIALS
...................................................................................
70
4.12.1
EXPLOSION
PROTECTION
MEASURES
.........................................................................
70
4.12.2
IGNITION
HAZARDS
DUE
TO
ELECTROSTATIC
CHARGING
..................................................
71
5
4.13
WORK
INVOLVING
LARGE
QUANTITIES
OF
HAZARDOUS
MATERIALS
...............................................
72
4.14
OPEN
EVAPORATION
...........................................................................................................
72
4.15
STORAGE
AND
PROVISION
OF
FLAMMABLE
LIQUIDS
..................................................................
73
4.15.1
LIMITING
QUANTITIES
AT
THE
WORKPLACE
..................................................................
73
4.15.2
WASHING
LIQUIDS
..................................................................................................
73
4.15.3
HANDLING
EMPTIED
CONTAINERS
.............................................................................
74
4.16
WASTE
MANAGEMENT
.......................................................................................................
74
4.16.1
COLLECTION
AND
TRANSPORT
.....................................................................................
74
4.16.1.1
COLLECTION
............................................................................................
74
4.16.1.2
CHEMICALLY
CONTAMINATED
APPLIANCES
.................................................
75
4.16.1.3
WASTE
COLLECTION
CONTAINERS
...............................................................
75
4.16.2
WASTE
DISPOSAL
....................................................................................................
76
4.17
CLEANING
.........................................................................................................................
76
4.18
SAFETY
DEVICES
.................................................................................................................
77
4.18.1
OPERATION
OF
SAFETY
DEVICES
................................................................................
77
4.18.2
WORK
ON
SAFETY
DEVICES
.......................................................................................
77
4.19
BANS
ON
MANUFACTURE
AND
USE
........................................................................................
78
4.20
ERGONOMICS.....................................................................................................................
78
4.20.1
GENERAL
REQUIREMENTS
.........................................................................................
78
4.20.2
LIGHTING
AND
EMERGENCY
LIGHTING
.......................................................................
79
4.20.2.1
LIGHTING
..............................................................................................
79
4.20.2.2
EMERGENCY
LIGHTING
FOR
ESCAPE
ROUTES
..............................................
80
4.20.2.3
EMERGENCY
LIGHTING
FOR
PARTICULARLY
HAZARDOUS
WORK
AREAS
...............
81
4.20.3
AMBIENT
CLIMATE
..................................................................................................
81
4.20.4
WORKSTATIONS
WITH
SCREENS.................................................................................
82
4.21
ACTIVITIES
OF
EXTERNAL
PERSONNEL
IN
THE
LABORATORY
..........................................................
82
4.22
NOTIFYING
THE
AUTHORITIES
................................................................................................
83
5
SPECIAL
OPERATING
INSTRUCTIONS...........
...............
....................................
.....
.
....
................................85
5.1
LABORATORY
ACTIVITIES
.......................................................................................................
85
5.1.1
WORK
INVOLVING
SPONTANEOUSLY
FLAMMABLE
MATERIALS
........................................
85
5.1.2
WORK
INVOLVING
PEROXIDE-FORMING
LIQUIDS
...........................................................
85
5.1.3
WORK
INVOLVING
EXPLOSIVE
MATERIALS
....................................................................
86
5.1.3.1
PROTECTIVE
MEASURES............................................................................
86
5.1.3.2
AMMONIACAL
SILVER
SALT
SOLUTIONS
.........................................................
87
5.1.3.3
ACETYLIDES
............................................................................................
87
5.1.3.4
PERCHLORATES
........................................................................................
88
5.1.3.5
ALKALI
METALS
AND
ALKALI
METAL
AMIDES
.................................................
88
5.1.4
DEALING
WITH
IONIZING
RADIATION
..........................................................................
89
5.1.5
DRYING
OF
SOLVENTS
...............................................................................................
90
5.1.6
WORKING
WITH
EVACUATED
EQUIPMENT
..................................................................
90
5.1.6.1
THIN-WALLED
GLASS
VESSELS...................................................................
90
5.1.6.2
VACUUM
DISTILLATION
............................................................................
91
5.1.7
WORKING
WITH
CATEGORY
1
AND
2
CARCINOGENIC,
MUTAGENIC
AND
REPROTOXIC
MATERIALS
....................................................................................
91
6
5.2
OPERATION
OF
APPARATUS
AND
EQUIPMENT
........................................................................
93
5.2.1
SETTING
UP
APPARATUS
..........................................................................................
93
5.2.1.1
ABSENCE
OF
STRESSES............................................................................
93
5.2.1.2
FLOW
CONDITIONS
.................................................................................
94
5.2.1.3
TALL
APPARATUS
.....................................................................................
95
5.2.2
WORKING
WITH
CYLINDRICAL
GLASS
PARTS
..................................................................
95
5.2.2.1
GLASS-BLOWING
WORK
...........................................................................
95
5.2.2.2
PERMISSIBLE
GLASS
TEMPERATURES
.........................................................
96
5.2.3
CONNECTORS
AND
STOPPERS
...................................................................................
96
5.2.4
HOSES
AND
FITTINGS
...............................................................................................
97
5.2.4.1
SELECTION
.............................................................................................
97
5.2.5
GAS
BURNERS
.........................................................................................................
98
5.2.6
OPERATING
APPARATUS
..........................................................................................
99
5.2.6.1
EXPLOSION
HAZARDS
..............................................................................
99
5.2.6.2
INCREASED
HAZARDS
IN
THE
EVENT
OF
A
POWER
FAILURE
..........................
100
5.2.6.3
DRYING
CAPILLARIES
AND
ABSORPTION
VESSELS.......................................
100
5.2.6.4
THERMAL
INSULATION
OF
HOT
PARTS
......................................................
100
5.2.6.5
BARRIER
VESSELS
...................................................................................
101
5.2.6.6
DISTILLATION
APPARATUS
......................................................................
101
5.2.6.7
MOBILE
ELECTRICAL
EQUIPMENT
............................................................
103
5.2.7
HEATING
BATHS
AND
HEATING
..............................................................................
104
5.2.7.1
HEATING
LIQUID
HEATING
BATHS
...........................................................
104
5.2.7.2
MAXIMUM
OPERATING
TEMPERATURE
OF
HEAT
CARRIERS
.........................
105
5.2.7.3
TEMPERATURE
CONTROL
........................................................................
105
5.2.7.4
STABILITY
...........................................................................................
106
5.2.7.5
HEAT
CARRIERS
....................................................................................
106
5.2.8
DRYING
IN
HEATING
OVENS
...................................................................................
107
5.2.8.1
EXPLOSION
PROTECTION
........................................................................
107
5.2.8.2
VENTILATION
.......................................................................................
107
5.2.8.3
THERMALLY
UNSTABLE
MATERIALS
..........................................................
108
5.2.9
REFRIGERATION
APPLIANCES
..................................................................................
108
5.2.9.1
REFRIGERATORS
AND
FREEZERS
................................................................
108
5.2.9.2
SIGNS
ON
REFRIGERATORS
......................................................................
109
5.2.10
DEEP
COOLING
.....................................................................................................
109
5.2.10.1
FIRE
AND
REACTION
HAZARDS
.................................................................
109
5.2.10.2
COVERING
DEEP
COOLING
BATHS
............................................................
110
5.2.10.3
DEWARVESSELS
..................................................................................
110
5.2.10.4
LIQUID
NITROGEN
.................................................................................
110
5.2.10.5
LOW-TEMPERATURE
COOLING
BATHS
......................................................
ILL
5.2.10.6
WORK
INVOLVING
LIQUEFIED
GASES
........................................................
ILL
5.2.11
COMPRESSED-GAS
CYLINDERS
AND
FITTINGS
............................................................
112
5.2.11.1
FIRE
PROTECTION
..................................................................................
112
5.2.11.2
WARNING
SIGNS
..................................................................................
113
5.2.11.3
SAFEGUARDS
AGAINST
EXTERNAL
EFFECTS
.................................................
113
5.2.11.4
PROTECTION
AGAINST
TOXIC
GASES
.........................................................
114
5.2.11.5
IDENTIFICATION
OF
COMPRESSED-GAS
CYLINDERS
.....................................
114
7
5.2.11.6
LIMITS
ON
VOLUMES
.............................................................................
116
5.2.11.7
OXIDIZING
COMPRESSED
GASES
..............................................................
116
5.2.11.8
TRANSFERRING
GASES
.............................................................................
116
5.2.11.9
GAS
HOSES
..........................................................................................
117
5.2.11.10
VALVES
................................................................................................
117
5.2.11.11
FEEDING
IN
GASES
...............................................................................
117
5.2.11.12
PRESSURE
REDUCERS
..............................................................................
118
5.2.11.13
LEAK
TEST
............................................................................................
119
5.2.11.14
TRANSPORT
..........................................................................................
119
5.2.11.15
INSPECTION
DATE
.................................................................................
120
5.2.12
PRESSURE
DEVICES
AND
EXPERIMENTAL
AUTOCLAVES
................................................
120
5.2.12.1
PRESSURE
DEVICES
...............................................................................
120
5.2.12.2
EXPERIMENTAL
AUTOCLAVES
..................................................................
120
5.2.13
CARIUS
TUBES
AND
CARIUS
OVENS
..........................................................................
121
5.2.13.1
CARIUS
TUBES
......................................................................................
121
5.2.13.2
CARIUS
OVENS
......................................................................................
121
5.2.14
LABORATORY
AND
ULTRA-CENTRIFUGES
.....................................................................
122
5.2.14.1
INSTALLATION
.......................................................................................
122
5.2.14.2
CENTRIFUGE
OPERATION
........................................................................
122
5.2.15
LASER
RADIATION
..................................................................................................
123
5.2.16
UV
RADIATION
......................................................................................................
124
5.2.17
ROTARY
EVAPORATORS
............................................................................................
125
5.2.18
HOT-AIRBLOWERS
................................................................................................
126
5.2.19
THERMOSTATS
.....................................................................................................
126
5.2.20
COMPRESSORS
AND
VACUUM
PUMPS
.....................................................................
127
5.2.21
ULTRASOUND
........................................................................................................
127
5.2.22
MICROWAVES
.......................................................................................................
128
5.2.22.1
GENERAL
.............................................................................................
128
5.2.22.2
SUPERHEATING
....................................................................................
128
5.2.22.3
REACTIONS
IN
MICROWAVE
EQUIPMENT
.................................................
128
5.2.23
CHROMATOGRAPHY
...............................................................................................
129
5.2.24
ROBOTS
AND
AUTOMATED
LABORATORY
EQUIPMENT
.................................................
130
5.2.25
ELECTROMAGNETIC
AND
MAGNETIC
FIELDS
...............................................................
130
5.2.26
NEEDLES
AND
CANNULAE
.......................................................................................
131
5.2.27
STIRRERS
..............................................................................................................
132
6
TECHNICAL
PROTECTIVE
MEASURES
............................................................................................
133
6.1
AVOIDING
HAZARDS
THROUGH
TECHNICAL
PROTECTIVE
MEASURES
..........................................
133
6.2
WORKPLACE
DESIGN
........................................................................................................
133
6.2.1
OPERATING
AND
CIRCULATION
AREAS
.......................................................................
133
6.2.1.1
LABORATORY
DOCUMENTATION
ZONES
....................................................
134
6.2.2
ESCAPE
AND
RESCUE
ROUTES
..................................................................................
137
6.2.3
DOORS
.................................................................................................................
138
8
6.2.4
FLOORS
................................................................................................................
139
6.2.5
VENTILATION
........................................................................................................
139
6.2.5.1
VENTILATION
SYSTEMS
...........................................................................
139
6.2.5.2
RECIRCULATION
OF
AIR
............................................................................
142
6.3
EXTRACTION
EQUIPMENT
...................................................................................................
142
6.3.1
FUME
HOODS
......................................................................................................
142
6.3.1.1
PROTECTION
OBJECTIVES
.........................................................................
142
6.3.1.2
MATERIALS
...........................................................................................
143
6.3.1.3
PRESSURE
RELIEF
....................................................................................
144
6.3.1.4
SASHES
..............................................................................................
144
6.3.1.5
MONITORING
THE
VENTILATION
FUNCTION
.................................................
145
6.3.1.6
OUTLETS
..............................................................................................
146
6.3.2
DUCTLESS
FILTERING
FUME
ENCLOSURES
...................................................................
146
6.4
WORKBENCHES
AND
THEIR
STORAGE
SPACES
........................................................................
149
6.4.1
WORKBENCHES
....................................................................................................
149
6.4.2
STORAGE
SPACES
FOR
HAZARDOUS
MATERIAL
WASTE
.................................................
149
6.5
SUPPLY
LINES
AND
FITTINGS
..............................................................................................
150
6.5.1
SUPPLY
LINES
.......................................................................................................
150
6.5.2
SHUTOFF
DEVICES
.................................................................................................
151
6.5.3
DRAINAGE
LINES
...................................................................................................
152
6.6
EMERGENCY
SHOWERS
.....................................................................................................
152
6.6.1
EMERGENCY
(OVERHEAD)
SHOWERS
........................................................................
152
6.6.1.1
WATER
FLOW
RATE
AND
LOCATION
...........................................................
152
6.6.1.2
MARKING
............................................................................................
153
6.6.2
EMERGENCY
EYE-WASH
UNITS
...............................................................................
154
6.6.2.1
GENERAL
REQUIREMENTS
.......................................................................
154
6.6.2.2
LOCATION
AND
MARKING
........................................................................
155
6.7
ELECTRICAL
EQUIPMENT
AND
APPLIANCES............................................................................
155
6.7.1
ELECTRICAL
POWER
SUPPLY
FACILITIES
......................................................................
155
6.7.2
EARTHING
............................................................................................................
156
6.7.2.1
CONTACT
PROTECTION
AND
POTENTIAL
EQUALIZATION
MEASURES
.................
156
6.7.2.2
ELECTROSTATIC
DISCHARGING
..................................................................
156
6.7.3
SWITCHES
AND
SOCKETS
........................................................................................
157
6.7.3.1
SWITCHES
AND
SOCKETS
........................................................................
157
6.7.3.2
PROTECTION
AGAINST
SPRAYING
WATER
...................................................
157
7
INSPECTIONS
..........................................
.......................................................
..............151
7.1
INSPECTIONS
...................................................................................................................
158
7.2
EMERGENCY
SHOWERS
.....................................................................................................
158
7.3
FUME
HOODS
..................................................................................................................
158
7.4
SAFETY
CABINETS
FOR
FLAMMABLE
LIQUIDS
.........................................................................
160
9
ANNEX
1:
SAMPLE
ESCAPE
AND
RESCUE
PLAN
...................................................................................
161
ANNEX
2:
SAMPLE
HAND
AND
SKIN
PROTECTION
PLAN
........................................................................
162
ANNEX
3:
LABORATORY
INSPECTIONS
......................
163
1
GENERAL
.................................................................................................................................
163
2
PERIODIC
LABORATORY
INSPECTIONS
.............................................................................................
164
3
PERIODIC
INSPECTIONS
OF
LABORATORY
AND
ANALYTICAL
EQUIPMENT
..............................................
166
4
DOCUMENTATION
......................................................................................................................
167
5
OVERVIEW
OF
INSPECTIONS
........................................................................................................
167
ANNEX
4:
SIMPLIFIED
LABELLING
OF
LABORATORY
CONTAINERS
..........................................
168
1
CHARACTERISTIC
OF
ACTIVITIES
WITH
HAZARDOUS
SUBSTANCES
IN
LABORATORIES
...............................
168
2
DGLIV
SYSTEM
FOR
LABORATORIES
..............................................................................................
169
2.1
CONDENSING
INFORMATION
IN
H-STATEMENTS
THROUGH
PHRASES
................................................
169
2.2
NUMBER
OF
PICTOGRAMS
.........................................................................................................
170
3
PRACTICAL
IMPLEMENTATION
.....................................................................................................
170
ANNEX
5:
CRITERIA
FOR
EXPERT
LABORATORY
DESIGN
UNDER
CONSIDERATION
OF
OCCUPATIONAL
SAFETY
AND
HEALTH
AND
ENVIRONMENTAL
PROTECTION
.......................................174
ANNEX
6:
BIBLIOGRAPHY
..............................
178
SUBJECT
INDEX
..........................
193
PICTURE
CREDITS
...................
199
IO
|
adam_txt |
TABLE
OF
CONTENTS
INTRODUCTION
.
12
1
SCOPE
OF
APPLICATION
.
14
*2
GENERAL.
_
16
3
HAZARD
ASSESSMENT
AND
SUBSTITUTION
CHECK
.
18
3.1
PROCEDURE
.
18
3.2
OBTAINING
INFORMATION
.
24
3.3
DETERMINING
LEVELS
OF
EXPOSURE
.
25
3.3.1
GENERAL
.
25
3.3.2
QUALIFICATION
OF
LABORATORY
PERSONNEL
.
25
3.3.3
STANDARD
LABORATORY
CONDITIONS
.
26
3.3.4
USE
OF
LARGER
QUANTITIES
.
27
3.4
SPECIAL
FEATURES
OF
LABORATORIES
.
27
3.4.1
EMERGENCIES
AND
FAULTS
.
27
3.4.2
INCORPORATION
OF
HAZARDOUS
MATERIALS
DUE
TO
INJURIES
.
28
3.4.3
THIRD-PARTY
ACTIVITIES
IN
LABORATORIES
.
28
3.4.4
TAKING
SPECIAL
ACTIVITIES
INTO
ACCOUNT
.
28
3.4.5
ACCOMMODATING
PERSONS
WITH
DISABILITIES
IN
THE
LABORATORY
.
29
3.4.5.1
BACKGROUND
.
29
3.4.5.2
TECHNICAL
AND
STRUCTURAL
MEASURES
.
30
3.4.5.3
ORGANISATIONAL
MEASURES
.
31
3.4.5.4
PERSONAL
PROTECTIVE
MEASURES
.
32
3.5
TAKING
THE
COURSE
OF
THE
REACTION
AND
NEW
MATERIALS
INTO
ACCOUNT
.
33
3.6
SUBSTITUTING
HAZARDOUS
MATERIALS
.
34
3.7
EMPLOYMENT
RESTRICTIONS
.
36
3.8
DOCUMENTATION
.
36
4
GENERALLY
VALID
OPERATING
INSTRUCTIONS.
.
38
4.1
OPERATING
INSTRUCTIONS
.
38
4.2
INSTRUCTION
.
39
4.3
GENERAL
PRINCIPLES
FOR
WORKING
IN
LABORATORIES
.
41
4.3.1
AVOIDING
HAZARDS
.
41
4.3.2
ASSIGNING
WORK
.
41
4.3.3
WORKING
ALONE
.
42
4.3.4
REPORTING
DEFECTS
.
42
4.3.5
MONITORING
AND
SAFEGUARDS
.
43
4.3.6
EFFECTIVENESS
OF
PROTECTIVE
MEASURES
.
43
4.3.7
TWO-WAY
INFORMATION
.
44
4
4.3.8
NOTIFYING
SUPERIORS
OF
DAMAGE
TO
HEALTH
.44
4.3.9
EMERGENCY
MEASURES
.44
4.4
CLOTHING
AND
FOOTWEAR
.
45
4.4.1
WORK
CLOTHES
AND
PROTECTIVE
CLOTHING
.
45
4.4.2
FOOTWEAR
.
46
4.5
PERSONAL
PROTECTIVE
EQUIPMENT
.
47
4.5.1
GENERAL
.
47
4.5.2
EYE
PROTECTION
.
47
4.5.3
HAND
PROTECTION
.
49
4.5.4
RESPIRATORY
DEVICES.
50
4.5.5
PROTECTIVE
CLOTHING
.
50
4.6
HYGIENE
.
51
4.6.1
GENERAL
MEASURES
.
51
4.6.2
FOOD,
BEVERAGES
AND
COSMETICS
.
51
4.6.3
SKIN
PROTECTION
.
52
4.6.4
STORING
WORK
CLOTHES
AND
PROTECTIVE
CLOTHING
.
52
4.6.5
CLEANING
WORK
CLOTHES
AND
PROTECTIVE
CLOTHING
.
52
4.6.6
RESPIRATORY
DEVICE
HYGIENE
.
53
4.7
FIRST
AID
AND
OCCUPATIONAL
MEDICINE
.
53
4.7.1
FIRST
AID
.
53
4.7.1.1
GENERAL
.
53
4.7.1.2
OBLIGATION
TO
PROVIDE
INFORMATION
.
54
4.7.1.3
FIRST
AID
EQUIPMENT
.
54
4.7.1.4
MEASURES.
55
4.7.2
OCCUPATIONAL
MEDICINE
.
56
4.8
FIRE
PROTECTION
.
57
4.8.1
FIRE
EXTINGUISHING
FACILITIES
.
57
4.8.2
EXTINGUISHING
DRILLS
.
59
4.8.3
CONDUCT
IN
THE
EVENT
OF
A
FIRE
.
59
4.8.4
FIRE-FIGHTING
.
59
4.8.5
COMPRESSED-GAS
CYLINDERS
IN
THE
EVENT
OF
A
FIRE
.
60
4.9
STORAGE
AND
AVAILABILITY
OF
HAZARDOUS
MATERIALS
.
60
4.9.1
GENERAL
SPECIFICATIONS
.
60
4.9.2
SETTING
DOWN
SAFELY
.
62
4.9.3
ACCESS
.
63
4.9.4
INVENTORY
CHECKING
.
64
4.10
TRANSFERRING
AND
TRANSPORTING
HAZARDOUS
MATERIALS
.
64
4.10.1
TRANSFER.
64
4.10.2
EMPTYING
AT
OVERPRESSURE.
65
4.10.3
TRANSPORT
.
65
4.11
RELEASE
OF
GASES,
VAPORS
OR
SUSPENDED
MATTER
.
66
4.11.1
WORK
IN
FUME
HOODS
.
66
4.11.2
UNINTENTIONAL
RELEASE
OF
MATERIALS
AND
ACCIDENTS
.
68
4.12
WORK
WITH
FLAMMABLE
MATERIALS
.
70
4.12.1
EXPLOSION
PROTECTION
MEASURES
.
70
4.12.2
IGNITION
HAZARDS
DUE
TO
ELECTROSTATIC
CHARGING
.
71
5
4.13
WORK
INVOLVING
LARGE
QUANTITIES
OF
HAZARDOUS
MATERIALS
.
72
4.14
OPEN
EVAPORATION
.
72
4.15
STORAGE
AND
PROVISION
OF
FLAMMABLE
LIQUIDS
.
73
4.15.1
LIMITING
QUANTITIES
AT
THE
WORKPLACE
.
73
4.15.2
WASHING
LIQUIDS
.
73
4.15.3
HANDLING
EMPTIED
CONTAINERS
.
74
4.16
WASTE
MANAGEMENT
.
74
4.16.1
COLLECTION
AND
TRANSPORT
.
74
4.16.1.1
COLLECTION
.
74
4.16.1.2
CHEMICALLY
CONTAMINATED
APPLIANCES
.
75
4.16.1.3
WASTE
COLLECTION
CONTAINERS
.
75
4.16.2
WASTE
DISPOSAL
.
76
4.17
CLEANING
.
76
4.18
SAFETY
DEVICES
.
77
4.18.1
OPERATION
OF
SAFETY
DEVICES
.
77
4.18.2
WORK
ON
SAFETY
DEVICES
.
77
4.19
BANS
ON
MANUFACTURE
AND
USE
.
78
4.20
ERGONOMICS.
78
4.20.1
GENERAL
REQUIREMENTS
.
78
4.20.2
LIGHTING
AND
EMERGENCY
LIGHTING
.
79
4.20.2.1
LIGHTING
.
79
4.20.2.2
EMERGENCY
LIGHTING
FOR
ESCAPE
ROUTES
.
80
4.20.2.3
EMERGENCY
LIGHTING
FOR
PARTICULARLY
HAZARDOUS
WORK
AREAS
.
81
4.20.3
AMBIENT
CLIMATE
.
81
4.20.4
WORKSTATIONS
WITH
SCREENS.
82
4.21
ACTIVITIES
OF
EXTERNAL
PERSONNEL
IN
THE
LABORATORY
.
82
4.22
NOTIFYING
THE
AUTHORITIES
.
83
5
SPECIAL
OPERATING
INSTRUCTIONS.
.
.
.
.
.
.85
5.1
LABORATORY
ACTIVITIES
.
85
5.1.1
WORK
INVOLVING
SPONTANEOUSLY
FLAMMABLE
MATERIALS
.
85
5.1.2
WORK
INVOLVING
PEROXIDE-FORMING
LIQUIDS
.
85
5.1.3
WORK
INVOLVING
EXPLOSIVE
MATERIALS
.
86
5.1.3.1
PROTECTIVE
MEASURES.
86
5.1.3.2
AMMONIACAL
SILVER
SALT
SOLUTIONS
.
87
5.1.3.3
ACETYLIDES
.
87
5.1.3.4
PERCHLORATES
.
88
5.1.3.5
ALKALI
METALS
AND
ALKALI
METAL
AMIDES
.
88
5.1.4
DEALING
WITH
IONIZING
RADIATION
.
89
5.1.5
DRYING
OF
SOLVENTS
.
90
5.1.6
WORKING
WITH
EVACUATED
EQUIPMENT
.
90
5.1.6.1
THIN-WALLED
GLASS
VESSELS.
90
5.1.6.2
VACUUM
DISTILLATION
.
91
5.1.7
WORKING
WITH
CATEGORY
1
AND
2
CARCINOGENIC,
MUTAGENIC
AND
REPROTOXIC
MATERIALS
.
91
6
5.2
OPERATION
OF
APPARATUS
AND
EQUIPMENT
.
93
5.2.1
SETTING
UP
APPARATUS
.
93
5.2.1.1
ABSENCE
OF
STRESSES.
93
5.2.1.2
FLOW
CONDITIONS
.
94
5.2.1.3
TALL
APPARATUS
.
95
5.2.2
WORKING
WITH
CYLINDRICAL
GLASS
PARTS
.
95
5.2.2.1
GLASS-BLOWING
WORK
.
95
5.2.2.2
PERMISSIBLE
GLASS
TEMPERATURES
.
96
5.2.3
CONNECTORS
AND
STOPPERS
.
96
5.2.4
HOSES
AND
FITTINGS
.
97
5.2.4.1
SELECTION
.
97
5.2.5
GAS
BURNERS
.
98
5.2.6
OPERATING
APPARATUS
.
99
5.2.6.1
EXPLOSION
HAZARDS
.
99
5.2.6.2
INCREASED
HAZARDS
IN
THE
EVENT
OF
A
POWER
FAILURE
.
100
5.2.6.3
DRYING
CAPILLARIES
AND
ABSORPTION
VESSELS.
100
5.2.6.4
THERMAL
INSULATION
OF
HOT
PARTS
.
100
5.2.6.5
BARRIER
VESSELS
.
101
5.2.6.6
DISTILLATION
APPARATUS
.
101
5.2.6.7
MOBILE
ELECTRICAL
EQUIPMENT
.
103
5.2.7
HEATING
BATHS
AND
HEATING
.
104
5.2.7.1
HEATING
LIQUID
HEATING
BATHS
.
104
5.2.7.2
MAXIMUM
OPERATING
TEMPERATURE
OF
HEAT
CARRIERS
.
105
5.2.7.3
TEMPERATURE
CONTROL
.
105
5.2.7.4
STABILITY
.
106
5.2.7.5
HEAT
CARRIERS
.
106
5.2.8
DRYING
IN
HEATING
OVENS
.
107
5.2.8.1
EXPLOSION
PROTECTION
.
107
5.2.8.2
VENTILATION
.
107
5.2.8.3
THERMALLY
UNSTABLE
MATERIALS
.
108
5.2.9
REFRIGERATION
APPLIANCES
.
108
5.2.9.1
REFRIGERATORS
AND
FREEZERS
.
108
5.2.9.2
SIGNS
ON
REFRIGERATORS
.
109
5.2.10
DEEP
COOLING
.
109
5.2.10.1
FIRE
AND
REACTION
HAZARDS
.
109
5.2.10.2
COVERING
DEEP
COOLING
BATHS
.
110
5.2.10.3
DEWARVESSELS
.
110
5.2.10.4
LIQUID
NITROGEN
.
110
5.2.10.5
LOW-TEMPERATURE
COOLING
BATHS
.
ILL
5.2.10.6
WORK
INVOLVING
LIQUEFIED
GASES
.
ILL
5.2.11
COMPRESSED-GAS
CYLINDERS
AND
FITTINGS
.
112
5.2.11.1
FIRE
PROTECTION
.
112
5.2.11.2
WARNING
SIGNS
.
113
5.2.11.3
SAFEGUARDS
AGAINST
EXTERNAL
EFFECTS
.
113
5.2.11.4
PROTECTION
AGAINST
TOXIC
GASES
.
114
5.2.11.5
IDENTIFICATION
OF
COMPRESSED-GAS
CYLINDERS
.
114
7
5.2.11.6
LIMITS
ON
VOLUMES
.
116
5.2.11.7
OXIDIZING
COMPRESSED
GASES
.
116
5.2.11.8
TRANSFERRING
GASES
.
116
5.2.11.9
GAS
HOSES
.
117
5.2.11.10
VALVES
.
117
5.2.11.11
FEEDING
IN
GASES
.
117
5.2.11.12
PRESSURE
REDUCERS
.
118
5.2.11.13
LEAK
TEST
.
119
5.2.11.14
TRANSPORT
.
119
5.2.11.15
INSPECTION
DATE
.
120
5.2.12
PRESSURE
DEVICES
AND
EXPERIMENTAL
AUTOCLAVES
.
120
5.2.12.1
PRESSURE
DEVICES
.
120
5.2.12.2
EXPERIMENTAL
AUTOCLAVES
.
120
5.2.13
CARIUS
TUBES
AND
CARIUS
OVENS
.
121
5.2.13.1
CARIUS
TUBES
.
121
5.2.13.2
CARIUS
OVENS
.
121
5.2.14
LABORATORY
AND
ULTRA-CENTRIFUGES
.
122
5.2.14.1
INSTALLATION
.
122
5.2.14.2
CENTRIFUGE
OPERATION
.
122
5.2.15
LASER
RADIATION
.
123
5.2.16
UV
RADIATION
.
124
5.2.17
ROTARY
EVAPORATORS
.
125
5.2.18
HOT-AIRBLOWERS
.
126
5.2.19
THERMOSTATS
.
126
5.2.20
COMPRESSORS
AND
VACUUM
PUMPS
.
127
5.2.21
ULTRASOUND
.
127
5.2.22
MICROWAVES
.
128
5.2.22.1
GENERAL
.
128
5.2.22.2
SUPERHEATING
.
128
5.2.22.3
REACTIONS
IN
MICROWAVE
EQUIPMENT
.
128
5.2.23
CHROMATOGRAPHY
.
129
5.2.24
ROBOTS
AND
AUTOMATED
LABORATORY
EQUIPMENT
.
130
5.2.25
ELECTROMAGNETIC
AND
MAGNETIC
FIELDS
.
130
5.2.26
NEEDLES
AND
CANNULAE
.
131
5.2.27
STIRRERS
.
132
6
TECHNICAL
PROTECTIVE
MEASURES
.
133
6.1
AVOIDING
HAZARDS
THROUGH
TECHNICAL
PROTECTIVE
MEASURES
.
133
6.2
WORKPLACE
DESIGN
.
133
6.2.1
OPERATING
AND
CIRCULATION
AREAS
.
133
6.2.1.1
LABORATORY
DOCUMENTATION
ZONES
.
134
6.2.2
ESCAPE
AND
RESCUE
ROUTES
.
137
6.2.3
DOORS
.
138
8
6.2.4
FLOORS
.
139
6.2.5
VENTILATION
.
139
6.2.5.1
VENTILATION
SYSTEMS
.
139
6.2.5.2
RECIRCULATION
OF
AIR
.
142
6.3
EXTRACTION
EQUIPMENT
.
142
6.3.1
FUME
HOODS
.
142
6.3.1.1
PROTECTION
OBJECTIVES
.
142
6.3.1.2
MATERIALS
.
143
6.3.1.3
PRESSURE
RELIEF
.
144
6.3.1.4
SASHES
.
144
6.3.1.5
MONITORING
THE
VENTILATION
FUNCTION
.
145
6.3.1.6
OUTLETS
.
146
6.3.2
DUCTLESS
FILTERING
FUME
ENCLOSURES
.
146
6.4
WORKBENCHES
AND
THEIR
STORAGE
SPACES
.
149
6.4.1
WORKBENCHES
.
149
6.4.2
STORAGE
SPACES
FOR
HAZARDOUS
MATERIAL
WASTE
.
149
6.5
SUPPLY
LINES
AND
FITTINGS
.
150
6.5.1
SUPPLY
LINES
.
150
6.5.2
SHUTOFF
DEVICES
.
151
6.5.3
DRAINAGE
LINES
.
152
6.6
EMERGENCY
SHOWERS
.
152
6.6.1
EMERGENCY
(OVERHEAD)
SHOWERS
.
152
6.6.1.1
WATER
FLOW
RATE
AND
LOCATION
.
152
6.6.1.2
MARKING
.
153
6.6.2
EMERGENCY
EYE-WASH
UNITS
.
154
6.6.2.1
GENERAL
REQUIREMENTS
.
154
6.6.2.2
LOCATION
AND
MARKING
.
155
6.7
ELECTRICAL
EQUIPMENT
AND
APPLIANCES.
155
6.7.1
ELECTRICAL
POWER
SUPPLY
FACILITIES
.
155
6.7.2
EARTHING
.
156
6.7.2.1
CONTACT
PROTECTION
AND
POTENTIAL
EQUALIZATION
MEASURES
.
156
6.7.2.2
ELECTROSTATIC
DISCHARGING
.
156
6.7.3
SWITCHES
AND
SOCKETS
.
157
6.7.3.1
SWITCHES
AND
SOCKETS
.
157
6.7.3.2
PROTECTION
AGAINST
SPRAYING
WATER
.
157
7
INSPECTIONS
.
.
.151
7.1
INSPECTIONS
.
158
7.2
EMERGENCY
SHOWERS
.
158
7.3
FUME
HOODS
.
158
7.4
SAFETY
CABINETS
FOR
FLAMMABLE
LIQUIDS
.
160
9
ANNEX
1:
SAMPLE
ESCAPE
AND
RESCUE
PLAN
.
161
ANNEX
2:
SAMPLE
HAND
AND
SKIN
PROTECTION
PLAN
.
162
ANNEX
3:
LABORATORY
INSPECTIONS
.
163
1
GENERAL
.
163
2
PERIODIC
LABORATORY
INSPECTIONS
.
164
3
PERIODIC
INSPECTIONS
OF
LABORATORY
AND
ANALYTICAL
EQUIPMENT
.
166
4
DOCUMENTATION
.
167
5
OVERVIEW
OF
INSPECTIONS
.
167
ANNEX
4:
SIMPLIFIED
LABELLING
OF
LABORATORY
CONTAINERS
.
168
1
CHARACTERISTIC
OF
ACTIVITIES
WITH
HAZARDOUS
SUBSTANCES
IN
LABORATORIES
.
168
2
DGLIV
SYSTEM
FOR
LABORATORIES
.
169
2.1
CONDENSING
INFORMATION
IN
H-STATEMENTS
THROUGH
PHRASES
.
169
2.2
NUMBER
OF
PICTOGRAMS
.
170
3
PRACTICAL
IMPLEMENTATION
.
170
ANNEX
5:
CRITERIA
FOR
EXPERT
LABORATORY
DESIGN
UNDER
CONSIDERATION
OF
OCCUPATIONAL
SAFETY
AND
HEALTH
AND
ENVIRONMENTAL
PROTECTION
.174
ANNEX
6:
BIBLIOGRAPHY
.
178
SUBJECT
INDEX
.
193
PICTURE
CREDITS
.
199
IO |
any_adam_object | 1 |
any_adam_object_boolean | 1 |
author | Conte, Paolo 1937- |
author_GND | (DE-588)12473698X |
author_facet | Conte, Paolo 1937- |
author_role | cmp |
author_sort | Conte, Paolo 1937- |
author_variant | p c pc |
building | Verbundindex |
bvnumber | BV047021393 |
contents | Aguaplano Amada mia Baci senza memoria Bartali Chiamami adesso Come - di Come mi vuoi? Do - do Don't throw it in the W.C. Elisir Genova per noi Gli impermeabli Gong - ho I giardini pensili hanno fatto il loro tempo <<Il>> maestro <<Il>> treno va <<La>> negra <<La>> petite tendresse <<La>> quadrille Max Nessuno mi ama Novecento Paris, les Paris Parole d'amore scritte a macchina Per quel che vale Sijmadicandhapajiee Sotto le stelle del jazz Troppo difficile Un fachiro al cinema Un gelato al limon Via con me |
ctrlnum | (OCoLC)1226704433 (DE-599)BVBBV047021393 |
format | Musical Score Book |
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id | DE-604.BV047021393 |
illustrated | Not Illustrated |
index_date | 2024-07-03T15:59:16Z |
indexdate | 2024-07-10T09:00:22Z |
institution | BVB |
language | English French Italian |
oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032428869 |
oclc_num | 1226704433 |
open_access_boolean | |
owner | DE-384 |
owner_facet | DE-384 |
physical | 1 Partitur (119 Seiten) |
publishDate | 2019 |
publishDateSearch | 2019 |
publishDateSort | 2019 |
publisher | Hal Leonard Europe |
record_format | marc |
spelling | Conte, Paolo 1937- (DE-588)12473698X cmp Antologia Paolo Conte [London] Hal Leonard Europe [2019] © 2019 1 Partitur (119 Seiten) ntm rdacontent n rdamedia nc rdacarrier Aguaplano Amada mia Baci senza memoria Bartali Chiamami adesso Come - di Come mi vuoi? Do - do Don't throw it in the W.C. Elisir Genova per noi Gli impermeabli Gong - ho I giardini pensili hanno fatto il loro tempo <<Il>> maestro <<Il>> treno va <<La>> negra <<La>> petite tendresse <<La>> quadrille Max Nessuno mi ama Novecento Paris, les Paris Parole d'amore scritte a macchina Per quel che vale Sijmadicandhapajiee Sotto le stelle del jazz Troppo difficile Un fachiro al cinema Un gelato al limon Via con me DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032428869&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis (DE-588)4173447-6 Partitur gnd-music |
spellingShingle | Conte, Paolo 1937- Antologia Aguaplano Amada mia Baci senza memoria Bartali Chiamami adesso Come - di Come mi vuoi? Do - do Don't throw it in the W.C. Elisir Genova per noi Gli impermeabli Gong - ho I giardini pensili hanno fatto il loro tempo <<Il>> maestro <<Il>> treno va <<La>> negra <<La>> petite tendresse <<La>> quadrille Max Nessuno mi ama Novecento Paris, les Paris Parole d'amore scritte a macchina Per quel che vale Sijmadicandhapajiee Sotto le stelle del jazz Troppo difficile Un fachiro al cinema Un gelato al limon Via con me |
title | Antologia |
title_alt | Aguaplano Amada mia Baci senza memoria Bartali Chiamami adesso Come - di Come mi vuoi? Do - do Don't throw it in the W.C. Elisir Genova per noi Gli impermeabli Gong - ho I giardini pensili hanno fatto il loro tempo <<Il>> maestro <<Il>> treno va <<La>> negra <<La>> petite tendresse <<La>> quadrille Max Nessuno mi ama Novecento Paris, les Paris Parole d'amore scritte a macchina Per quel che vale Sijmadicandhapajiee Sotto le stelle del jazz Troppo difficile Un fachiro al cinema Un gelato al limon Via con me |
title_auth | Antologia |
title_exact_search | Antologia |
title_exact_search_txtP | Antologia |
title_full | Antologia Paolo Conte |
title_fullStr | Antologia Paolo Conte |
title_full_unstemmed | Antologia Paolo Conte |
title_short | Antologia |
title_sort | antologia |
url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032428869&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
work_keys_str_mv | AT contepaolo antologia |