Practical rubber rheology and dynamic properties:
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[2023]
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| Beschreibung: | XV, 368 Seiten Illustrationen, Diagramme 25 cm |
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MARC
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| 020 | |a 9781569906170 |c : EUR 139.95 (DE) |9 978-1-56990-617-0 | ||
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| 100 | 1 | |a Dick, John S. |d 1945- |e Verfasser |0 (DE-588)1145742114 |4 aut | |
| 245 | 1 | 0 | |a Practical rubber rheology and dynamic properties |c John S. Dick, Henry Pawlowski |
| 264 | 1 | |a Munich |b Hanser |c [2023] | |
| 264 | 4 | |c © 2023 | |
| 300 | |a XV, 368 Seiten |b Illustrationen, Diagramme |c 25 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 0 | 7 | |a Viskosimetrie |0 (DE-588)4188415-2 |2 gnd |9 rswk-swf |
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| 650 | 0 | 7 | |a Dynamisches Verhalten |0 (DE-588)4140475-0 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Rheologische Eigenschaft |0 (DE-588)4366895-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Kautschukindustrie |0 (DE-588)4163517-6 |2 gnd |9 rswk-swf |
| 653 | |a FBKTKAUT: Elastomere und Kautschuk | ||
| 653 | |a PLAS2020 | ||
| 689 | 0 | 0 | |a Rheologie |0 (DE-588)4049828-1 |D s |
| 689 | 0 | 1 | |a Kautschukindustrie |0 (DE-588)4163517-6 |D s |
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| 689 | 1 | 3 | |a Dynamisches Verhalten |0 (DE-588)4140475-0 |D s |
| 689 | 1 | |5 DE-604 | |
| 700 | 1 | |a Pawlowski, Henry |e Verfasser |4 aut | |
| 710 | 2 | |a Hanser Publications |0 (DE-588)1064064051 |4 pbl | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe |z 978-1-56990-618-7 |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032309824&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
Datensatz im Suchindex
| _version_ | 1805075496055078912 |
|---|---|
| adam_text |
THE
AUTHORS
V
PREFACE
.
VII
1
OVERVIEW
OF
RUBBER
RHEOLOGY
AND
DYNAMIC
PROPERTY
TESTS
.
1
1.1
INTRODUCTION
TO
THE
UNIQUENESS
OF
RUBBER
RHEOLOGY
.
1
1.2
BASIC
TENSILE
TESTING
.
3
1.3
HARDNESS
TESTING
.
5
1.4
DENSITY
.
6
1.5
MOONEY
VISCOSITY
.
7
1.6
ODR
CUREMETER
.
10
1.7
CAPILLARY
RHEOMETER
.
12
1.8
MOVING
DIE
RHEOMETER
(MDR)
.
13
1.9
RUBBER
PROCESS
ANALYZER
(RPA)
.
15
1.10
DYNAMIC
MECHANICAL
ANALYZER
(DMA)
.
16
1.11
FLEX
FATIGUE
TESTERS
.
18
1.12
FLEXOMETER
DELTA
T
.
19
1.13
MEASURING
DISPERSION
.
20
1.14
OTHER
RELEVANT
RUBBER
TESTS
.
22
1.14.1
COMPRESSION
PLASTIMETERS
.
22
1.14.2
TEAR
PROPERTIES
.
23
1.14.3
ELECTRICAL
CONDUCTIVITY
PROPERTIES
.
24
1.14.4
DIFFERENTIAL
SCANNING
CALORIMETRY
(DSC)
.
24
1.14.5
THERMOGRAVIMETRIC
ANALYSIS
(TGA)
.
25
1.14.6
FOURIER
TRANSFORM
INFRARED
SPECTROSCOPY
(FTIR)
.
26
1.14.7
ATTENUATED
TOTAL
REFLECTANCE
(ATR)
.
28
1.14.8
GEL
PERMEATION
CHROMATOGRAPHY
(GPC)
.
28
1.14.9
NUCLEAR
MAGNETIC
RESONANCE
SPECTROSCOPY
(NMR)
.
28
1.14.10
BET
(BRUNAUER,
EMMETT,
AND
TELLER)
NITROGEN
ADSORPTION
SURFACE
AREA
APPARATUS
.
29
1.14.11
THERMAL
CONDUCTIVITY
METERS
.
29
2
MOONEY
VISCOMETER
.
35
2.1
DESCRIPTION
OF
THE
MOONEY
VISCOMETER
.
35
2.2
MOONEY
TESTS
.
37
2.3
MOONEY
VISCOSITY
.
37
2.4
MEASURING
MOONEY
SCORCH
.
42
2.5
MEASURING
MOONEY
STRESS
RELAXATION
.
46
2.6
DELTA
MOONEY
TEST
FOR
OIL
EXTENDED
EMULSION
SBR
.
48
2.7
VARIABLE
SPEED
MOONEY
.
49
2.8
LIMITATIONS
OF
THE
MOONEY
VISCOMETER
.
51
3
CAPILLARY
RHEOMETER
.
55
3.1
INTRODUCTION
.
55
3.2
BASIC
TYPES
OF
CAPILLARY
RHEOMETERS
.
57
3.3
MEASUREMENT
OF
VISCOSITY
WITH
A
CAPILLARY
RHEOMETER
.
58
3.4
TYPES
OF
CAPILLARY
RHEOMETER
TESTS
.
59
3.4.1
STABILITY
TEST
.
60
3.4.2
SHEAR
RATE
SWEEP
.
61
3.4.3
MEASURE
OF
TRUE
VISCOSITY
WITH
CAPILLARY
RHEOMETERS
BY
USING
CORRECTIONS
.
63
3.4.3.1
BAGLEY
CORRECTION
.
63
3.4.3.2
RABINOWITSCH
CORRECTION
.
64
3.4.4
CAPILLARY
RHEOMETER
WALL
SLIPPAGE
.
64
3.5
BEHAVIOR
OF
NON-NEWTONIAN
MATERIALS
.
65
3.6
APPEARANCE
OF
CAPILLARY
RHEOMETER
EXTRUDATE
.
69
3.7
CAPILLARY
RHEOMETRY
IN
FACTORY
PROBLEM
SOLVING
.
71
3.8
PREDICTION
OF
FACTORY
PROCESSABILITY
WITH
CAPILLARY
RHEOMETERS
.
72
3.9
LIMITATIONS
OF
CAPILLARY
RHEOMETERS
IN
RUBBER
TESTING
.
74
4
CUREMETERS
.
77
4.1
OSCILLATING
DISC
RHEOMETER
.
77
4.2
MOVING
DIE
RHEOMETER
.
79
4.3
ASTM
D2084
AND
D5289
DATA
POINTS
FOR
CUREMETERS
.
84
4.4
DYNAMIC
PROPERTIES
MEASURED
WITH
AN
MDR
.
87
4.5
ASTM
AND
ISO
STANDARDS
FOR
CUREMETERS
AND
THE
SELECTION
OF
TEST
CONDITIONS
.
92
4.6
THE
RPA
AS
A
CUREMETER
.
94
4.6.1
DESCRIPTION
OF
THE
RPA
AS
A
CUREMETER
.
94
4.6.2
USING
RPA
DYNAMIC
DATA
FOR
ANALYZING
CURE
CURVES
.
94
4.6.2.1
TMAXS
DURING
CURE
(TIME
TO
S"
PEAK)
.
94
4.6.2.2
S'
AND
S"
DUE
TO
CROSSLINK
DENSITY
.
96
4.6.2.3
S'
AND
S"
DUE
TO
FILLER
LOADING
.
97
4.6.3
EFFECT
OF
OIL
.
99
5
VISCOELASTIC
CHARACTERIZATION
OF
RUBBER
.
101
5.1
INTRODUCTION
TO
THE
VISCOELASTIC
PROPERTY
.
101
5.2
PURE
ELASTICITY
.
101
5.3
PURE
VISCOSITY
.
103
5.4
MODELING
VISCOSITY
.
106
5.5
VISCOELASTIC
PROPERTIES
.
107
5.6
MEASUREMENT
OF
VISCOELASTIC
PROPERTIES
WITH
SINUSOIDAL
DEFORMATION
.
110
5.7
APPLICATIONS
FOR
VISCOELASTIC
PROPERTIES
.
114
5.8
INSTRUMENTS
WITH
MULTIPLE
TEST
CAPABILITIES
.
114
5.9
RPA
TEST
CONDITIONS
.
123
5.10
THE
ADVANTAGES
OF
THE
RPA
OVER
SCIENTIFIC
DMAS
.
125
5.11
THE
BASICS
OF
MEASURING
AND
CALCULATING
DYNAMIC
MODULI
.
128
5.12
THE
BASICS
OF
MEASURING
AND
CALCULATING
DYNAMIC
VISCOSITY
.
132
5.13
COMPLIANCE
.
136
5.14
EXTENSION/COMPRESSION
MODULUS
AND
COMPLIANCE
.
137
5.15
SPRING
RATE
CONSTANTS
AND
DAMPING
COEFFICIENTS
.
140
5.16
TIME
TEMPERATURE
SUPERPOSITIONING
(TTS)
.
142
5.17
STATISTICAL
EVALUATION
OF
RHEOMETERS
.
145
6
TYPES
OF
RUBBER
RPA
RHEOLOGICAL
TESTS
.
151
6.1
SUMMARY
OF
RPA
RHEOLOGICAL
DATA
.
151
6.2
TYPES
OF
RPA
RHEOLOGICAL
SUBTESTS
.
152
6.2.1
TIMED
.
152
6.2.2
TEMPERATURE
SWEEP
.
154
6.2.3
VTA
(THERMAL
RAMP)
.
157
6.2.4
FREQUENCY
SWEEP
.
159
6.2.5
STRAIN
SWEEP:
LOW
.
161
6.2.6
STRAIN
SWEEP:
HIGH
.
163
6.2.7
MATRIX
.
165
6.2.8
LAOS
SWEEP
.
165
6.2.9
STRESS
RELAXATION
.
169
6.3
ASTM,
ISO,
AND
DIN
STANDARD
METHODS
FOR
RPA
TESTING
OF
ELASTOMERS
AND
COMPOUNDS
.
170
6.3.1
ASTM
D6204
PART
A
.
170
6.3.2
ASTM
D6204
PART
B
.
172
6.3.3
ASTM
D6204
PARTC
.
172
6.3.4
ASTM
D6204AB
FOR
R&D
.
174
6.3.5
ASTM
D6601
.
175
6.3.6
ASTMD8059
.
177
6.3.7
ASTMD6048
.
179
6.3.8
ASTM
D7050
.
181
6.3.9
ASTM
D7605
.
182
6.3.10
ASTM
D5289
.
184
6.3.11
DIN
53529
.
184
6.3.12
ISO
13145
.
185
6.4
NONSTANDARD
METHODS
FOR
RPA
TESTING
OF
ELASTOMERS
AND
COMPOUNDS
.
186
6.4.1
DISPERSION
USING
DYNAMIC
MECHANICAL
METHODS
.
186
6.4.2
MULTIPLE
FREQUENCY
SWEEPS
WITH INCREASING
STRAINS
.
187
6.4.3
MULTIPLE
IDENTICAL
STRAIN
SWEEPS
.
188
6.4.4
ANAEROBIC
HEAT
AGING
.
189
6.4.5
AEROBIC
HEAT
AGING
.
189
6.4.6
VISCOUS
HEATING
OF
UNCURED
RUBBER
COMPOUNDS
.
190
6.4.7
HEAT
BUILDUP
AT
FOR
CURED
RUBBER
COMPOUND
.
191
7
RAW
RUBBER
EFFECTS
ON
PROCESSABILITY
.
195
7.1
NATURAL
RUBBER
.
195
7.2
SYNTHETIC
RAW
RUBBER
.
201
7.2.1
AVERAGE
MOLECULAR
WEIGHT
.
203
7.2.2
MOLECULAR
WEIGHT
DISTRIBUTION
.
205
7.2.3
LONG
CHAIN
BRANCHING
.
207
7.2.4
GEL
.
209
7.2.5
CHANGES
IN
THE
CHEMICAL
COMPOSITION
.
210
7.2.6
STATISTICAL
CONFOUNDING
.
212
7.3
HIGH
STRAIN
TESTING
OF
SYNTHETIC
ELASTOMERS
.
213
7.4
MEASURING
IMPARTED
DIFFERENCES
IN
SHEAR
THINNING
PROPERTIES
.
214
7.5
STRESS
RELAXATION
OF
ELASTOMERS
AND
PROCESSABILITY
.
215
7.6
MASTER
CURVE
AND
GLASS
TRANSITION
TEMPERATURE
.
217
7.7
WLF
SHIFTS
FOR
RAW
ELASTOMERS
.
220
7.8
TESTING
LIQUID
ELASTOMERS
.
221
7.9
TESTING
THERMOPLASTIC
ELASTOMERS
(TPE)
.
223
7.10
PROCESSABILITY
DATA
ANALYSIS
.
224
8
FILLER
EFFECTS
ON
RUBBER
COMPOUND
PROCESSABILITY
.
229
8.1
FILLER
EFFECTS
ON
RUBBER
COMPOUND
PROPERTIES
.
229
8.2
CARBON
BLACK
EFFECTS
.
232
8.2.1
CARBON
BLACK
SURFACE
AREA
.
234
8.2.2
CORRELATION
WITH
CARBON
BLACK
STRUCTURE
.
240
8.2.3
CORRELATION
WITH
CARBON
BLACK
SURFACE
ACTIVITY
.
245
8.2.4
EFFECTS
OF
VARIATION
IN
LOADING
ON
UNCURED
VS.
CURED
DYNAMIC
PROPERTIES
.
246
8.3
OIL
EFFECTS
.
249
8.4
SILICA
EFFECTS
.
254
8.4.1
EFFECTS
OF
SILANIZATION
.
254
8.4.2
EFFECTS
OF
SILICA
SURFACE
AREA
.
256
8.4.3
EFFECTS
OF
SILICA
LOADING
.
257
8.4.4
RECOVERY
OF
THE
SILICA
NETWORK
AFTER
DESTRUCTION
.
258
8.4.5
SPECIAL
ROLE
OF
STRUCTURE
FOR
SILICA
.
259
8.5
EFFECTS
OF
FULLY
REINFORCING
FILLERS
ON
THE
COX-MERZ
CORRELATION
.
261
8.6
EFFECTS
OF
FILLER
TYPE
AND
CONCENTRATION
ON
SHEAR
THINNING
PROFILES
.
262
8.7
EFFECTS
OF
FILLER
ROOM
TEMPERATURE
STORAGE
ON
FORMATION
OF
BOUND
RUBBER
AND
RHEOLOGY
OF
FILLED
RUBBER
COMPOUNDS
.
263
9
MEASURING
QUALITY
OF
MIX
AND
PROCESSABILITY
.
267
9.1
DISPERSION
OF
FILLERS
DURING
MIXING
.
267
9.2
MASTICATION
OF
ELASTOMERS
DURING
MIXING
.
268
9.3
RHEOLOGICAL
CHANGES
DURING
MIXING
.
268
9.4
OPTIMAL
RHEOLOGICAL
CONDITIONS
FOR
MIX
QUALITY
MEASUREMENT
.
269
9.5
STATE
OF
MIX
AND
PERCENT
DISPERSION
.
271
9.6
EFFECT
OF
OIL
ON
RUBBER
MIXING
.
272
9.7
EFFECT
OF
PHASE
MIXING
.
275
9.8
SPECIAL
TEST
CONDITIONS
FOR
MEASURING
STATE
OF
MIX
.
277
9.8.1
MOONEY
VISCOSITY
.
ZT1
9.8.2
RPA
AT
100%
STRAIN
(ASTM
D6204
PART
B)
.
277
9.8.3
RPA
PAYNE
EFFECT
PLATEAU
(ASTM
D8059)
.
280
9.8.4
RPA
STRESS
RELAXATION
(ASTM
D6048)
.
281
9.8.5
SPECIAL
REFLECTIVE
MICROSCOPE
WITH
COMPUTER
ANALYSIS
(ASTM
D7723)
.
283
9.9
SCORCH
SAFETY
MEASUREMENTS
.
283
9.9.1
TRADITIONAL
MOONEY
SCORCH
.
284
9.9.2
TRADITIONAL
CUREMETER
SCORCH
MEASUREMENTS
.
285
9.9.3
DYNAMIC
PROPERTY
MEASUREMENTS
OF
SCORCH
.
285
9.9.4
LOWER
CURE
TEMPERATURE
EFFECTS
.
286
9.9.5
VARIABLE
TEMPERATURE
MEASUREMENTS
OF
SCORCH
.
286
9.9.6
OPTIMIZING
STRAIN
AND
FREQUENCY
EFFECTS
FOR
SCORCH
MEASUREMENTS
.
286
9.9.7
EFFECTS
OF
CONTROLLED
STRESS
MEASUREMENTS
ON
SCORCH
.
287
9.10
CURE
RATE
MEASUREMENTS
.
287
9.11
WORK
HISTORY
VS.
HEAT
HISTORY
.
289
9.12
STATE
OF
CURE
.
291
9.13
CAPILLARY
RHEOMETER
VISCOSITY
VS.
DYNAMIC
VISCOSITY
.
293
9.14
SELECTING
BEST
TEST
CONDITIONS
FOR
FACTORY
CONTROL
.
294
9.15
USING
SPC
CHARTS
OF
KEY
PARAMETERS
.
295
9.16
DOWNSTREAM
PROCESSABILITY
STAGES
.
296
9.16.1
CALENDERING
.
297
9.16.2
EXTRUSION
.
297
9.16.3
CURING
.
298
10
AFTER-CURE
DYNAMIC
PROPERTIES
.
303
10.1
COMPARISON
OF
AFTER-CURE
DYNAMIC
PROPERTIES
AND
PRODUCT
PERFORMANCE
.
304
10.1.1
TIRES
.
305
10.1.2
AUTOMOTIVE
ISOLATORS
AND
DAMPERS
.
310
10.1.3
SPORTS
APPLICATIONS
.
312
10.1.4
RUBBER
SEALS
AND
GASKETS
.
313
10.1.5
BLOWOUT
PREVENTER
.
313
10.1.6
CONVEYOR
BELTS,
TIMING
BELTS,
AND
POWER
BELTS
.
313
10.2
PAYNE
EFFECT
FOR
CURED
RUBBER
COMPOUNDS
.
314
10.3
MULLINS
EFFECT
FOR
CURED
RUBBER
COMPOUNDS
.
321
10.4
LOW
STRAIN
VS.
HIGH
STRAIN
MEASUREMENTS
OF
CURED
VULCANIZATES
.
324
10.5
ASTM
STANDARD
TEST
METHOD
USING
RPA
.
325
10.6
RELATION
OF
COMPRESSION
AND
EXTENSION
DYNAMIC
PROPERTIES
TO
SHEAR
MEASUREMENTS
.
330
11
METHODS
FOR
ANALYZING
THE
CURE
REACTION
.
337
11.1
REACTION
KINETICS
.
340
11.1.1
THE
REACTION
RATE
CONSTANT
.
340
11.1.2
ARRHENIUS
MODEL
.
344
11.1.3
ORDER
OF
REACTION
(N)
IN
CURE
KINETICS
.
349
11.2
APPLICATIONS
OF
THE
MAXIMUM
CURE
RATE
(MCR)
.
349
11.3
APPLICATIONS
FOR
THE
RPA
THERMAL
RAMP
.
351
11.4
CONCEPT
OF
CURE
EQUIVALENTS
.
354
11.5
DIRECT
MEASUREMENT
OF
COMPLEX
NON-ISOTHERMAL
CURES
.
357
INDEX
.
363 |
| adam_txt |
THE
AUTHORS
V
PREFACE
.
VII
1
OVERVIEW
OF
RUBBER
RHEOLOGY
AND
DYNAMIC
PROPERTY
TESTS
.
1
1.1
INTRODUCTION
TO
THE
UNIQUENESS
OF
RUBBER
RHEOLOGY
.
1
1.2
BASIC
TENSILE
TESTING
.
3
1.3
HARDNESS
TESTING
.
5
1.4
DENSITY
.
6
1.5
MOONEY
VISCOSITY
.
7
1.6
ODR
CUREMETER
.
10
1.7
CAPILLARY
RHEOMETER
.
12
1.8
MOVING
DIE
RHEOMETER
(MDR)
.
13
1.9
RUBBER
PROCESS
ANALYZER
(RPA)
.
15
1.10
DYNAMIC
MECHANICAL
ANALYZER
(DMA)
.
16
1.11
FLEX
FATIGUE
TESTERS
.
18
1.12
FLEXOMETER
DELTA
T
.
19
1.13
MEASURING
DISPERSION
.
20
1.14
OTHER
RELEVANT
RUBBER
TESTS
.
22
1.14.1
COMPRESSION
PLASTIMETERS
.
22
1.14.2
TEAR
PROPERTIES
.
23
1.14.3
ELECTRICAL
CONDUCTIVITY
PROPERTIES
.
24
1.14.4
DIFFERENTIAL
SCANNING
CALORIMETRY
(DSC)
.
24
1.14.5
THERMOGRAVIMETRIC
ANALYSIS
(TGA)
.
25
1.14.6
FOURIER
TRANSFORM
INFRARED
SPECTROSCOPY
(FTIR)
.
26
1.14.7
ATTENUATED
TOTAL
REFLECTANCE
(ATR)
.
28
1.14.8
GEL
PERMEATION
CHROMATOGRAPHY
(GPC)
.
28
1.14.9
NUCLEAR
MAGNETIC
RESONANCE
SPECTROSCOPY
(NMR)
.
28
1.14.10
BET
(BRUNAUER,
EMMETT,
AND
TELLER)
NITROGEN
ADSORPTION
SURFACE
AREA
APPARATUS
.
29
1.14.11
THERMAL
CONDUCTIVITY
METERS
.
29
2
MOONEY
VISCOMETER
.
35
2.1
DESCRIPTION
OF
THE
MOONEY
VISCOMETER
.
35
2.2
MOONEY
TESTS
.
37
2.3
MOONEY
VISCOSITY
.
37
2.4
MEASURING
MOONEY
SCORCH
.
42
2.5
MEASURING
MOONEY
STRESS
RELAXATION
.
46
2.6
DELTA
MOONEY
TEST
FOR
OIL
EXTENDED
EMULSION
SBR
.
48
2.7
VARIABLE
SPEED
MOONEY
.
49
2.8
LIMITATIONS
OF
THE
MOONEY
VISCOMETER
.
51
3
CAPILLARY
RHEOMETER
.
55
3.1
INTRODUCTION
.
55
3.2
BASIC
TYPES
OF
CAPILLARY
RHEOMETERS
.
57
3.3
MEASUREMENT
OF
VISCOSITY
WITH
A
CAPILLARY
RHEOMETER
.
58
3.4
TYPES
OF
CAPILLARY
RHEOMETER
TESTS
.
59
3.4.1
STABILITY
TEST
.
60
3.4.2
SHEAR
RATE
SWEEP
.
61
3.4.3
MEASURE
OF
TRUE
VISCOSITY
WITH
CAPILLARY
RHEOMETERS
BY
USING
CORRECTIONS
.
63
3.4.3.1
BAGLEY
CORRECTION
.
63
3.4.3.2
RABINOWITSCH
CORRECTION
.
64
3.4.4
CAPILLARY
RHEOMETER
WALL
SLIPPAGE
.
64
3.5
BEHAVIOR
OF
NON-NEWTONIAN
MATERIALS
.
65
3.6
APPEARANCE
OF
CAPILLARY
RHEOMETER
EXTRUDATE
.
69
3.7
CAPILLARY
RHEOMETRY
IN
FACTORY
PROBLEM
SOLVING
.
71
3.8
PREDICTION
OF
FACTORY
PROCESSABILITY
WITH
CAPILLARY
RHEOMETERS
.
72
3.9
LIMITATIONS
OF
CAPILLARY
RHEOMETERS
IN
RUBBER
TESTING
.
74
4
CUREMETERS
.
77
4.1
OSCILLATING
DISC
RHEOMETER
.
77
4.2
MOVING
DIE
RHEOMETER
.
79
4.3
ASTM
D2084
AND
D5289
DATA
POINTS
FOR
CUREMETERS
.
84
4.4
DYNAMIC
PROPERTIES
MEASURED
WITH
AN
MDR
.
87
4.5
ASTM
AND
ISO
STANDARDS
FOR
CUREMETERS
AND
THE
SELECTION
OF
TEST
CONDITIONS
.
92
4.6
THE
RPA
AS
A
CUREMETER
.
94
4.6.1
DESCRIPTION
OF
THE
RPA
AS
A
CUREMETER
.
94
4.6.2
USING
RPA
DYNAMIC
DATA
FOR
ANALYZING
CURE
CURVES
.
94
4.6.2.1
TMAXS
DURING
CURE
(TIME
TO
S"
PEAK)
.
94
4.6.2.2
S'
AND
S"
DUE
TO
CROSSLINK
DENSITY
.
96
4.6.2.3
S'
AND
S"
DUE
TO
FILLER
LOADING
.
97
4.6.3
EFFECT
OF
OIL
.
99
5
VISCOELASTIC
CHARACTERIZATION
OF
RUBBER
.
101
5.1
INTRODUCTION
TO
THE
VISCOELASTIC
PROPERTY
.
101
5.2
PURE
ELASTICITY
.
101
5.3
PURE
VISCOSITY
.
103
5.4
MODELING
VISCOSITY
.
106
5.5
VISCOELASTIC
PROPERTIES
.
107
5.6
MEASUREMENT
OF
VISCOELASTIC
PROPERTIES
WITH
SINUSOIDAL
DEFORMATION
.
110
5.7
APPLICATIONS
FOR
VISCOELASTIC
PROPERTIES
.
114
5.8
INSTRUMENTS
WITH
MULTIPLE
TEST
CAPABILITIES
.
114
5.9
RPA
TEST
CONDITIONS
.
123
5.10
THE
ADVANTAGES
OF
THE
RPA
OVER
SCIENTIFIC
DMAS
.
125
5.11
THE
BASICS
OF
MEASURING
AND
CALCULATING
DYNAMIC
MODULI
.
128
5.12
THE
BASICS
OF
MEASURING
AND
CALCULATING
DYNAMIC
VISCOSITY
.
132
5.13
COMPLIANCE
.
136
5.14
EXTENSION/COMPRESSION
MODULUS
AND
COMPLIANCE
.
137
5.15
SPRING
RATE
CONSTANTS
AND
DAMPING
COEFFICIENTS
.
140
5.16
TIME
TEMPERATURE
SUPERPOSITIONING
(TTS)
.
142
5.17
STATISTICAL
EVALUATION
OF
RHEOMETERS
.
145
6
TYPES
OF
RUBBER
RPA
RHEOLOGICAL
TESTS
.
151
6.1
SUMMARY
OF
RPA
RHEOLOGICAL
DATA
.
151
6.2
TYPES
OF
RPA
RHEOLOGICAL
SUBTESTS
.
152
6.2.1
TIMED
.
152
6.2.2
TEMPERATURE
SWEEP
.
154
6.2.3
VTA
(THERMAL
RAMP)
.
157
6.2.4
FREQUENCY
SWEEP
.
159
6.2.5
STRAIN
SWEEP:
LOW
.
161
6.2.6
STRAIN
SWEEP:
HIGH
.
163
6.2.7
MATRIX
.
165
6.2.8
LAOS
SWEEP
.
165
6.2.9
STRESS
RELAXATION
.
169
6.3
ASTM,
ISO,
AND
DIN
STANDARD
METHODS
FOR
RPA
TESTING
OF
ELASTOMERS
AND
COMPOUNDS
.
170
6.3.1
ASTM
D6204
PART
A
.
170
6.3.2
ASTM
D6204
PART
B
.
172
6.3.3
ASTM
D6204
PARTC
.
172
6.3.4
ASTM
D6204AB
FOR
R&D
.
174
6.3.5
ASTM
D6601
.
175
6.3.6
ASTMD8059
.
177
6.3.7
ASTMD6048
.
179
6.3.8
ASTM
D7050
.
181
6.3.9
ASTM
D7605
.
182
6.3.10
ASTM
D5289
.
184
6.3.11
DIN
53529
.
184
6.3.12
ISO
13145
.
185
6.4
NONSTANDARD
METHODS
FOR
RPA
TESTING
OF
ELASTOMERS
AND
COMPOUNDS
.
186
6.4.1
DISPERSION
USING
DYNAMIC
MECHANICAL
METHODS
.
186
6.4.2
MULTIPLE
FREQUENCY
SWEEPS
WITH INCREASING
STRAINS
.
187
6.4.3
MULTIPLE
IDENTICAL
STRAIN
SWEEPS
.
188
6.4.4
ANAEROBIC
HEAT
AGING
.
189
6.4.5
AEROBIC
HEAT
AGING
.
189
6.4.6
VISCOUS
HEATING
OF
UNCURED
RUBBER
COMPOUNDS
.
190
6.4.7
HEAT
BUILDUP
AT
FOR
CURED
RUBBER
COMPOUND
.
191
7
RAW
RUBBER
EFFECTS
ON
PROCESSABILITY
.
195
7.1
NATURAL
RUBBER
.
195
7.2
SYNTHETIC
RAW
RUBBER
.
201
7.2.1
AVERAGE
MOLECULAR
WEIGHT
.
203
7.2.2
MOLECULAR
WEIGHT
DISTRIBUTION
.
205
7.2.3
LONG
CHAIN
BRANCHING
.
207
7.2.4
GEL
.
209
7.2.5
CHANGES
IN
THE
CHEMICAL
COMPOSITION
.
210
7.2.6
STATISTICAL
CONFOUNDING
.
212
7.3
HIGH
STRAIN
TESTING
OF
SYNTHETIC
ELASTOMERS
.
213
7.4
MEASURING
IMPARTED
DIFFERENCES
IN
SHEAR
THINNING
PROPERTIES
.
214
7.5
STRESS
RELAXATION
OF
ELASTOMERS
AND
PROCESSABILITY
.
215
7.6
MASTER
CURVE
AND
GLASS
TRANSITION
TEMPERATURE
.
217
7.7
WLF
SHIFTS
FOR
RAW
ELASTOMERS
.
220
7.8
TESTING
LIQUID
ELASTOMERS
.
221
7.9
TESTING
THERMOPLASTIC
ELASTOMERS
(TPE)
.
223
7.10
PROCESSABILITY
DATA
ANALYSIS
.
224
8
FILLER
EFFECTS
ON
RUBBER
COMPOUND
PROCESSABILITY
.
229
8.1
FILLER
EFFECTS
ON
RUBBER
COMPOUND
PROPERTIES
.
229
8.2
CARBON
BLACK
EFFECTS
.
232
8.2.1
CARBON
BLACK
SURFACE
AREA
.
234
8.2.2
CORRELATION
WITH
CARBON
BLACK
STRUCTURE
.
240
8.2.3
CORRELATION
WITH
CARBON
BLACK
SURFACE
ACTIVITY
.
245
8.2.4
EFFECTS
OF
VARIATION
IN
LOADING
ON
UNCURED
VS.
CURED
DYNAMIC
PROPERTIES
.
246
8.3
OIL
EFFECTS
.
249
8.4
SILICA
EFFECTS
.
254
8.4.1
EFFECTS
OF
SILANIZATION
.
254
8.4.2
EFFECTS
OF
SILICA
SURFACE
AREA
.
256
8.4.3
EFFECTS
OF
SILICA
LOADING
.
257
8.4.4
RECOVERY
OF
THE
SILICA
NETWORK
AFTER
DESTRUCTION
.
258
8.4.5
SPECIAL
ROLE
OF
STRUCTURE
FOR
SILICA
.
259
8.5
EFFECTS
OF
FULLY
REINFORCING
FILLERS
ON
THE
COX-MERZ
CORRELATION
.
261
8.6
EFFECTS
OF
FILLER
TYPE
AND
CONCENTRATION
ON
SHEAR
THINNING
PROFILES
.
262
8.7
EFFECTS
OF
FILLER
ROOM
TEMPERATURE
STORAGE
ON
FORMATION
OF
BOUND
RUBBER
AND
RHEOLOGY
OF
FILLED
RUBBER
COMPOUNDS
.
263
9
MEASURING
QUALITY
OF
MIX
AND
PROCESSABILITY
.
267
9.1
DISPERSION
OF
FILLERS
DURING
MIXING
.
267
9.2
MASTICATION
OF
ELASTOMERS
DURING
MIXING
.
268
9.3
RHEOLOGICAL
CHANGES
DURING
MIXING
.
268
9.4
OPTIMAL
RHEOLOGICAL
CONDITIONS
FOR
MIX
QUALITY
MEASUREMENT
.
269
9.5
STATE
OF
MIX
AND
PERCENT
DISPERSION
.
271
9.6
EFFECT
OF
OIL
ON
RUBBER
MIXING
.
272
9.7
EFFECT
OF
PHASE
MIXING
.
275
9.8
SPECIAL
TEST
CONDITIONS
FOR
MEASURING
STATE
OF
MIX
.
277
9.8.1
MOONEY
VISCOSITY
.
ZT1
9.8.2
RPA
AT
100%
STRAIN
(ASTM
D6204
PART
B)
.
277
9.8.3
RPA
PAYNE
EFFECT
PLATEAU
(ASTM
D8059)
.
280
9.8.4
RPA
STRESS
RELAXATION
(ASTM
D6048)
.
281
9.8.5
SPECIAL
REFLECTIVE
MICROSCOPE
WITH
COMPUTER
ANALYSIS
(ASTM
D7723)
.
283
9.9
SCORCH
SAFETY
MEASUREMENTS
.
283
9.9.1
TRADITIONAL
MOONEY
SCORCH
.
284
9.9.2
TRADITIONAL
CUREMETER
SCORCH
MEASUREMENTS
.
285
9.9.3
DYNAMIC
PROPERTY
MEASUREMENTS
OF
SCORCH
.
285
9.9.4
LOWER
CURE
TEMPERATURE
EFFECTS
.
286
9.9.5
VARIABLE
TEMPERATURE
MEASUREMENTS
OF
SCORCH
.
286
9.9.6
OPTIMIZING
STRAIN
AND
FREQUENCY
EFFECTS
FOR
SCORCH
MEASUREMENTS
.
286
9.9.7
EFFECTS
OF
CONTROLLED
STRESS
MEASUREMENTS
ON
SCORCH
.
287
9.10
CURE
RATE
MEASUREMENTS
.
287
9.11
WORK
HISTORY
VS.
HEAT
HISTORY
.
289
9.12
STATE
OF
CURE
.
291
9.13
CAPILLARY
RHEOMETER
VISCOSITY
VS.
DYNAMIC
VISCOSITY
.
293
9.14
SELECTING
BEST
TEST
CONDITIONS
FOR
FACTORY
CONTROL
.
294
9.15
USING
SPC
CHARTS
OF
KEY
PARAMETERS
.
295
9.16
DOWNSTREAM
PROCESSABILITY
STAGES
.
296
9.16.1
CALENDERING
.
297
9.16.2
EXTRUSION
.
297
9.16.3
CURING
.
298
10
AFTER-CURE
DYNAMIC
PROPERTIES
.
303
10.1
COMPARISON
OF
AFTER-CURE
DYNAMIC
PROPERTIES
AND
PRODUCT
PERFORMANCE
.
304
10.1.1
TIRES
.
305
10.1.2
AUTOMOTIVE
ISOLATORS
AND
DAMPERS
.
310
10.1.3
SPORTS
APPLICATIONS
.
312
10.1.4
RUBBER
SEALS
AND
GASKETS
.
313
10.1.5
BLOWOUT
PREVENTER
.
313
10.1.6
CONVEYOR
BELTS,
TIMING
BELTS,
AND
POWER
BELTS
.
313
10.2
PAYNE
EFFECT
FOR
CURED
RUBBER
COMPOUNDS
.
314
10.3
MULLINS
EFFECT
FOR
CURED
RUBBER
COMPOUNDS
.
321
10.4
LOW
STRAIN
VS.
HIGH
STRAIN
MEASUREMENTS
OF
CURED
VULCANIZATES
.
324
10.5
ASTM
STANDARD
TEST
METHOD
USING
RPA
.
325
10.6
RELATION
OF
COMPRESSION
AND
EXTENSION
DYNAMIC
PROPERTIES
TO
SHEAR
MEASUREMENTS
.
330
11
METHODS
FOR
ANALYZING
THE
CURE
REACTION
.
337
11.1
REACTION
KINETICS
.
340
11.1.1
THE
REACTION
RATE
CONSTANT
.
340
11.1.2
ARRHENIUS
MODEL
.
344
11.1.3
ORDER
OF
REACTION
(N)
IN
CURE
KINETICS
.
349
11.2
APPLICATIONS
OF
THE
MAXIMUM
CURE
RATE
(MCR)
.
349
11.3
APPLICATIONS
FOR
THE
RPA
THERMAL
RAMP
.
351
11.4
CONCEPT
OF
CURE
EQUIVALENTS
.
354
11.5
DIRECT
MEASUREMENT
OF
COMPLEX
NON-ISOTHERMAL
CURES
.
357
INDEX
.
363 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Dick, John S. 1945- Pawlowski, Henry |
| author_GND | (DE-588)1145742114 |
| author_facet | Dick, John S. 1945- Pawlowski, Henry |
| author_role | aut aut |
| author_sort | Dick, John S. 1945- |
| author_variant | j s d js jsd h p hp |
| building | Verbundindex |
| bvnumber | BV046900152 |
| classification_rvk | ZM 5100 UV 9150 |
| ctrlnum | (OCoLC)1409132798 (DE-599)DNB1211017826 |
| discipline | Chemie / Pharmazie Physik Werkstoffwissenschaften / Fertigungstechnik |
| discipline_str_mv | Chemie / Pharmazie Werkstoffwissenschaften / Fertigungstechnik |
| format | Book |
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| id | DE-604.BV046900152 |
| illustrated | Illustrated |
| index_date | 2024-07-03T15:24:07Z |
| indexdate | 2024-07-20T05:42:19Z |
| institution | BVB |
| institution_GND | (DE-588)1064064051 |
| isbn | 9781569906170 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032309824 |
| oclc_num | 1409132798 |
| open_access_boolean | |
| owner | DE-29T DE-1050 DE-210 DE-91 DE-BY-TUM DE-12 DE-703 |
| owner_facet | DE-29T DE-1050 DE-210 DE-91 DE-BY-TUM DE-12 DE-703 |
| physical | XV, 368 Seiten Illustrationen, Diagramme 25 cm |
| publishDate | 2023 |
| publishDateSearch | 2023 |
| publishDateSort | 2023 |
| publisher | Hanser |
| record_format | marc |
| spelling | Dick, John S. 1945- Verfasser (DE-588)1145742114 aut Practical rubber rheology and dynamic properties John S. Dick, Henry Pawlowski Munich Hanser [2023] © 2023 XV, 368 Seiten Illustrationen, Diagramme 25 cm txt rdacontent n rdamedia nc rdacarrier Viskosimetrie (DE-588)4188415-2 gnd rswk-swf Kautschuk (DE-588)4030108-4 gnd rswk-swf Rheologie (DE-588)4049828-1 gnd rswk-swf Dynamisches Verhalten (DE-588)4140475-0 gnd rswk-swf Rheologische Eigenschaft (DE-588)4366895-1 gnd rswk-swf Kautschukindustrie (DE-588)4163517-6 gnd rswk-swf FBKTKAUT: Elastomere und Kautschuk PLAS2020 Rheologie (DE-588)4049828-1 s Kautschukindustrie (DE-588)4163517-6 s DE-604 Kautschuk (DE-588)4030108-4 s Rheologische Eigenschaft (DE-588)4366895-1 s Viskosimetrie (DE-588)4188415-2 s Dynamisches Verhalten (DE-588)4140475-0 s Pawlowski, Henry Verfasser aut Hanser Publications (DE-588)1064064051 pbl Erscheint auch als Online-Ausgabe 978-1-56990-618-7 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032309824&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Dick, John S. 1945- Pawlowski, Henry Practical rubber rheology and dynamic properties Viskosimetrie (DE-588)4188415-2 gnd Kautschuk (DE-588)4030108-4 gnd Rheologie (DE-588)4049828-1 gnd Dynamisches Verhalten (DE-588)4140475-0 gnd Rheologische Eigenschaft (DE-588)4366895-1 gnd Kautschukindustrie (DE-588)4163517-6 gnd |
| subject_GND | (DE-588)4188415-2 (DE-588)4030108-4 (DE-588)4049828-1 (DE-588)4140475-0 (DE-588)4366895-1 (DE-588)4163517-6 |
| title | Practical rubber rheology and dynamic properties |
| title_auth | Practical rubber rheology and dynamic properties |
| title_exact_search | Practical rubber rheology and dynamic properties |
| title_exact_search_txtP | Practical rubber rheology and dynamic properties |
| title_full | Practical rubber rheology and dynamic properties John S. Dick, Henry Pawlowski |
| title_fullStr | Practical rubber rheology and dynamic properties John S. Dick, Henry Pawlowski |
| title_full_unstemmed | Practical rubber rheology and dynamic properties John S. Dick, Henry Pawlowski |
| title_short | Practical rubber rheology and dynamic properties |
| title_sort | practical rubber rheology and dynamic properties |
| topic | Viskosimetrie (DE-588)4188415-2 gnd Kautschuk (DE-588)4030108-4 gnd Rheologie (DE-588)4049828-1 gnd Dynamisches Verhalten (DE-588)4140475-0 gnd Rheologische Eigenschaft (DE-588)4366895-1 gnd Kautschukindustrie (DE-588)4163517-6 gnd |
| topic_facet | Viskosimetrie Kautschuk Rheologie Dynamisches Verhalten Rheologische Eigenschaft Kautschukindustrie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032309824&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT dickjohns practicalrubberrheologyanddynamicproperties AT pawlowskihenry practicalrubberrheologyanddynamicproperties AT hanserpublications practicalrubberrheologyanddynamicproperties |