Holdings: Characterization of magnetic nanoparticles

Characterization of magnetic nanoparticles: standardizing the metrological size characterization of magnetic nanoparticles

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Bibliographic Details
Main Author:	Balceris, Christoph Erik (Author)
Format:	Thesis Book
Language:	English
Published:	Berlin Mensch und Buch Verlag 2019
Series:	Berichte aus dem Institut für Elektrische Messtechnik und Grundlagen der Elektrotechnik Band 64
Subjects:	Teilchengröße Magnetteilchen Eisenoxide Nanopartikel Messung Hochschulschrift
Online Access:	Inhaltsverzeichnis Inhaltsverzeichnis
Physical Description:	xv, 184 Seiten Illustrationen, Diagramme
ISBN:	9783863879655

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MARC


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adam_text	CONTENTS GLOSSARY VII SYMBOLS IX CONTENTS XIII 1 INTRODUCTION 1 2 MAGNETIC NANOPARTICLES 3 2.1 APPLICATIONS ........................................................................... 3 2.2 SYNTHESIS .............................................................................. 4 2.3 CLASSES OF MNP ..................................................................... 5 2.4 SIZE DEFINITIONS ..................................................................... 7 2.5 SIZE DISTRIBUTION .................................................................. 9 2.6 WEIGHTING .............................................................................. 11 2.7 SAMPLE PREPARATION ............................................................ 12 3 FUNDAMENTALS 15 3.1 FERRO-MAGNETISM .................................................................. 15 3.2 MAGNETIC DOMAINS ............................................................... 17 3.3 ANISOTROPY ENERGY ............................................................... 18 3.4 MAGNETIZATION OF SINGLE-DOMAIN PARTICLES ........................ 21 3.5 MAGNETIZATION OF AN ENSEMBLE ............................................. 23 3.6 SUSCEPTIBILITY ........................................................................ 24 3.7 RELAXATION MECHANISMS ...................................................... 25 3.8 AC SUSCEPTIBILITY .................................................................. 27 4 CHARACTERIZATION TECHNIQUES 29 4.1 AC SUSCEPTOMETRY ............................................................... 30 4.2 MAGNETORELAXOMETRY ............................................................ 39 4.3 ROTATING MAGNETIC FIELD METHOD ....................................... 41 4.4 DYNAMIC LIGHT SCATTERING ................................................... 43 4.5 TRANSMISSION ELECTRON MICROSCOPY .................................... 45 4.6 STATIC MAGNETIZATION ............................................................ 46 4.7 SMALL-ANGLE X-RAY SCATTERING ............................................. 47 4.8 ASYMMETRIC FLOW FIELD-FLOW FRACTIONATION ..................... 48 5 CHARACTERIZATION OF MAGNETIC NANOPARTICLES 49 5.1 SINGLE-CORE MNP ANALYSIS .................................................... 53 XIV CONTENTS 5.2 MULTI-CORE PARTICLE ANALYSIS ................................................ 66 5.3 NANOFLOWER PARTICLE ANALYSIS ............................................. 77 5.4 CLASSIFICATION OF MNP CLASSES BY MRX MEASUREMENTS ... 92 6 CHALLENGES OF MNP CHARACTERIZATION 99 6.1 IMMOBILIZATION STUDIES ......................................................... 99 6.2 FREEZE-DRYING WITH D-MANNITOL MATRIX .................................. 110 6.3 CONCENTRATION AND FIELD DEPENDENT AGGLOMERATION EFFECTS . 116 6.4 REPRODUCIBILITY OF ACS MEASUREMENT PROCEDURES ............ 120 7 CONCLUSION 125 A ACS SOP 129 A. L PURPOSE ................................................................................ 129 A. 2 PROCEDURE ............................................................................. 129 A. 3 SAMPLE PREPARATION .............................................................. 130 A. 4 MEASUREMENT PROCEDURE ..................................................... 131 A. 5 DATA ANALYSIS ....................................................................... 133 A. 6 UNCERTAINTY ........................................................................... 136 A. 7 SYSTEM QUALIFICATION .............................................................. 137 A. 8 HEALTH, SAFETY AND ENVIRONMENTAL CONSIDERATIONS .................. 138 A. 9 MEASUREMENT REPORT ........................................................... 138 B MRX SOP 141 B. L PURPOSE ................................................................................ 141 B. 2 PROCEDURE ............................................................................. 141 B. 3 MEASUREMENT PROCEDURE ..................................................... 143 B. 4 DATA ANALYSIS ....................................................................... 144 B. 5 UNCERTAINTY .......................................................................... 145 B. 6 SYSTEM QUALIFICATION ........................................................... 146 B. 7 HEALTH, SAFETY AND ENVIRONMENTAL CONSIDERATIONS .................. 146 B. 8 MEASUREMENT REPORT ........................................................... 146 C RMF SOP 151 C. L PURPOSE ................................................................................ 151 C. 2 PROCEDURE ............................................................................. 151 C. 3 SAMPLE PREPARATION .............................................................. 152 C. 4 MEASUREMENT PROCEDURE ..................................................... 153 C. 5 DATA ANALYSIS ....................................................................... 153 C. 6 UNCERTAINTY .......................................................................... 154 C. 7 SYSTEM QUALIFICATION ........................................................... 154 C. 8 HEALTH, SAFETY AND ENVIRONMENTAL CONSIDERATIONS .................. 154 C.9 MEASUREMENT REPORT ........................................................... 155 LIST OF FIGURES 159 LIST OF TABLES 165 REFERENCES 167 CONTENTS ACKNOWLEDGEMENTS XV 183
any_adam_object	1
author	Balceris, Christoph Erik
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author_sort	Balceris, Christoph Erik
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ctrlnum	(OCoLC)1137850442 (DE-599)DNB1192451171
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dewey-raw	620.50287
dewey-search	620.50287
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dewey-tens	620 - Engineering and allied operations
discipline	Maschinenbau / Maschinenwesen Werkstoffwissenschaften / Fertigungstechnik
format	Thesis Book
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spelling	Balceris, Christoph Erik Verfasser aut Characterization of magnetic nanoparticles standardizing the metrological size characterization of magnetic nanoparticles von Christoph Erik Balceris Berlin Mensch und Buch Verlag 2019 xv, 184 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Berichte aus dem Institut für Elektrische Messtechnik und Grundlagen der Elektrotechnik Band 64 Dissertation Technische Universität Carolo-Wilhelmina zu Braunschweig 2018 Teilchengröße (DE-588)4509483-4 gnd rswk-swf Magnetteilchen (DE-588)4406122-5 gnd rswk-swf Eisenoxide (DE-588)4151589-4 gnd rswk-swf Nanopartikel (DE-588)4333369-2 gnd rswk-swf Messung (DE-588)4038852-9 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Magnetteilchen (DE-588)4406122-5 s Eisenoxide (DE-588)4151589-4 s Nanopartikel (DE-588)4333369-2 s Teilchengröße (DE-588)4509483-4 s Messung (DE-588)4038852-9 s DE-604 Berichte aus dem Institut für Elektrische Messtechnik und Grundlagen der Elektrotechnik Band 64 (DE-604)BV012421175 64 B:DE-101 application/pdf https://d-nb.info/1192451171/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=031615740&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	Balceris, Christoph Erik Characterization of magnetic nanoparticles standardizing the metrological size characterization of magnetic nanoparticles Berichte aus dem Institut für Elektrische Messtechnik und Grundlagen der Elektrotechnik Teilchengröße (DE-588)4509483-4 gnd Magnetteilchen (DE-588)4406122-5 gnd Eisenoxide (DE-588)4151589-4 gnd Nanopartikel (DE-588)4333369-2 gnd Messung (DE-588)4038852-9 gnd
subject_GND	(DE-588)4509483-4 (DE-588)4406122-5 (DE-588)4151589-4 (DE-588)4333369-2 (DE-588)4038852-9 (DE-588)4113937-9
title	Characterization of magnetic nanoparticles standardizing the metrological size characterization of magnetic nanoparticles
title_auth	Characterization of magnetic nanoparticles standardizing the metrological size characterization of magnetic nanoparticles
title_exact_search	Characterization of magnetic nanoparticles standardizing the metrological size characterization of magnetic nanoparticles
title_full	Characterization of magnetic nanoparticles standardizing the metrological size characterization of magnetic nanoparticles von Christoph Erik Balceris
title_fullStr	Characterization of magnetic nanoparticles standardizing the metrological size characterization of magnetic nanoparticles von Christoph Erik Balceris
title_full_unstemmed	Characterization of magnetic nanoparticles standardizing the metrological size characterization of magnetic nanoparticles von Christoph Erik Balceris
title_short	Characterization of magnetic nanoparticles
title_sort	characterization of magnetic nanoparticles standardizing the metrological size characterization of magnetic nanoparticles
title_sub	standardizing the metrological size characterization of magnetic nanoparticles
topic	Teilchengröße (DE-588)4509483-4 gnd Magnetteilchen (DE-588)4406122-5 gnd Eisenoxide (DE-588)4151589-4 gnd Nanopartikel (DE-588)4333369-2 gnd Messung (DE-588)4038852-9 gnd
topic_facet	Teilchengröße Magnetteilchen Eisenoxide Nanopartikel Messung Hochschulschrift
url	https://d-nb.info/1192451171/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=031615740&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
volume_link	(DE-604)BV012421175
work_keys_str_mv	AT balcerischristopherik characterizationofmagneticnanoparticlesstandardizingthemetrologicalsizecharacterizationofmagneticnanoparticles

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