Atlas literarischer Orte: von Wunderland bis Mittelerde
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Weitere Verfasser: | , |
| Format: | Buch |
| Sprache: | German Spanish |
| Veröffentlicht: |
München
Knesebeck
[2019]
|
| Ausgabe: | Deutsche Erstausgabe |
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis Inhaltsverzeichnis |
| Beschreibung: | 128 Seiten Illustrationen 27 cm |
| ISBN: | 9783957282569 395728256X |
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Datensatz im Suchindex
| _version_ | 1804179472999514112 |
|---|---|
| adam_text | JUSTUS-LIEBIG-UNIVERSITAT GIEFIEN
INSTITUT FUR ANORGANISCHE UND
ANALYTISCHE CHEMIE
FACHBEREICH
BIOLOGIE UND
CHEMIE
SYNTHESIS, CHARACTERIZATION AND REACTIVITY
OF COPPER CLUSTER COMPLEXES
INAUGURAL-DISSERTATION ZUR ERLANGUNG DES
DOKTORGRADES DER NATURWISSENSCHAFTEN
VORGELEGT VON SABINE LOW AUS WETZLAR
HTTP://D-NB.INFO/1057851817
CONTENTS
1. INTRODUCTION 1
1.1. COPPER IN GENERAL 1
1.2. COPPER CHLORIDE IN INDUSTRIAL PROCESSES AND ORGANIC REACTIONS 2
1.2.1. COPPER CHLORIDE AS CHLORINATION REAGENT 3
1.2.2. COPPER CHLORIDE AS COUPLING REAGENT 3
1.2.3. COPPER CHLORIDE AS CATALYST IN OXIDATION REACTIONS . 4
1.3. COPPER CLUSTER COMPLEXES 7
1.4. RESEARCH GOALS 10
1.4.1. REACTIONS OF COPPER(LL) CHLORIDE WITH BENZYLAMINE 10
1.4.2. REACTIONS OF COPPER(II) CHLORIDE WITH DERIVATIVES OF
BENZYLAMINE AND ORGANIC SOLVENTS 11
1.4.3. REACTIONS OF COPPER(I) CHLORIDE-WITH BENZYLAMINE . . 11
2. REACTIONS OF COPPER(LL) CHLORIDE WITH BENZYLAMINE 15
2.1. REACTIONS OF COPPER(II) CHLORIDE IN SOLUTION: FACILE FORMA
TION OF TETRANUCLEAR COPPER CLUSTERS AND OTHER COMPLEXES
THAT ARE RELEVANT IN CATALYTIC REDOX PROCESSES 17
2.1.1. INTRODUCTION 18
2.1.2. RESULTS AND DISCUSSION 19
2.1.3. CONCLUSION 34
2.1.4. EXPERIMENTAL SECTION 35
2.1.5. ACKNOWLEDGEMENTS 39
2.2. SELECTED SUPPORTING INFORMATION AND UNPUBLISHED MATERIAL . 40
2.2.1. REACTIVITY OF CLUSTER I 40
2.2.2. CLUSTER I IN OXYGENATION REACTIONS 41
2.2.3. APPROACHES WITH ZNCB 47
2.2.4. MOLECULAR STRUCTURES OF THE SOLVENT CLUSTERS .... 49
3. REACTIONS OF COPPER(LL) CHLORIDE WITH DERIVATIVES OF BENZYLAMINE
AND ORGANIC SOLVENTS 51
3.1. INVESTIGATIONS CONCERNING [CU
4
OCL
6
L
4
]-CLUSTER FORMATION OF
CUCL
2
WITH AMINES AND IN ORGANIC SOLVENTS 53
3.1.1. INTRODUCTION 53
3.1.2. EXPERIMENTAL SECTION 55
I
3.1.3. RESULTS AND DISCUSSION 62
3.1.4. CONCLUSION 81
3.1.5. ACKNOWLEDGEMENTS 82
3.2. SELECTED SUPPORTING INFORMATION AND UNPUBLISHED MATERIAL . 83
3.2.1. INVESTIGATIONS CONCERNING THE CATALYTIC ACTIVITY OF
SOLVENT CLUSTERS 83
3.2.2. REACTIVITY OF CLUSTER I 84
3.2.3. ADDITIONAL MOLECULAR STRUCTURES 88
4. REACTIONS OF COPPER(L) CHLORIDE WITH BENZYLAMINE 91
4.1. SYNTHESIS. STRUCTURE AND REACTIVITY OF THE COMPOUND
[C
U
(C
7
H
7
NH
2
)C1]
4
93
4.1.1. INTRODUCTION 93
4.1.2. RESULTS AND DISCUSSION 94
4.1.3. CONCLUSION 103
4.1.4. EXPERIMENTAL SECTION 104
4.2. SELECTED SUPPORTING INFORMATION AND UNPUBLISHED MATERIAL . 106
5. MATERIALS, METHODS AND SPECTROSCOPY 109
5.1. MATERIALS AND METHODS 109
5.1.1. CHEMICALS AND SOLVENTS 109
5.1.2. AIR SENSITIVE COMPOUNDS 109
5.1.3. CRYSTALLOGRAPHY 109
5.1.4. INFRARED SPECTROSCOPY 110
5.1.5. ELEMENTAL ANALYSIS 110
5.1.6. GC-MS SPECTROMETRY 110
5.1.7. UV-VIS SPECTROSCOPY 110
5.2. CRYSTALLOGRAPHY ILL
5.2.1. CRYSTALLOGRAPHIC DATA FOR CHAPTER 2 ILL
5.2.2. CRYSTALLOGRAPHIC DATA FOR CHAPTER 3 147
5.2.3. CRYSTALLOGRAPHIC DATA FOR CHAPTER 4 187
5.3. INFRARED SPECTROSCOPY AND ELEMENTAL ANALYSES 196
5.3.1. DATA FOR CHAPTER 2 196
5.3.2. DATA FOR CHAPTER 3 209
5.3.3. DATA FOR CHAPTER 4 234
6. SUMMARY/ZUSAMMENFASSUNG 237
6.1. SUMMARY 237
6.1.1. REACTION OF COPPER(II) CHLORIDE WITH BENZYLAMINE, ITS
DERIVATIVES AND SOLVENT MOLECULES 238
6.1.2. REACTION OF COPPER(I) CHLORIDE WITH BENZYLAMINE . . . 244
6.2. ZUSAMMENFASSUNG 245
II
6.2.1. REAKTIONEN VON KUPFER(II)-CHLORID MIT BENZYLAMIN . 246
6.2.2. REAKTIONEN VON KUPFER(I)-CHLORID MIT BENZYLAMIN . . 252
7. LIST OF FIGURES 255
8. LIST OF TABLES 261
9. BIBLIOGRAPHY 265
A. PUBLICATIONS 275
B. CURRICULUM VITAE 277
III
|
| any_adam_object | 1 |
| author | Oliver, Cris F. |
| author2 | Krichtel, Janika Fuentes, Julio |
| author2_role | trl ill |
| author2_variant | j k jk j f jf |
| author_facet | Oliver, Cris F. Krichtel, Janika Fuentes, Julio |
| author_role | aut |
| author_sort | Oliver, Cris F. |
| author_variant | c f o cf cfo |
| building | Verbundindex |
| bvnumber | BV045521371 |
| classification_rvk | EC 5400 |
| ctrlnum | (OCoLC)1057851817 (DE-599)DNB1169234917 |
| dewey-full | 809.9332 |
| dewey-hundreds | 800 - Literature (Belles-lettres) and rhetoric |
| dewey-ones | 809 - History, description & criticism |
| dewey-raw | 809.9332 |
| dewey-search | 809.9332 |
| dewey-sort | 3809.9332 |
| dewey-tens | 800 - Literature (Belles-lettres) and rhetoric |
| discipline | Literaturwissenschaft |
| edition | Deutsche Erstausgabe |
| format | Book |
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| id | DE-604.BV045521371 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T08:20:25Z |
| institution | BVB |
| institution_GND | (DE-588)1065102941 |
| isbn | 9783957282569 395728256X |
| language | German Spanish |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-030905667 |
| oclc_num | 1057851817 |
| open_access_boolean | |
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| owner_facet | DE-12 DE-19 DE-BY-UBM DE-128 DE-127 DE-M336 DE-824 DE-54 |
| physical | 128 Seiten Illustrationen 27 cm |
| publishDate | 2019 |
| publishDateSearch | 2019 |
| publishDateSort | 2019 |
| publisher | Knesebeck |
| record_format | marc |
| spelling | Oliver, Cris F. Verfasser aut Atlas de los lugares literarios Atlas literarischer Orte von Wunderland bis Mittelerde Cris F. Oliver ; aus dem Spanischen von Janika Krichtel ; Illustrationen von Julio Fuentes Deutsche Erstausgabe München Knesebeck [2019] © 2019 128 Seiten Illustrationen 27 cm txt rdacontent sti rdacontent n rdamedia nc rdacarrier Imaginärer Schauplatz (DE-588)4161292-9 gnd rswk-swf Gotham Sherlock Holmes Der Zauberer von Oz Alice im Wunderland Oz Panem Orwell Schokoladenfabrik Camelot Romane Autorinnen Atlas Bibliophilie Literatur Autoren Anekdoten Geschichte Liliput Narnia Hogwarts magische Orte berühmte Orte Lieblingsbücher Karten Illustrationen Geschenkbuch Porträt Bestseller moderner Literatur Mittelerde Wunderland Literaturatlas Orte der Fantasie Design Geschenkbücher Imaginärer Schauplatz (DE-588)4161292-9 s DE-604 Krichtel, Janika trl Fuentes, Julio ill von dem Knesebeck GmbH & Co. Verlag KG (DE-588)1065102941 pbl X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=0a89597f611d4d37b8820cb446fdcee3&prov=M&dok_var=1&dok_ext=htm Inhaltstext B:DE-101 application/pdf http://d-nb.info/1169234917/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030905667&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Oliver, Cris F. Atlas literarischer Orte von Wunderland bis Mittelerde Imaginärer Schauplatz (DE-588)4161292-9 gnd |
| subject_GND | (DE-588)4161292-9 |
| title | Atlas literarischer Orte von Wunderland bis Mittelerde |
| title_alt | Atlas de los lugares literarios |
| title_auth | Atlas literarischer Orte von Wunderland bis Mittelerde |
| title_exact_search | Atlas literarischer Orte von Wunderland bis Mittelerde |
| title_full | Atlas literarischer Orte von Wunderland bis Mittelerde Cris F. Oliver ; aus dem Spanischen von Janika Krichtel ; Illustrationen von Julio Fuentes |
| title_fullStr | Atlas literarischer Orte von Wunderland bis Mittelerde Cris F. Oliver ; aus dem Spanischen von Janika Krichtel ; Illustrationen von Julio Fuentes |
| title_full_unstemmed | Atlas literarischer Orte von Wunderland bis Mittelerde Cris F. Oliver ; aus dem Spanischen von Janika Krichtel ; Illustrationen von Julio Fuentes |
| title_short | Atlas literarischer Orte |
| title_sort | atlas literarischer orte von wunderland bis mittelerde |
| title_sub | von Wunderland bis Mittelerde |
| topic | Imaginärer Schauplatz (DE-588)4161292-9 gnd |
| topic_facet | Imaginärer Schauplatz |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=0a89597f611d4d37b8820cb446fdcee3&prov=M&dok_var=1&dok_ext=htm http://d-nb.info/1169234917/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030905667&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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