Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Herzogenrath
Shaker
2019
|
| Ausgabe: | 1. Auflage |
| Schriftenreihe: | Schriftenreihe des IME
58 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 185 Seiten 12 Illustrationen 21 cm x 14.8 cm, 278 g |
| ISBN: | 9783844064223 3844064222 |
Internformat
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| 245 | 1 | 0 | |a Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide |c Rafael Bolívar León |
| 250 | |a 1. Auflage | ||
| 263 | |a 201901 | ||
| 264 | 1 | |a Herzogenrath |b Shaker |c 2019 | |
| 300 | |a 185 Seiten |b 12 Illustrationen |c 21 cm x 14.8 cm, 278 g | ||
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| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Schriftenreihe des IME |v 58 | |
| 502 | |b Dissertation |c RWTH Aachen University |d 2018 | ||
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| 653 | |a Magnesiothermic reduction | ||
| 653 | |a Titanium dioxide reduction | ||
| 653 | |a Titanium powder production | ||
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Datensatz im Suchindex
| _version_ | 1804179412635090944 |
|---|---|
| adam_text | TABLE OF CONTENT
1
INTRODUCTION...........................................................................1
2 TITANIUM, CONSUME AND PRICE
2.1 TITANIUM COMPONENTS COST....
2.2 TITANIUM ECONOMICS
...............
2.2.1 TITANIUM POWDER MARKET
.........
3 POWDER METALLURGY AND POWDER PRODUCTION OF
TITANIUM..............................................................................10
3.1 METHODS OF POWDER METALLURGY
.......................................
11
3.1.1 METAL POWDER INJECTION
MOLDING......................................11
3.1.2 NET SHAPE
TECHNIQUES....................................................12
3.2 VARIABLES IN POWDER METALLURGY
......................................
17
3.2.1 POWDER CHARACTERISTICS
....................................................
17
3.2.2 POWDER
CHEMISTRY............................................................ 19
3.3 TITANIUM POWDER
CLASSIFICATION......................................20
3.4 INDUSTRIAL POWDER PRODUCTION PROCESSES
......................
20
3.4.1 HISTORICAL
OVERVIEW...........................................................21
3.4.2 CHEMICAL REDUCTION
........................................................
22
3.4.3 PLASMA ROTATING ELECTRODE PROCESS (PREP)................24
3.4.4 HYDRIDING-DEHYDRIDING (HDH) PROCESS..........................26
3.4.5 ADMA PROCESS
.................................................................
28
3.4.6 ARMSTRONG
PROCESS/ITP...................................................29
3.5 PRE-COMMERCIAL POWDER PRODUCTION PROCESSES
..........
31
3.5.1 TIRO* PROCESS
.................................................................
31
3.5.2 MER
PROCESS....................................................................33
3.5.3 FCC
PROCESS.....................................................................34
3.5.4 EMR/MSE
PROCESS...........................................................35
3.5.5 PPR
PROCESS.....................................................................37
3.6 POWDER
PRODUCTION...........................................................37
3.7 COMPARISON OF POWDER PRODUCTION PROCESSES
...........
42
3.8 PROPOSED PROCESS FOR TI-POWDER PRODUCTION................44
4 PROCESS DEVELOPMENT
.....................................................
45
4.1 HISTORIC OVERVIEW OF MAGNESIOTHERMIC REDUCTION
.....
45
4.2 THERMOCHEMICAL BACKGROUND OF MAGNESIOTHERMIC
REDUCTION..........................................................................
48
4.2.1 MODELLING OF THE TERNARY DIAGRAM T I-M G -0
..................
49
4.2.2 REACTION
PROGRESS............................................................51
4.2.3 STABLE PHASES AFTER COOLING
...........................................
56
4.2.4 PROCESS TEMPERATURE
......................................................
59
CO CO 00
4.3 EXPERIMENTAL SET U P
..........................................................61
4.3.1 REACTOR
1.............................................................................61
4.3.2 REACTOR 11
...........................................................................
64
4.3.3 REACTOR III
..........................................................................
67
4.4 PRODUCTS
CHARACTERISATION................................................69
4.4.1 STRONGLY REDUCED PRODUCT
...............................................
70
4.4.2 WEAKLY REDUCED
PRODUCT................................................77
4.4.3 OTHER
PRODUCTS..................................................................78
4.4.4 DISTRIBUTION OF REACTION
PRODUCTS...................................80
5 IMPACT OF PARAMETER VARIATION ON MAGNESIOTHERMIC
REDUCTION
..........................................................................
86
5.1 INFLUENCE OF THE MOLAR COMPOSITION RATIO ((P)...............86
5.2 SET TEMPERATURE AND HOLDING REACTION TIME
..............
87
5.3 THE SHAPE OF MAGNESIUM USED FOR REDUCTION
............
88
5.4 PARTICLE SIZE AND FORM OF THE TITANIUM O XIDE
.............
90
6 THE MECHANISM-PATHWAY OF THE MAGNESIOTHERMIC
REDUCTION
..........................................................................
92
6.1 STARTING OF
REACTION..........................................................92
6.2 MAGNESIUM PARTIAL PRESSURE
...........................................
93
6.3 PHASE FORMATION
..............................................................
95
6.4 THE THERMOCHEMICAL STAIRCASE OF THE MAGNESIOTHERMIC
REDUCTION
..........................................................................
96
6.4.1 STAGE I: REDUCTION OF TIUE
2
TO TH03 AND MG2TI04
.........
98
6.4.2 STAGE II: REDUCTION FROM MG2TI04 TO TI[0]S
...................
98
6.4.3 REACTANTS IN CONTACT WITH EACH OTHER AND HIGH MOLAR
RATIO...................................................................................
99
6.4.4 REACTANTS IN CONTACT WITH EACH OTHER AND LOW MOLAR
RATIO.................................................................................
100
6.4.5 REACTANTS SEPARATE EACH
OTHER....................................101
6.5 REACTOR DESIGN, THE KEY TO A HIGH EFFICIENCY
REACTION...........................................................................101
6.5.1 EVAPORATION
SYSTEM........................................................103
6.5.2 REDUCTION ZONES
............................................................
103
6.5.3 COLLECTOR
VESSEL...............................................................103
7 LEACHING OF THE MAGNESIOTHERMIC REDUCTION
PRODUCTS...........................................................................105
7.1
EXPERIMENTAL....................................................................
105
7.2 RESULTS AND
ANALYSIS......................................................107
8 THE OBTAINED
POWDER.....................................................110
8.1 DEGREE OF
REDUCTION........................................................110
8.2 MORPHOLOGY OF POWDER FROM RL (ARGON PROTECTIVE
REACTOR)............................................................................110
8.3 MORPHOLOGY OF POWDER FROM RLL (SEALED REACTOR).... 111
8.4 MORPHOLOGY OF POWDER FROM RILL (TWO COMPARTMENT
REACTOR)............................................................................112
8.4.1 EQUIAXED
PARTICLES.......................................................... 112
8.4.2 SPHERICAL AND SEMI-SPHERICAL PARTICLES.......................113
8.4.3 CONTINUOUS MATRIX STRUCTURE
.........................................
114
8.5 MORPHOLOGY CONCLUSIONS
...............................................
115
8.5.1 REACTION STEPS OF MAGNESIOTHERMIC REACTION............116
9 CONCLUSIONS AND OUTLOOK...............................................
118
10 BIBLIOGRAPHY AND WEBOGRAPHY
.....................................
122
11
ANNEXES...........................................................................131
11.1 SIZE DISTRIBUTION OF THE UE O
2
PIGMENT
..........................
131
11.2 DRAWING OF
REACTORS........................................................132
11.2.1 DRAWING OF REACTOR
II......................................................132
11.2.2 DRAWING OF REACTOR
III......................................................134
11.3 EXPERIMENTAL PLANNING AND RESULTS FOR REACTOR I
.......
139
11.3.1 FIRST EXPERIMENTAL SERIES RL (ARGON PROTECTIVE
REACTOR)............................................................................139
11.3.2 SECOND EXPERIMENTAL SERIES RL
.....................................
139
11.3.3 THIRD EXPERIMENTAL SERIES RL
........................................
141
11.4 EXPERIMENTAL AND RESULTS REACTOR LL(SEALED
REACTOR)............................................................................141
11.4.1 FIRST EXPERIMENTAL SERIES R LL
........................................
141
11.4.2 SECOND EXPERIMENTAL SERIES
RLL....................................142
11.5 EXPERIMENTAL PLANNING AND RESULTS FOR REACTOR III (TWO
COMPARTMENT REACTOR)
..................................................
143
11.5.1 FIRST EXPERIMENTAL SERIES R ILL
........................................
143
11.5.2 SECOND EXPERIMENTAL SERIES
RILL...................................144
11.5.3 THIRD EXPERIMENTAL SERIES RILL
......................................
144
11.5.4 LEACHING OF THE WEAKLY REDUCED PRODUCT
..................
145
11.5.5 MORPHOLOGY OF WEAKLY REDUCED PRODUCT FROM RLLL-
NI4.....................................................................................147
|
| any_adam_object | 1 |
| author | Bolívar León, Rafael |
| author_GND | (DE-588)1176668676 |
| author_facet | Bolívar León, Rafael |
| author_role | aut |
| author_sort | Bolívar León, Rafael |
| author_variant | l r b lr lrb |
| building | Verbundindex |
| bvnumber | BV045488783 |
| ctrlnum | (DE-599)DNB1173519165 |
| edition | 1. Auflage |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV045488783 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T08:19:27Z |
| institution | BVB |
| institution_GND | (DE-588)1064118135 |
| isbn | 9783844064223 3844064222 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-030873699 |
| open_access_boolean | |
| owner | DE-83 |
| owner_facet | DE-83 |
| physical | 185 Seiten 12 Illustrationen 21 cm x 14.8 cm, 278 g |
| publishDate | 2019 |
| publishDateSearch | 2019 |
| publishDateSort | 2019 |
| publisher | Shaker |
| record_format | marc |
| series | Schriftenreihe des IME |
| series2 | Schriftenreihe des IME |
| spelling | Bolívar León, Rafael Verfasser (DE-588)1176668676 aut Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide Rafael Bolívar León 1. Auflage 201901 Herzogenrath Shaker 2019 185 Seiten 12 Illustrationen 21 cm x 14.8 cm, 278 g txt rdacontent n rdamedia nc rdacarrier Schriftenreihe des IME 58 Dissertation RWTH Aachen University 2018 Reduktion Chemie (DE-588)4277879-7 gnd rswk-swf Reaktionstechnik (DE-588)4136173-8 gnd rswk-swf Reinigungsverfahren (DE-588)4391913-3 gnd rswk-swf Titandioxid (DE-588)4185549-8 gnd rswk-swf Pulverherstellung (DE-588)4228872-1 gnd rswk-swf Prozessentwicklung Technik (DE-588)4278925-4 gnd rswk-swf Titan (DE-588)4140648-5 gnd rswk-swf Magnesium (DE-588)4128915-8 gnd rswk-swf Reduktionsmittel (DE-588)4177311-1 gnd rswk-swf Magnesiothermic reduction Titanium dioxide reduction Titanium powder production (DE-588)4113937-9 Hochschulschrift gnd-content Titan (DE-588)4140648-5 s Pulverherstellung (DE-588)4228872-1 s Titandioxid (DE-588)4185549-8 s Reduktion Chemie (DE-588)4277879-7 s Magnesium (DE-588)4128915-8 s Reduktionsmittel (DE-588)4177311-1 s Prozessentwicklung Technik (DE-588)4278925-4 s Reaktionstechnik (DE-588)4136173-8 s Reinigungsverfahren (DE-588)4391913-3 s DE-604 Shaker Verlag (DE-588)1064118135 pbl Schriftenreihe des IME 58 (DE-604)BV016981907 58 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030873699&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Bolívar León, Rafael Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide Schriftenreihe des IME Reduktion Chemie (DE-588)4277879-7 gnd Reaktionstechnik (DE-588)4136173-8 gnd Reinigungsverfahren (DE-588)4391913-3 gnd Titandioxid (DE-588)4185549-8 gnd Pulverherstellung (DE-588)4228872-1 gnd Prozessentwicklung Technik (DE-588)4278925-4 gnd Titan (DE-588)4140648-5 gnd Magnesium (DE-588)4128915-8 gnd Reduktionsmittel (DE-588)4177311-1 gnd |
| subject_GND | (DE-588)4277879-7 (DE-588)4136173-8 (DE-588)4391913-3 (DE-588)4185549-8 (DE-588)4228872-1 (DE-588)4278925-4 (DE-588)4140648-5 (DE-588)4128915-8 (DE-588)4177311-1 (DE-588)4113937-9 |
| title | Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide |
| title_auth | Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide |
| title_exact_search | Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide |
| title_full | Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide Rafael Bolívar León |
| title_fullStr | Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide Rafael Bolívar León |
| title_full_unstemmed | Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide Rafael Bolívar León |
| title_short | Synthesis of titanium powder by magnesiothermic reduction from titanium dioxide |
| title_sort | synthesis of titanium powder by magnesiothermic reduction from titanium dioxide |
| topic | Reduktion Chemie (DE-588)4277879-7 gnd Reaktionstechnik (DE-588)4136173-8 gnd Reinigungsverfahren (DE-588)4391913-3 gnd Titandioxid (DE-588)4185549-8 gnd Pulverherstellung (DE-588)4228872-1 gnd Prozessentwicklung Technik (DE-588)4278925-4 gnd Titan (DE-588)4140648-5 gnd Magnesium (DE-588)4128915-8 gnd Reduktionsmittel (DE-588)4177311-1 gnd |
| topic_facet | Reduktion Chemie Reaktionstechnik Reinigungsverfahren Titandioxid Pulverherstellung Prozessentwicklung Technik Titan Magnesium Reduktionsmittel Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030873699&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV016981907 |
| work_keys_str_mv | AT bolivarleonrafael synthesisoftitaniumpowderbymagnesiothermicreductionfromtitaniumdioxide AT shakerverlag synthesisoftitaniumpowderbymagnesiothermicreductionfromtitaniumdioxide |