Basic principles of formulation types:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin
De Gruyter
[2018]
|
| Schriftenreihe: | Formulation science and technology / Tharwat F. Tadros
volume 2 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis http://www.degruyter.com/search?f_0=isbnissn&q_0=9783110587487&searchTitles=true Inhaltsverzeichnis |
| Beschreibung: | xv, 308 Seiten Illustrationen 25 cm, 728 g |
| ISBN: | 9783110587487 3110587483 |
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Datensatz im Suchindex
| _version_ | 1804178770375999488 |
|---|---|
| adam_text | CONTENTS
PREFACE
1
1.1
1.2
1
.
2.1
1
.
2.2
1.2.3
1.2.4
1.2.5
1.3
1.3.1
1.3.2
1.3.3
1.3.4
1.4
1.5
2
2.1
2.2
2.3
2.4
2.5
2.6
2.7
2.8
2.9
2.10
2.11
3
3.1
3.2
3.3
FORMULATION OF SOLID/LIQUID DISPERSIONS (SUSPENSIONS) * 1
INTRODUCTION * 1
PREPARATION OF SUSPENSION CONCENTRATES BY THE BOTTOM-UP PROCESS *
NUCLEATION AND GROWTH * 10
PRECIPITATION KINETICS * 13
SEEDED NUCLEATION AND GROWTH * 17
SURFACE MODIFICATION * 18
OTHER METHODS FOR PREPARATION OF SUSPENSIONS
BY THE BOTTOM-UP PROCESS * 19
PREPARATION OF SUSPENSIONS USING THE TOP-DOWN PROCESS
----
21
WETTING OF THE BULK POWDER * 22
BREAKING OF AGGREGATES AND AGGLOMERATES INTO INDIVIDUAL UNITS * 26
WET MILLING OR COMMINUTION
----
32
STABILIZATION OF THE SUSPENSION DURING DISPERSION AND MILLING
AND THE RESULTING SUSPENSION * 37
PREVENTION OF OSTWALD RIPENING (CRYSTAL GROWTH) * 41
SEDIMENTATION OF SUSPENSIONS AND PREVENTION OF FORMATION
OF HARD SEDIMENTS * 46
FORMULATION OF LIQUID/LIQUID DISPERSIONS (EMULSIONS)
* 53
INTRODUCTION
----
53
THERMODYNAMICS OF EMULSION FORMATION AND BREAKDOWN
----
57
INTERACTION FORCES BETWEEN EMULSION DROPLETS AND FACTORS
AFFECTING THEIR STABILITY * 60
MECHANISM OF EMULSIFICATION AND THE ROLE OF THE EMULSIFIER
----
62
METHODS OF EMULSIFICATION * 70
SELECTION OF EMULSIFIERS * 79
DREAMING/SEDIMENTATION OF EMULSIONS AND ITS PREVENTION
----
87
FLOCCULATION OF EMULSIONS
----
92
OSTWALD RIPENING IN EMULSIONS AND ITS PREVENTION * 101
EMULSION COALESCENCE AND ITS PREVENTION * 106
PHASE INVERSION AND ITS PREVENTION * 111
FORMULATION OF FOAMS
* 115
INTRODUCTION
----
115
FOAM PREPARATION * 116
FOAM STRUCTURE * 117
3.4 CLASSIFICATION OF FOAM STABILITY * 118
3.5 DRAINAGE AND THINNING OF FOAM FILMS * 119
3.6 THEORIES OF FOAM STABILITY * 122
3.6.1 SURFACE VISCOSITY AND ELASTICITY THEORY * 122
3.6.2 THE GIBBS-MARANGONI EFFECT THEORY * 123
3.6.3 SURFACE FORCES THEORY (DISJOINING PRESSURE ZR) * 124
3.6.4 STABILIZATION BY MICELLES (HIGH SURFACTANT CONCENTRATIONS CMC) *
127
3.6.5 STABILIZATION BY LAMELLAR LIQUID CRYSTALLINE PHASES * 127
3.6.6 STABILIZATION OF FOAM FILMS BY MIXED SURFACTANTS * 127
3.7 FOAM INHIBITORS * 127
3.7.1 CHEMICAL INHIBITORS THAT LOWER VISCOSITY AND INCREASE DRAINAGE *
128
3.7.2 SOLUBILIZED CHEMICALS WHICH CAUSE ANTIFOAMING * 128
3.7.3 DROPLETS AND OIL LENSES WHICH CAUSE ANTIFOAMING AND DEFOAMING *
128
3.7.4 SURFACE TENSION GRADIENTS (INDUCED BY ANTIFOAMERS) * 130
3.7.5 HYDROPHOBIC PARTICLES AS ANTIFOAMERS * 130
3.7.6 MIXTURES OF HYDROPHOBIC PARTICLES AND OILS AS ANTIFOAMERS * 131
3.8 PHYSICAL PROPERTIES OF FOAMS * 131
3.8.1 MECHANICAL PROPERTIES * 131
3.8.2 RHEOLOGICAL PROPERTIES * 132
3.8.3 ELECTRICAL PROPERTIES * 133
3.8.4 ELECTROKINETIC PROPERTIES * 133
3.8.5 OPTICAL PROPERTIES * 133
3.9 EXPERIMENTAL TECHNIQUES FOR STUDYING FOAMS * 134
3.9.1 TECHNIQUES FOR STUDYING FOAM FILMS * 134
3.9.2 TECHNIQUES FOR STUDYING STRUCTURAL PARAMETERS OF FOAMS * 135
3.9.3 MEASURING FOAM DRAINAGE * 135
3.9.4 MEASURING FOAM COLLAPSE * 136
4 FORMULATION OF GELS * 139
4.1 INTRODUCTION * 139
4.2 CLASSIFICATION OF GELS * 139
4.3 GEL-FORMING MATERIALS * 140
4.4 RHEOLOGICAL BEHAVIOUR OF A GEL
----
141
4.4.1 STRESS RELAXATION (AFTER SUDDEN APPLICATION OF STRAIN) * 141
4.4.2 CONSTANT STRESS (CREEP) MEASUREMENTS * 143
4.4.3 DYNAMIC (OSCILLATORY) MEASUREMENTS * 143
4.5 POLYMER GELS * 145
4.5.1 PHYSICAL GELS OBTAINED BY CHAIN OVERLAP * 145
4.5.2 GELS PRODUCED BY ASSOCIATIVE THICKENERS * 146
4.5.3 CROSS LINKED GELS (CHEMICAL GELS) * 150
4.6 PARTICULATE GELS * 150
4.6.1 AQUEOUS CLAY GELS * 151
4.6.2
4.6.3
4.7
4.8
5
5.1
5.2
5.3
5.4
5.5
6
6.1
6.2
6.3
6.3.1
6.3.2
6.4
6.4.1
6.4.2
6.5
6.6
6
.
6.1
6
.
6.2
6.6.3
6.6.4
6.6.5
6.7
6.8
6.9
7
7.1
7.2
7.3
7.4
7.5
ORGANO-CLAYS (BENTONES) * 154
OXIDE GELS * 154
GELS PRODUCED BY MIXTURES OF POLYMERS AND FINELY DIVIDED
PARTICULATE SOLIDS * 155
GELS BASED ON SURFACTANT SYSTEMS * 156
FORMULATION OF POLYMER COLLOIDS (LATEXES)
* 161
INTRODUCTION * 161
EMULSION POLYMERIZATION * 161
POLYMERIC SURFACTANTS FOR STABILIZING
PREFORMED LATEX DISPERSIONS * 172
DISPERSION POLYMERIZATION * 176
PARTICLE FORMATION IN POLAR MEDIA * 180
FORMULATION OF MICROEMULSIONS
* 183
INTRODUCTION * 183
THERMODYNAMIC DEFINITION OF MICROEMULSIONS * 184
MIXED FILM AND SOLUBILIZATION THEORIES OF MICROEMULSIONS * 185
MIXED FILM THEORIES * 185
SOLUBILIZATION THEORIES * 187
THERMODYNAMIC THEORY OF MICROEMULSION FORMATION * 189
REASON FOR COMBINING TWO SURFACTANTS * 189
FREE ENERGY OF FORMATION OF MICROEMULSIONS * 190
FACTORS DETERMINING W/O VERSUS O/W MICROEMULSIONS * 192
CHARACTERIZATION OF MICROEMULSIONS USING SCATTERING TECHNIQUES * 194
TIME-AVERAGE (STATIC) LIGHT SCATTERING * 195
CALCULATION OF DROPLET SIZE FROM INTERFACIAL AREA * 197
DYNAMIC LIGHT SCATTERING (PHOTON CORRELATION SPECTROSCOPY, PCS) * 198
NEUTRON SCATTERING * 199
CONTRAST MATCHING FOR DETERMINING THE STRUCTURE
OF MICROEMULSIONS * 200
CHARACTERIZATION OF MICROEMULSIONS USING CONDUCTIVITY * 200
NMR MEASUREMENTS * 203
FORMULATION OF MICROEMULSIONS * 204
CONTROLLED-RELEASE FORMULATIONS
* 207
INTRODUCTION * 207
MICROENCAPSULATION * 207
MECHANISM OF RELEASE OF ACTIVE INGREDIENT FROM MICROCAPSULES * 209
ENCAPSULATION BY PHASE SEPARATION FROM AQUEOUS SOLUTION * 209
MICROENCAPSULATION OF SOLID PARTICLES * 210
7.6 CONTROLLED-RELEASE OF AGROCHEMICALS
FROM MATRIX-BASED MICROPARTICLES * 211
7.7 MECHANISM OF CONTROLLED-RELEASE FROM MICROPARTICLES * 212
7.8 CONTROLLED RELEASE FROM GRANULES * 214
8 SOLID DOSAGE FORMULATIONS * 219
8.1 INTRODUCTION * 219
8.2 AGGLOMERATION * 219
8.3 TYPES OF GRANULATORS
----
223
8.4 COMPACTION OF SOLIDS * 227
8.5 SOLID DOSAGE FORMULATIONS IN THE PHARMACEUTICAL INDUSTRY * 229
8.5.1 FORMULATION OF TABLETS * 229
8.5.2 TABLET DISINTEGRATION * 236
8.5.3 DRUG DISSOLUTION RATES FROM TABLETS * 239
8.5.4 EFFECT OF POROSITY ON RELEASE RATES * 240
8.5.5 TABLET COATING
----
241
8.6 HARD AND SOFT-SHELL GELATIN CAPSULES * 242
8.7 SUSTAINED-RELEASE PELLETS * 244
9 ASSESSMENTS OF THE STABILITY OF FORMULATIONS * 249
9.1 INTRODUCTION
----
249
9.2 MEASURING PARTICLE AND DROPLET SIZE DISTRIBUTIONS * 249
9.2.1 OPTICAL MICROSCOPY * 250
9.2.2 ELECTRON MICROSCOPY
----
252
9.2.3 CONFOCAL LASER SCANNING MICROSCOPY (CLSM) * 253
9.2.4 SCANNING PROBE MICROSCOPY (SPM) * 254
9.2.5 SCANNING TUNNELLING MICROSCOPY (STM) * 254
9.2.6 ATOMIC FORCE MICROSCOPY (AFM)
----
255
9.3 SCATTERING TECHNIQUES * 255
9.3.1 LIGHT SCATTERING TECHNIQUES * 255
9.3.2 TURBIDITY MEASUREMENTS * 257
9.3.3 LIGHT DIFFRACTION TECHNIQUES * 257
9.3.4 DYNAMIC LIGHT SCATTERING - PHOTON CORRELATION SPECTROSCOPY
(PCS)
----
259
9.3.5 BACKSCATTERING TECHNIQUES * 262
9.4 ELECTROKINETIC AND ZETA POTENTIAL MEASUREMENTS * 263
9.5 MEASURING THE RATE OF FLOCCULATION * 269
9.6 MEASURING INCIPIENT FLOCCULATION * 270
9.7 MEASURING OSTWALD RIPENING * 271
9.8 MEASURING THE RATE OF COALESCENCE FOR EMULSIONS * 271
9.9 ASSESSING SEDIMENTATION OR CREAMING OF DISPERSIONS
----
272
9.10 BULK PROPERTIES OF SUSPENSIONS AND EMULSIONS. EQUILIBRIUM SEDIMENT
VOLUME (OR HEIGHT) AND REDISPERSION * 278
9.11 METHODS FOR EVALUATING FORMULATIONS WITHOUT DILUTION -
RHEOLOGICAL TECHNIQUES * 279
9.12 APPLICATION OF RHEOLOGICAL TECHNIQUES FOR THE ASSESSMENT AND
PREDICTION
OF THE PHYSICAL STABILITY OF SUSPENSIONS
----
279
9.12.1 RHEOLOGICAL TECHNIQUES FOR ASSESSING SEDIMENTATION OR CREAMING
AND SYNERESIS * 279
9.12.2 ASSESSING FLOCCULATION USING RHEOLOGICAL TECHNIQUES * 281
9.13 PREDICTING CREAMING, SEDIMENTATION, FLOCCULATION AND COALESCENCE
OF FORMULATIONS
----
285
9.13.1 PREDICTING CREAMING AND SEDIMENTATION - ACCELERATED TESTS
AND THEIR LIMITATIONS
----
285
9.13.2 RHEOLOGICAL TECHNIQUES FOR PREDICTING SEDIMENTATION OR CREAMING
AND SYNERESIS * 286
9.13.3 EXAMPLES OF CORRELATION OF SEDIMENTATION OR CREAMING
WITH RESIDUAL (ZERO SHEAR) VISCOSITY * 288
9.13.4 EXAMPLES OF APPLICATIONS OF RHEOLOGY FOR PREDICTING FLOCCULATION
----
297
9.13.5 PREDICTING EMULSION COALESCENCE USING RHEOLOGICAL TECHNIQUES
----
300
INDEX
----
307
|
| any_adam_object | 1 |
| author | Tadros, Tharwat F. 1937-2018 |
| author_GND | (DE-588)129740837 |
| author_facet | Tadros, Tharwat F. 1937-2018 |
| author_role | aut |
| author_sort | Tadros, Tharwat F. 1937-2018 |
| author_variant | t f t tf tft |
| building | Verbundindex |
| bvnumber | BV045120493 |
| ctrlnum | (OCoLC)1048436523 (DE-599)DNB1148966862 |
| dewey-full | 660 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660 |
| dewey-search | 660 |
| dewey-sort | 3660 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| format | Book |
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| illustrated | Illustrated |
| indexdate | 2024-07-10T08:09:15Z |
| institution | BVB |
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| isbn | 9783110587487 3110587483 |
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| physical | xv, 308 Seiten Illustrationen 25 cm, 728 g |
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| publisher | De Gruyter |
| record_format | marc |
| series2 | Formulation science and technology / Tharwat F. Tadros |
| spelling | Tadros, Tharwat F. 1937-2018 Verfasser (DE-588)129740837 aut Basic principles of formulation types Tharwat F. Tadros Berlin De Gruyter [2018] xv, 308 Seiten Illustrationen 25 cm, 728 g txt rdacontent n rdamedia nc rdacarrier Formulation science and technology / Tharwat F. Tadros volume 2 Formulierung Technische Chemie (DE-588)4246877-2 gnd rswk-swf Formulierung Technische Chemie (DE-588)4246877-2 s DE-604 Walter de Gruyter GmbH & Co. KG (DE-588)10095502-2 pbl Erscheint auch als 9783110587975 Erscheint auch als Online-Ausgabe 9783110587968 Erscheint auch als Online-Ausgabe 9783110587579 Erscheint auch als Online-Ausgabe Tadros, Tharwat F., 1937- Basic Principles of Formulation Types Berlin/Boston : De Gruyter, 2018 Online-Ressource, 317 Seiten Tharwat F. Tadros Formulation science and technology volume 2 (DE-604)BV045083254 2 B:DE-101 application/pdf http://d-nb.info/1148966862/04 Inhaltsverzeichnis X:MVB http://www.degruyter.com/search?f_0=isbnissn&q_0=9783110587487&searchTitles=true DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030510641&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Tadros, Tharwat F. 1937-2018 Basic principles of formulation types Formulierung Technische Chemie (DE-588)4246877-2 gnd |
| subject_GND | (DE-588)4246877-2 |
| title | Basic principles of formulation types |
| title_auth | Basic principles of formulation types |
| title_exact_search | Basic principles of formulation types |
| title_full | Basic principles of formulation types Tharwat F. Tadros |
| title_fullStr | Basic principles of formulation types Tharwat F. Tadros |
| title_full_unstemmed | Basic principles of formulation types Tharwat F. Tadros |
| title_short | Basic principles of formulation types |
| title_sort | basic principles of formulation types |
| topic | Formulierung Technische Chemie (DE-588)4246877-2 gnd |
| topic_facet | Formulierung Technische Chemie |
| url | http://d-nb.info/1148966862/04 http://www.degruyter.com/search?f_0=isbnissn&q_0=9783110587487&searchTitles=true http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030510641&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV045083254 |
| work_keys_str_mv | AT tadrostharwatf basicprinciplesofformulationtypes AT walterdegruytergmbhcokg basicprinciplesofformulationtypes |
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