Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement: implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Erlangen ; Nürnberg
Friedrich-Alexander-Universität Erlangen-Nürnberg
2018
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Beschreibung: | ix, 133 Seiten Illustrationen, Diagramme 21 cm |
Internformat
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| 100 | 1 | |a Stabler, Christopher |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement |b implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten |c vorgelegt von Christopher Stabler |
| 246 | 1 | 1 | |a Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement |
| 264 | 1 | |a Erlangen ; Nürnberg |b Friedrich-Alexander-Universität Erlangen-Nürnberg |c 2018 | |
| 300 | |a ix, 133 Seiten |b Illustrationen, Diagramme |c 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c Friedrich-Alexander-Universität Erlangen-Nürnberg |d 2018 | ||
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Datensatz im Suchindex
| _version_ | 1804178714393575424 |
|---|---|
| adam_text | CONTENT
ACKNOWLEDGEMENTS...........................................................................................................................I
NOMENCLATURE AND
ABBREVIATIONS....................................................................................................
II
ABSTRACT.............................................................................................................................................IV
ZUSAMMENFASSUNG............................................................................................................................V
C
ONTENT...........................................................................................................................................
VII
1
INTRODUCTION......................................................................................................................1
2 STATE OF
KNOWLEDGE.........................................................................................................3
2.1 EARLY HYDRATION OF
OPC..................................................................................................
3
2.2 SULFATES IN O P C
...............................................................................................................
6
2.3 RETARDERS FOR O P C
...........................................................................................................
8
2.4 FRUIT
ACIDS.........................................................................................................................9
2.5 FRUIT ACIDS AS
RETARDERS...................................................................................................10
2.6 STRUCTURAL RELATIVES OF THE FRUIT ACID
S.............................................................................
12
2.7 DISSOCIATION CONSTANTS OF THE FRUIT ACIDS AND THEIR STRUCTURAL
RELATIVES........................15
3 MATERIALS AND
METHODS...................................................................................................17
3.1 CEMENTS AND
ADDITIVES....................................................................................................
17
3.2 X- RAY
DIFFRACTION.............................................................................................................17
3.2.1 PHASE ANALYSIS AND REFINEMENT OF THE DRY SAM PLES
...............................................
18
3.2.2 QUANTITATIVE REFINEMENT OF THE HYDRATING SAMPLES
................................................
19
3.2.3 REVERSE VOGUE
CALCULATION.....................................................................................20
3.2.4 FITTING OF THE
DATA....................................................................................................
21
3.2.5 DETERMINATION OF THE ONSET O F RENEWED
DISSOLUTION..............................................22
3.3 HEAT FLOW
CALORIMETRY.....................................................................................................23
3.4 HEAT FLOW
CALCULATIONS..................................................................................................
23
3.4.1 THEORETICAL
BACKGROUND...........................................................................................
23
3.4.2 HEAT FLOW CALCULATIONS BASED ON PHASE DEVELOPMENT IN THE PASTE
.......................
24
3.5 SETTING
TIME....................................................................................................................
26
4
RESULTS............................................................................................................................28
4.1 CHARACTERIZATION OF THE DRY
CEMENTS..............................................................................28
4.1.1 PARTICLE SIZE DISTRIBUTION AND SPECIFIC SURFACE
.......................................................
28
4.1.2 CHEMICAL AND PHASE
ANALYSIS...................................................................................28
4.2 CHARACTERIZATION OF THE HYDRATING OPC 42.5 R
.......................................................... 30
4.2.1 HEAT FLOW
CALORIMETRY..............................................................................................31
4.2.2 SETTING TIM
E..............................................................................................................
33
4.2.3 IN SITU PHASE DEVELOPMENT OF THE HYDRATING OPC 42.5 R
.....................................
35
4.2.3.1 SILICATE
REACTION.................................................................................................
36
4.2.3.2 ALUMINATE
REACTION...........................................................................................
39
4.2.3.2.1 ALUMINATE
DISSOLUTION..................................................................................
39
4.2.3.2.2 CA-SUL FATE
DISSOLUTION.................................................................................
41
4.2.3.2.3 ETTRINGITE AND MONOSULFATE
PRECIPITATION..................................................43
4.2.4 DEGREE OF REACTION IN THE HYDRATING OPC 42.5 R
..................................................45
4.3 CHARACTERIZATION OF THE HYDRATING OPC 52.5 R
.......................................................... 47
4.3.1 HEAT FLOW
CALORIMETRY.............................................................................................
47
4.3.1.1 EFFECT O F DIFFERENT CONCENTRATIONS O F TARTARIC ACID ON THE
HYDRATION
..............
47
4.3.1.2 EFFECT O F DIFFERENT CONCENTRATIONS OF CITRIC ACID ON THE
HYDRATION
.................
51
4.3.1.3 EFFECT O F 0.1 AND 0.28 WT.% OF TARTARIC AND CITRIC ACID ON THE
HYDRATION
.....
53
4.3.1 .4 EFFECT O F 0.28 WT.% FRUIT ACID PRESENT AS A MIXTURE O F
TARTARIC AND
CITRIC ACID ON THE HYDRATION
.............................................................................
54
4.3.2 IN SITU PHASE DEVELOPMENT IN PRESENCE OF TARTARIC AND CITRIC A CID
........................56
4.3.2.1 SILICATE
REACTION.................................................................................................
57
4.3.2.2 ALUMINATE
REACTION............................................................................................
60
4.3.2.2.1 ALUMINATE
DISSOLUTION..................................................................................
60
4.3.2.2.2 CA-SULFATE
DISSOLUTION.................................................................................
62
4.3.2.2.3 ETTRINGITE AND MONOSULFATE PRECIPITATION
.................................................
64
4.3.3 HYDRATION IN PRESENCE O F STRUCTURAL RELATIVES O F TARTARIC AND
CITRIC ACID
..............
67
4.3.3.1 HEAT FLOW
CALORIMETRY.......................................................................................
67
4.3.3.2 QUANTITATIVE ASSESSMENT OF THE SILICATE
REACTION.............................................70
4.3.3.3 QUANTITATIVE ASSESSMENT O F THE ALUMINATE
REACTION.........................................71
4.3.3.3.1 ALUMINATE
DISSOLUTION..................................................................................
71
4.3.3.3.2 CA-SULFATE DISSOLUTION
................................................................
73
4.3.3.3.3 ETTRINGITE AND MONOSULFATE
PRECIPITATION..................................................74
4.3.4 RESULTS OF THE HEAT FLOW
CALCULATIONS......................................................................77
4.3.4.1 HEAT FLOW CALCULATION FOR THE BLANK PASTE
(REFERENCE).....................................77
4.3 4.2 HEAT FLOW CALCULATION FOR THE PASTE IN PRESENCE OF TARTARIC AND
CITRIC ACID.. 77
5
DISCUSSION.......................................................................................................................81
5.1 CHARACTERIZATION OF THE DRY
CEMENTS..............................................................................
81
5.2 TIME RESOLUTION OF THE IN SITU XRD
EXPERIMENTS.........................................................82
5.3 IMPACT OF TARTARIC AND CITRIC ACID ON THE SETTING BEHAVIOR O F OPC
42.5 R
.................
83
5.4 INFLUENCE OF TARTARIC AND CITRIC ACID ON THE HYDRATION AND PHASE
DEVELOPMENT
OF OPC
PASTES................................................................................................................
85
5.4.1 SILICATE
REACTION.......................................................................................................85
5.4.2 ALUMINATE
REACTION.................................................................................................
87
5.4.3 IMPACT ON HEAT FLOW EVOLUTION AND CUMULATIVE HEAT AFTER 24 HOURS O
F
HYDRATION..................................................................................................................
93
5.5 INFLUENCE OF THE STRUCTURAL RELATIVES ON THE HYDRATION
..................................................
98
5.6 POSSIBLE MECHANISM O F ACTION OF TARTARIC AND CITRIC ACID AND
IMPLICATIONS ON THE
HYDRATION OF OPC
PASTES...............................................................................................
99
5.6.1 DISCUSSION OF PUBLISHED DATA WITH RESPECT TO THE OBSERVATIONS IN
THIS STUDY
.......
99
5.6.2 PROPOSED MECHANISM FOR TARTARIC AND CITRIC A CID
...............................................
105
5.6.2.1 TARTARIC
ACID....................................................................................................106
5.6.2.2 CITRIC
ACID.......................................................................................................
I L L
5.6.2.3 MIX O F TARTARIC AND CITRIC
ACID........................................................................114
6
CONCLUSION....................................................................................................................116
7
REFERENCES...................................................................................................................
120
|
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| author | Stabler, Christopher |
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| spelling | Stabler, Christopher Verfasser aut Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten vorgelegt von Christopher Stabler Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement Erlangen ; Nürnberg Friedrich-Alexander-Universität Erlangen-Nürnberg 2018 ix, 133 Seiten Illustrationen, Diagramme 21 cm txt rdacontent n rdamedia nc rdacarrier Dissertation Friedrich-Alexander-Universität Erlangen-Nürnberg 2018 Abbinden (DE-588)4140977-2 gnd rswk-swf Portlandzement (DE-588)4175393-8 gnd rswk-swf Fruchtsäuren (DE-588)4155516-8 gnd rswk-swf Hydratation (DE-588)4193125-7 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Portlandzement (DE-588)4175393-8 s Hydratation (DE-588)4193125-7 s Abbinden (DE-588)4140977-2 s Fruchtsäuren (DE-588)4155516-8 s DE-604 B:DE-101 application/pdf http://d-nb.info/1160727805/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030481595&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Stabler, Christopher Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten Abbinden (DE-588)4140977-2 gnd Portlandzement (DE-588)4175393-8 gnd Fruchtsäuren (DE-588)4155516-8 gnd Hydratation (DE-588)4193125-7 gnd |
| subject_GND | (DE-588)4140977-2 (DE-588)4175393-8 (DE-588)4155516-8 (DE-588)4193125-7 (DE-588)4113937-9 |
| title | Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten |
| title_alt | Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement |
| title_auth | Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten |
| title_exact_search | Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten |
| title_full | Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten vorgelegt von Christopher Stabler |
| title_fullStr | Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten vorgelegt von Christopher Stabler |
| title_full_unstemmed | Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten vorgelegt von Christopher Stabler |
| title_short | Impact of chosen fruit acids on the early hydration of Ordinary Portland Cement |
| title_sort | impact of chosen fruit acids on the early hydration of ordinary portland cement implications on hydration kinetics phase development and setting der einfluss von ausgewahlten fruchtsauren auf die fruhe hydratation von portlandzement auswirkungen auf hydratationskinetik phasenentwicklung und abbindeverhalten |
| title_sub | implications on hydration kinetics, phase development and setting = Der Einfluss von ausgewählten Fruchtsäuren auf die frühe Hydratation von Portlandzement : Auswirkungen auf Hydratationskinetik, Phasenentwicklung und Abbindeverhalten |
| topic | Abbinden (DE-588)4140977-2 gnd Portlandzement (DE-588)4175393-8 gnd Fruchtsäuren (DE-588)4155516-8 gnd Hydratation (DE-588)4193125-7 gnd |
| topic_facet | Abbinden Portlandzement Fruchtsäuren Hydratation Hochschulschrift |
| url | http://d-nb.info/1160727805/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030481595&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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