Investigation of deformation mechanisms in magnesium crystals:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Aachen
Shaker
2017
|
| Edition: | [1. Auflage] |
| Series: | Berichte aus der Materialwissenschaft
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Physical Description: | xiv, 184 Seiten Illustrationen 21 cm, 296 g |
| ISBN: | 9783844055900 3844055908 |
Staff View
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| 245 | 1 | 0 | |a Investigation of deformation mechanisms in magnesium crystals |c Konstantin D. Molodov |
| 250 | |a [1. Auflage] | ||
| 264 | 1 | |a Aachen |b Shaker |c 2017 | |
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Record in the Search Index
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|---|---|
| adam_text | TABLE OF CONTENTS
LIST OF ACRONYMS XIII
1 INTRODUCTION 1
2 BACKGROUND 5
2.1 CRYSTALLOGRAPHIC GLIDE IN
MAGNESIUM..............................................................................
5
2.1.1
SLIP OF
(A)
TYPE DISLOCATIONS
........................................................................................
5
2.1.2 PYRAMIDAL SLIP OF (C + A)
DISLOCATIONS................................................................................7
2.2 DEFORMATION
TWINNING...................................................................................................
11
2.2.1 CRYSTALLOGRAPHY OF DEFORMATION
TWINNING.........................................................................11
2.2.2 ATOMIC
SHUFFLING...............................................................................................................
13
2.2.3 TWINNING MODES IN
MAGNESIUM........................................................................................13
2.2.4 DOUBLE
TWINNING...............................................................................................................
17
2.2.5 MACROSCOPIC DEFORMATION ASSOCIATED WITH MECHANICAL TWINNING
....................................
19
2.2.6 TWIN VARIANT
SELECTION.......................................................................................................
19
2.3 SLIP TRANSMISSION THROUGH TWIN
BOUNDARIES..................................................................20
2.4 DYNAMIC
RECRYSTALLIZATION............................................................................................
24
3 EXPERIMENTAL 27
3.1 SINGLE AND BI-CRYSTAL
GROWTH........................................................................................
27
3.2 CHANNEL-DIE PLANE STRAIN COMPRESSION
TESTS.................................................................30
3.3 IN-SITU SEM
TESTS...........................................................................................................
32
3.4 SAMPLE
PREPARATION........................................................................................................34
3.5 CHARACTERIZATION TECHNIQUES
4 DIVERSITY OF THE PLASTIC RESPONSE OF PURE MAGNESIUM IN PLANE STRAIN
COMPRESSION AT ROOM TEMPERATURE 39
4.1
RESULTS............................................................................................................................
39
4.1.1 FLOW BEHAVIOR OF PURE MG SINGLE CRYSTALS AT ROOM TEMPERATURE
.....................................
39
4.1.2 CONTRACTION ALONG THE C-AXIS (ORIENTATIONS A AND
B).........................................................40
4.1.3 EXTENSION ALONG THE C-AXIS (ORIENTATIONS C AND
D)............................................................44
4.1.4 CONSTRAINED C-AXIS (ORIENTATIONS E AND
F)........................................................................47
4.1.5 COMPRESSION AT 45 TO THE C-AXIS (ORIENTATIONS G AND
H)..................................................50
4.2
DISCUSSION......................................................................................................................
51
4.2.1 DEFORMATION BEHAVIOR AND FAILURE OF CRYSTALS WITH *HARD*
ORIENTATIONS
............................
51
4.2.2 EFFECT OF {1012} EXTENSION TWINNING ON THE DUCTILITY OF
DIFFERENTLY ORIENTED
MG SINGLE CRYSTALS SUBJECTED TO COMPRESSION PERPENDICULAR TO THE
C-AXIS.......................54
4.2.3 MECHANICAL RESPONSE OF CRYSTALS WITH SOFT ORIENTATIONS
...................................................
59
4.3
SUMMARY........................................................................................................................
61
5 COOPERATIVE TWINNING AND PRISMATIC SLIP AT ROOM AND ELEVATED
TEMPERATURES 63
5.1
RESULTS............................................................................................................................
63
5.2
DISCUSSION......................................................................................................................67
5.2.1 COOPERATIVE TWINNING AND SHEAR
LOCALIZATION....................................................................
67
5.2.2 PRISMATIC
SLIP.....................................................................................................................
69
5.3
SUMMARY........................................................................................................................
70
6 MULTIPLE TWINNING AND DYNAMIC RECRYSTALLIZATION AT ROOM TEMPERATURE 73
6.1
RESULTS............................................................................................................................
73
6.1.1 MECHANICAL BEHAVIOR OF C-ORIENTED
CRYSTALS....................................................................73
6.1.2 MACROTEXTURE EVOLUTION DURING
DEFORMATION.....................................................................
74
6.1.3 MICROSTRUCTURE EVOLUTION AS OBTAINED BY EBSD MEASUREMENTS
.......................................
76
6.1.4 SIZE AND ORIENTATION DISTRIBUTION OF RECRYSTALLIZED GRAINS AT THE
FINAL STRAIN
.....................
81
6.2
DISCUSSION......................................................................................................................
82
6.2.1 TEXTURE EVOLUTION DURING MULTIPLE
TWINNING.....................................................................
82
6.2.2 TEXTURE EVOLUTION DURING CONTINUOUS DYNAMIC RECRYSTALLIZATION
.....................................
86
6.2.3 SHEAR LOCALIZATION IN DEFORMATION
TWINS...........................................................................
90
6.2.4 TWIN FRAGMENTATION AND DYNAMIC RECRYSTALLIZATION
........................................................
91
6.2.5 ORIGIN OF GRAIN BOUNDARIES WITH A MISORIENTATION ANGLE OF 30
.......................................
93
6.3
SUMMARY.........................................................................................................................95
7 ORIGIN AND ROLE OF ANOMALOUS TWINNING IN THE PLASTICITY AND
MICROSTRUCTURE
EVOLUTION OF MAGNESIUM 97
7.1
RESULTS............................................................................................................................98
7.1.1 MECHANICAL BEHAVIOR OF G-ORIENTED
CRYSTALS....................................................................98
7.1.2 MICROSTRUCTURE EVOLUTION DURING
DEFORMATION...................................................................99
7.2
DISCUSSION....................................................................................................................102
7.2.1 LATTICE ROTATION DUE TO
SLIP...............................................................................................
102
7.2.2 SERRATED PLASTIC
FLOW.......................................................................................................
103
7.2.3 ANOMALOUS
TWINNING.......................................................................................................
104
7.2.4 DEFORMATION
HETEROGENEITY.............................................................................................110
7.3
SUMMARY......................................................................................................................112
8 EFFECT OF GADOLINIUM ADDITION ON THE DEFORMATION AND RECRYSTALLIZATION
BEHAVIOR OF MG SINGLE CRYSTALS 115
8.1
RESULTS..........................................................................................................................115
8.1.1 MECHANICAL BEHAVIOR OF SELECTED MG-0.8 GD SINGLE CRYSTALS
........................................
115
8.1.2 EFFECT OF GD ON THE MICROSTRUCTURE EVOLUTION OF SELECTED MG SINGLE
CRYSTALS
...............
117
8.2
DISCUSSION....................................................................................................................120
8.3
SUMMARY......................................................................................................................124
9 PROFUSE SLIP TRANSMISSION ACROSS TWIN BOUNDARIES IN MAGNESIUM 125
9.1
RESULTS..........................................................................................................................126
9.1.1 IN-SITU OBSERVATIONS OF {1012} EXTENSION
TWINNING.......................................................126
9.1.2 BASAL SLIP TRANSMISSION ACROSS {1012} TWIN BOUNDARIES AT ROOM
TEMPERATURE
...............
128
9.1.3 NON-BASAL SLIP TRACES AT ELEVATED TEMPERATURE IN {1012} EXTENSION
TWINS
....................
129
9.1.4 SLIP TRANSMISSION THROUGH CONTRACTION AND DOUBLE
TWINS................................................130
9.2
DISCUSSION....................................................................................................................131
9.2.1 SHEAR-COUPLED TWIN BOUNDARY
MIGRATION........................................................................131
9.2.2 SLIP TRACES THROUGH {1012} EXTENSION
TWINS..................................................................
134
9.2.3 DIRECT AND INDIRECT SLIP TRANSFER (SPECIMEN I)..
9.2.4 DIRECT AND INDIRECT SLIP TRANSFER (SPECIMEN
II)..............................................................139
9.2.5 ACTIVATION OF NON-BASAL SLIP (SPECIMEN
III)..................................................................140
9.2.6 CONTRACTION AND DOUBLE TWINS (SPECIMEN IV)
.................................................................
142
9.3
SUMMARY......................................................................................................................
143
10 GENERAL CONCLUSIONS 145
10.1 PURE MG SINGLE CRYSTAL
DEFORMATION...........................................................................
145
10.2 MG-GD SINGLE CRYSTAL
DEFORMATION..............................................................................147
10.3 SLIP TRANSMISSION THROUGH TWIN
BOUNDARIES................................................................
148
APPENDIX A - SUPPLEMENTARY STRESS-STRAIN CURVES 149
A. 1 PURE MG SINGLE CRYSTALS IN CHANNEL-DIE PLANE STRAIN COMPRESSION AT
ROOM AND ELEVATED
TEMPERATURE...................................................................................
149
A.2 MG-0.8 WT.% GD SINGLE CRYSTALS IN CHANNEL-DIE PLANE STRAIN
COMPRESSION AT ROOM AND ELEVATED TEMPERATURE
.........................................................
150
APPENDIX B - SUPPLEMENTARY OPTICAL MICROGRAPHS 151
APPENDIX C 155
C. 1 CALCULATION OF THE SCHMID FACTOR (SF) FOR SLIP AND TWINNING IN
CHANNEL-
DIE
PSC.........................................................................................................................
155
C.2 DISPLACEMENT GRADIENT TENSOR FOR {1012} EXTENSION
TWINNING..................................156
C.3 SLIP
TRANSFER..................................................................................................................157
C.4 EXPERIMENTAL DETERMINATION OF THE TWINNING SHEAR FOR {1012}
TWINS........................158
BIBLIOGRAPHY 161
LIST OF PUBLICATIONS 179
ABSTRACT 181
KURZZUSAMMENFASSUNG
183
|
| any_adam_object | 1 |
| author | Molodov, Konstantin D. 1985- |
| author_GND | (DE-588)114738990X |
| author_facet | Molodov, Konstantin D. 1985- |
| author_role | aut |
| author_sort | Molodov, Konstantin D. 1985- |
| author_variant | k d m kd kdm |
| building | Verbundindex |
| bvnumber | BV044699720 |
| classification_rvk | ZM 4610 |
| ctrlnum | (OCoLC)1021377157 (DE-599)DNB1141924706 |
| dewey-full | 620.18799 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 620 - Engineering and allied operations |
| dewey-raw | 620.18799 |
| dewey-search | 620.18799 |
| dewey-sort | 3620.18799 |
| dewey-tens | 620 - Engineering and allied operations |
| discipline | Maschinenbau / Maschinenwesen Werkstoffwissenschaften / Fertigungstechnik |
| edition | [1. Auflage] |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV044699720 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T07:59:41Z |
| institution | BVB |
| institution_GND | (DE-588)1064118135 |
| isbn | 9783844055900 3844055908 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-030096454 |
| oclc_num | 1021377157 |
| open_access_boolean | |
| owner | DE-83 |
| owner_facet | DE-83 |
| physical | xiv, 184 Seiten Illustrationen 21 cm, 296 g |
| publishDate | 2017 |
| publishDateSearch | 2017 |
| publishDateSort | 2017 |
| publisher | Shaker |
| record_format | marc |
| series2 | Berichte aus der Materialwissenschaft |
| spelling | Molodov, Konstantin D. 1985- Verfasser (DE-588)114738990X aut Investigation of deformation mechanisms in magnesium crystals Konstantin D. Molodov [1. Auflage] Aachen Shaker 2017 xiv, 184 Seiten Illustrationen 21 cm, 296 g txt rdacontent n rdamedia nc rdacarrier Berichte aus der Materialwissenschaft Dissertation RWTH Aachen University 2017 Einkristall (DE-588)4013901-3 gnd rswk-swf Rekristallisationstextur (DE-588)4177657-4 gnd rswk-swf Kristallorientierung (DE-588)4623755-0 gnd rswk-swf Magnesiumlegierung (DE-588)4168536-2 gnd rswk-swf Plastische Deformation (DE-588)4115572-5 gnd rswk-swf Werkstoffprüfung (DE-588)4037934-6 gnd rswk-swf Magnesium (DE-588)4128915-8 gnd rswk-swf Duktilität (DE-588)4290955-7 gnd rswk-swf Mikrostruktur (DE-588)4131028-7 gnd rswk-swf Magnesium Plasticity Recrystallization (DE-588)4113937-9 Hochschulschrift gnd-content Magnesium (DE-588)4128915-8 s Einkristall (DE-588)4013901-3 s Plastische Deformation (DE-588)4115572-5 s Werkstoffprüfung (DE-588)4037934-6 s DE-604 Magnesiumlegierung (DE-588)4168536-2 s Duktilität (DE-588)4290955-7 s Mikrostruktur (DE-588)4131028-7 s Rekristallisationstextur (DE-588)4177657-4 s Kristallorientierung (DE-588)4623755-0 s Shaker Verlag (DE-588)1064118135 pbl B:DE-101 application/pdf http://d-nb.info/1141924706/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030096454&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Molodov, Konstantin D. 1985- Investigation of deformation mechanisms in magnesium crystals Einkristall (DE-588)4013901-3 gnd Rekristallisationstextur (DE-588)4177657-4 gnd Kristallorientierung (DE-588)4623755-0 gnd Magnesiumlegierung (DE-588)4168536-2 gnd Plastische Deformation (DE-588)4115572-5 gnd Werkstoffprüfung (DE-588)4037934-6 gnd Magnesium (DE-588)4128915-8 gnd Duktilität (DE-588)4290955-7 gnd Mikrostruktur (DE-588)4131028-7 gnd |
| subject_GND | (DE-588)4013901-3 (DE-588)4177657-4 (DE-588)4623755-0 (DE-588)4168536-2 (DE-588)4115572-5 (DE-588)4037934-6 (DE-588)4128915-8 (DE-588)4290955-7 (DE-588)4131028-7 (DE-588)4113937-9 |
| title | Investigation of deformation mechanisms in magnesium crystals |
| title_auth | Investigation of deformation mechanisms in magnesium crystals |
| title_exact_search | Investigation of deformation mechanisms in magnesium crystals |
| title_full | Investigation of deformation mechanisms in magnesium crystals Konstantin D. Molodov |
| title_fullStr | Investigation of deformation mechanisms in magnesium crystals Konstantin D. Molodov |
| title_full_unstemmed | Investigation of deformation mechanisms in magnesium crystals Konstantin D. Molodov |
| title_short | Investigation of deformation mechanisms in magnesium crystals |
| title_sort | investigation of deformation mechanisms in magnesium crystals |
| topic | Einkristall (DE-588)4013901-3 gnd Rekristallisationstextur (DE-588)4177657-4 gnd Kristallorientierung (DE-588)4623755-0 gnd Magnesiumlegierung (DE-588)4168536-2 gnd Plastische Deformation (DE-588)4115572-5 gnd Werkstoffprüfung (DE-588)4037934-6 gnd Magnesium (DE-588)4128915-8 gnd Duktilität (DE-588)4290955-7 gnd Mikrostruktur (DE-588)4131028-7 gnd |
| topic_facet | Einkristall Rekristallisationstextur Kristallorientierung Magnesiumlegierung Plastische Deformation Werkstoffprüfung Magnesium Duktilität Mikrostruktur Hochschulschrift |
| url | http://d-nb.info/1141924706/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030096454&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT molodovkonstantind investigationofdeformationmechanismsinmagnesiumcrystals AT shakerverlag investigationofdeformationmechanismsinmagnesiumcrystals |
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