Verfügbarkeit: Investigation of deformation mechanisms in magnesium crystals

Investigation of deformation mechanisms in magnesium crystals:

Gespeichert in:

Bibliographische Detailangaben
1. Verfasser:	Molodov, Konstantin D. 1985- (VerfasserIn)
Format:	Abschlussarbeit Buch
Sprache:	English
Veröffentlicht:	Aachen Shaker 2017
Ausgabe:	[1. Auflage]
Schriftenreihe:	Berichte aus der Materialwissenschaft
Schlagworte:	Einkristall Rekristallisationstextur Kristallorientierung Magnesiumlegierung Plastische Deformation Werkstoffprüfung Magnesium Duktilität Mikrostruktur Plasticity Recrystallization Hochschulschrift
Online-Zugang:	Inhaltsverzeichnis Inhaltsverzeichnis
Beschreibung:	xiv, 184 Seiten Illustrationen 21 cm, 296 g
ISBN:	9783844055900 3844055908

Internformat

MARC


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Datensatz im Suchindex

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adam_text	TABLE OF CONTENTS LIST OF ACRONYMS XIII 1 INTRODUCTION 1 2 BACKGROUND 5 2.1 CRYSTALLOGRAPHIC GLIDE IN MAGNESIUM.............................................................................. 5 2.1.1 SLIP OF (A) TYPE DISLOCATIONS ........................................................................................ 5 2.1.2 PYRAMIDAL SLIP OF (C + A) DISLOCATIONS................................................................................7 2.2 DEFORMATION TWINNING................................................................................................... 11 2.2.1 CRYSTALLOGRAPHY OF DEFORMATION TWINNING.........................................................................11 2.2.2 ATOMIC SHUFFLING............................................................................................................... 13 2.2.3 TWINNING MODES IN MAGNESIUM........................................................................................13 2.2.4 DOUBLE TWINNING............................................................................................................... 17 2.2.5 MACROSCOPIC DEFORMATION ASSOCIATED WITH MECHANICAL TWINNING .................................... 19 2.2.6 TWIN VARIANT SELECTION....................................................................................................... 19 2.3 SLIP TRANSMISSION THROUGH TWIN BOUNDARIES..................................................................20 2.4 DYNAMIC RECRYSTALLIZATION............................................................................................ 24 3 EXPERIMENTAL 27 3.1 SINGLE AND BI-CRYSTAL GROWTH........................................................................................ 27 3.2 CHANNEL-DIE PLANE STRAIN COMPRESSION TESTS.................................................................30 3.3 IN-SITU SEM TESTS........................................................................................................... 32 3.4 SAMPLE PREPARATION........................................................................................................34 3.5 CHARACTERIZATION TECHNIQUES 4 DIVERSITY OF THE PLASTIC RESPONSE OF PURE MAGNESIUM IN PLANE STRAIN COMPRESSION AT ROOM TEMPERATURE 39 4.1 RESULTS............................................................................................................................ 39 4.1.1 FLOW BEHAVIOR OF PURE MG SINGLE CRYSTALS AT ROOM TEMPERATURE ..................................... 39 4.1.2 CONTRACTION ALONG THE C-AXIS (ORIENTATIONS A AND B).........................................................40 4.1.3 EXTENSION ALONG THE C-AXIS (ORIENTATIONS C AND D)............................................................44 4.1.4 CONSTRAINED C-AXIS (ORIENTATIONS E AND F)........................................................................47 4.1.5 COMPRESSION AT 45 TO THE C-AXIS (ORIENTATIONS G AND H)..................................................50 4.2 DISCUSSION...................................................................................................................... 51 4.2.1 DEFORMATION BEHAVIOR AND FAILURE OF CRYSTALS WITH HARD ORIENTATIONS ............................ 51 4.2.2 EFFECT OF {1012} EXTENSION TWINNING ON THE DUCTILITY OF DIFFERENTLY ORIENTED MG SINGLE CRYSTALS SUBJECTED TO COMPRESSION PERPENDICULAR TO THE C-AXIS.......................54 4.2.3 MECHANICAL RESPONSE OF CRYSTALS WITH SOFT ORIENTATIONS ................................................... 59 4.3 SUMMARY........................................................................................................................ 61 5 COOPERATIVE TWINNING AND PRISMATIC SLIP AT ROOM AND ELEVATED TEMPERATURES 63 5.1 RESULTS............................................................................................................................ 63 5.2 DISCUSSION......................................................................................................................67 5.2.1 COOPERATIVE TWINNING AND SHEAR LOCALIZATION.................................................................... 67 5.2.2 PRISMATIC SLIP..................................................................................................................... 69 5.3 SUMMARY........................................................................................................................ 70 6 MULTIPLE TWINNING AND DYNAMIC RECRYSTALLIZATION AT ROOM TEMPERATURE 73 6.1 RESULTS............................................................................................................................ 73 6.1.1 MECHANICAL BEHAVIOR OF C-ORIENTED CRYSTALS....................................................................73 6.1.2 MACROTEXTURE EVOLUTION DURING DEFORMATION..................................................................... 74 6.1.3 MICROSTRUCTURE EVOLUTION AS OBTAINED BY EBSD MEASUREMENTS ....................................... 76 6.1.4 SIZE AND ORIENTATION DISTRIBUTION OF RECRYSTALLIZED GRAINS AT THE FINAL STRAIN ..................... 81 6.2 DISCUSSION...................................................................................................................... 82 6.2.1 TEXTURE EVOLUTION DURING MULTIPLE TWINNING..................................................................... 82 6.2.2 TEXTURE EVOLUTION DURING CONTINUOUS DYNAMIC RECRYSTALLIZATION ..................................... 86 6.2.3 SHEAR LOCALIZATION IN DEFORMATION TWINS........................................................................... 90 6.2.4 TWIN FRAGMENTATION AND DYNAMIC RECRYSTALLIZATION ........................................................ 91 6.2.5 ORIGIN OF GRAIN BOUNDARIES WITH A MISORIENTATION ANGLE OF 30 ....................................... 93 6.3 SUMMARY.........................................................................................................................95 7 ORIGIN AND ROLE OF ANOMALOUS TWINNING IN THE PLASTICITY AND MICROSTRUCTURE EVOLUTION OF MAGNESIUM 97 7.1 RESULTS............................................................................................................................98 7.1.1 MECHANICAL BEHAVIOR OF G-ORIENTED CRYSTALS....................................................................98 7.1.2 MICROSTRUCTURE EVOLUTION DURING DEFORMATION...................................................................99 7.2 DISCUSSION....................................................................................................................102 7.2.1 LATTICE ROTATION DUE TO SLIP............................................................................................... 102 7.2.2 SERRATED PLASTIC FLOW....................................................................................................... 103 7.2.3 ANOMALOUS TWINNING....................................................................................................... 104 7.2.4 DEFORMATION HETEROGENEITY.............................................................................................110 7.3 SUMMARY......................................................................................................................112 8 EFFECT OF GADOLINIUM ADDITION ON THE DEFORMATION AND RECRYSTALLIZATION BEHAVIOR OF MG SINGLE CRYSTALS 115 8.1 RESULTS..........................................................................................................................115 8.1.1 MECHANICAL BEHAVIOR OF SELECTED MG-0.8 GD SINGLE CRYSTALS ........................................ 115 8.1.2 EFFECT OF GD ON THE MICROSTRUCTURE EVOLUTION OF SELECTED MG SINGLE CRYSTALS ............... 117 8.2 DISCUSSION....................................................................................................................120 8.3 SUMMARY......................................................................................................................124 9 PROFUSE SLIP TRANSMISSION ACROSS TWIN BOUNDARIES IN MAGNESIUM 125 9.1 RESULTS..........................................................................................................................126 9.1.1 IN-SITU OBSERVATIONS OF {1012} EXTENSION TWINNING.......................................................126 9.1.2 BASAL SLIP TRANSMISSION ACROSS {1012} TWIN BOUNDARIES AT ROOM TEMPERATURE ............... 128 9.1.3 NON-BASAL SLIP TRACES AT ELEVATED TEMPERATURE IN {1012} EXTENSION TWINS .................... 129 9.1.4 SLIP TRANSMISSION THROUGH CONTRACTION AND DOUBLE TWINS................................................130 9.2 DISCUSSION....................................................................................................................131 9.2.1 SHEAR-COUPLED TWIN BOUNDARY MIGRATION........................................................................131 9.2.2 SLIP TRACES THROUGH {1012} EXTENSION TWINS.................................................................. 134 9.2.3 DIRECT AND INDIRECT SLIP TRANSFER (SPECIMEN I).. 9.2.4 DIRECT AND INDIRECT SLIP TRANSFER (SPECIMEN II)..............................................................139 9.2.5 ACTIVATION OF NON-BASAL SLIP (SPECIMEN III)..................................................................140 9.2.6 CONTRACTION AND DOUBLE TWINS (SPECIMEN IV) ................................................................. 142 9.3 SUMMARY...................................................................................................................... 143 10 GENERAL CONCLUSIONS 145 10.1 PURE MG SINGLE CRYSTAL DEFORMATION........................................................................... 145 10.2 MG-GD SINGLE CRYSTAL DEFORMATION..............................................................................147 10.3 SLIP TRANSMISSION THROUGH TWIN BOUNDARIES................................................................ 148 APPENDIX A - SUPPLEMENTARY STRESS-STRAIN CURVES 149 A. 1 PURE MG SINGLE CRYSTALS IN CHANNEL-DIE PLANE STRAIN COMPRESSION AT ROOM AND ELEVATED TEMPERATURE................................................................................... 149 A.2 MG-0.8 WT.% GD SINGLE CRYSTALS IN CHANNEL-DIE PLANE STRAIN COMPRESSION AT ROOM AND ELEVATED TEMPERATURE ......................................................... 150 APPENDIX B - SUPPLEMENTARY OPTICAL MICROGRAPHS 151 APPENDIX C 155 C. 1 CALCULATION OF THE SCHMID FACTOR (SF) FOR SLIP AND TWINNING IN CHANNEL- DIE PSC......................................................................................................................... 155 C.2 DISPLACEMENT GRADIENT TENSOR FOR {1012} EXTENSION TWINNING..................................156 C.3 SLIP TRANSFER..................................................................................................................157 C.4 EXPERIMENTAL DETERMINATION OF THE TWINNING SHEAR FOR {1012} TWINS........................158 BIBLIOGRAPHY 161 LIST OF PUBLICATIONS 179 ABSTRACT 181 KURZZUSAMMENFASSUNG 183
any_adam_object	1
author	Molodov, Konstantin D. 1985-
author_GND	(DE-588)114738990X
author_facet	Molodov, Konstantin D. 1985-
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author_sort	Molodov, Konstantin D. 1985-
author_variant	k d m kd kdm
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dewey-hundreds	600 - Technology (Applied sciences)
dewey-ones	620 - Engineering and allied operations
dewey-raw	620.18799
dewey-search	620.18799
dewey-sort	3620.18799
dewey-tens	620 - Engineering and allied operations
discipline	Maschinenbau / Maschinenwesen Werkstoffwissenschaften / Fertigungstechnik
edition	[1. Auflage]
format	Thesis Book
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series2	Berichte aus der Materialwissenschaft
spelling	Molodov, Konstantin D. 1985- Verfasser (DE-588)114738990X aut Investigation of deformation mechanisms in magnesium crystals Konstantin D. Molodov [1. Auflage] Aachen Shaker 2017 xiv, 184 Seiten Illustrationen 21 cm, 296 g txt rdacontent n rdamedia nc rdacarrier Berichte aus der Materialwissenschaft Dissertation RWTH Aachen University 2017 Einkristall (DE-588)4013901-3 gnd rswk-swf Rekristallisationstextur (DE-588)4177657-4 gnd rswk-swf Kristallorientierung (DE-588)4623755-0 gnd rswk-swf Magnesiumlegierung (DE-588)4168536-2 gnd rswk-swf Plastische Deformation (DE-588)4115572-5 gnd rswk-swf Werkstoffprüfung (DE-588)4037934-6 gnd rswk-swf Magnesium (DE-588)4128915-8 gnd rswk-swf Duktilität (DE-588)4290955-7 gnd rswk-swf Mikrostruktur (DE-588)4131028-7 gnd rswk-swf Magnesium Plasticity Recrystallization (DE-588)4113937-9 Hochschulschrift gnd-content Magnesium (DE-588)4128915-8 s Einkristall (DE-588)4013901-3 s Plastische Deformation (DE-588)4115572-5 s Werkstoffprüfung (DE-588)4037934-6 s DE-604 Magnesiumlegierung (DE-588)4168536-2 s Duktilität (DE-588)4290955-7 s Mikrostruktur (DE-588)4131028-7 s Rekristallisationstextur (DE-588)4177657-4 s Kristallorientierung (DE-588)4623755-0 s Shaker Verlag (DE-588)1064118135 pbl B:DE-101 application/pdf http://d-nb.info/1141924706/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030096454&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	Molodov, Konstantin D. 1985- Investigation of deformation mechanisms in magnesium crystals Einkristall (DE-588)4013901-3 gnd Rekristallisationstextur (DE-588)4177657-4 gnd Kristallorientierung (DE-588)4623755-0 gnd Magnesiumlegierung (DE-588)4168536-2 gnd Plastische Deformation (DE-588)4115572-5 gnd Werkstoffprüfung (DE-588)4037934-6 gnd Magnesium (DE-588)4128915-8 gnd Duktilität (DE-588)4290955-7 gnd Mikrostruktur (DE-588)4131028-7 gnd
subject_GND	(DE-588)4013901-3 (DE-588)4177657-4 (DE-588)4623755-0 (DE-588)4168536-2 (DE-588)4115572-5 (DE-588)4037934-6 (DE-588)4128915-8 (DE-588)4290955-7 (DE-588)4131028-7 (DE-588)4113937-9
title	Investigation of deformation mechanisms in magnesium crystals
title_auth	Investigation of deformation mechanisms in magnesium crystals
title_exact_search	Investigation of deformation mechanisms in magnesium crystals
title_full	Investigation of deformation mechanisms in magnesium crystals Konstantin D. Molodov
title_fullStr	Investigation of deformation mechanisms in magnesium crystals Konstantin D. Molodov
title_full_unstemmed	Investigation of deformation mechanisms in magnesium crystals Konstantin D. Molodov
title_short	Investigation of deformation mechanisms in magnesium crystals
title_sort	investigation of deformation mechanisms in magnesium crystals
topic	Einkristall (DE-588)4013901-3 gnd Rekristallisationstextur (DE-588)4177657-4 gnd Kristallorientierung (DE-588)4623755-0 gnd Magnesiumlegierung (DE-588)4168536-2 gnd Plastische Deformation (DE-588)4115572-5 gnd Werkstoffprüfung (DE-588)4037934-6 gnd Magnesium (DE-588)4128915-8 gnd Duktilität (DE-588)4290955-7 gnd Mikrostruktur (DE-588)4131028-7 gnd
topic_facet	Einkristall Rekristallisationstextur Kristallorientierung Magnesiumlegierung Plastische Deformation Werkstoffprüfung Magnesium Duktilität Mikrostruktur Hochschulschrift
url	http://d-nb.info/1141924706/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030096454&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT molodovkonstantind investigationofdeformationmechanismsinmagnesiumcrystals AT shakerverlag investigationofdeformationmechanismsinmagnesiumcrystals

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