Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2: = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | German English |
| Veröffentlicht: |
Erlangen ; Nürnberg
2017
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | VII, 327 Seiten Illustrationen, Diagramme |
Internformat
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| 245 | 1 | 0 | |a Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 |b = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 |c vorgelegt von Sabine D. Dommer aus Nürnberg |
| 246 | 1 | 1 | |a Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 |
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| adam_text | DESIGN, SYNTHESIS, AND SUPRAMOLECULAR PROPERTIES
OF IMIDAZOLIUM-BASED ORGANIC CATIONS FOR THE
ABSORPTION OR REDUCTION OF CO2
DESIGN, SYNTHESE UND SUPRAMOLEKULARE
EIGENSCHAFTEN VON AUF IMIDAZOLIUM BASIERENDEN
ORGANISCHEN KATIONEN ZUR ABSORPTION ODER
REDUKTION VON CO2
DER NATURWISSENSCHAFTLICHEN FAKULTAET
DER FRIEDRICH-ALEXANDER-UNIVERSITAET ERLANGEN-NUERNBERG
ZUR
ERLANGUNG DES DOKTORGRADES DR. RER. NAT.
VORGELEGT VON
SABINE D. DOMMER
AUS NUERNBERG
TABLE OF CONTENTS
TABLE OF
CONTENTS....................................................................................................................I
LIST OF
ABBREVIATIONS...........................................................................................................IV
1
INTRODUCTION.........................................................................................................1
1.1 C02 CAPTURE AND STORAGE
(CCS)........................................................................2
1.1.1 C02 CAPTURE
TECHNOLOGIES.....................................................................................
3
1.1.2 NEW MATERIALS FOR THE CHEMICAL ABSORPTION OF
C02.............................................7
1.2 C02 REDUCTION AND USES AS CHEMICAL FEEDSTOCK
.........................................
13
1.2.1 THE C02
MOLECULE.................................................................................................
13
1.2.2 INDUSTRIAL REACTIONS WITH
C02.............................................................................14
1.2.3 C02
TRANSFORMATIONS............................................................................................
15
1.3 SUPRAMOLECULAR
CHEMISTRY..............................................................................20
1.3.1 ANION RECEPTORS
................
21
1.3.2 ANTON RECEPTORS WITH DIFFERENT BINDING MOTIFS
.................................................
29
1.4 AZAANGULENIUM
SALTS.......................................................................................34
2
MOTIVATION..........................................................................................................37
3 RESULTS AND
DISCUSSION....................................................................................
41
3.1 SOLVENTS FOR THE ABSORPTION OF C02 FROM RAW BIOGAS
...............................
41
3.1.1 IMIDAZOLIUM-BASED IONIC LIQUIDS (IMIDAZOLIUM SALTS)
......................................
46
3.1.2 POLY(AMIDOAMINE) DENDRIMERS
(PAMAM).........................................................61
3.1.3 RESULTS OF THE C02-SOLUBILITY MEASUREMENTS
....................................................
71
3.2 MULTINUCLEAR IMIDAZOLIUM SALTS FOR THE CHEMICAL ACTIVATION OF C02
....77
3.2.1 MODULAR SYNTHESIS OF MULTINUCLEAR IMIDAZOLIUM SALTS (MISS)
...........................
80
3.2.2 C02 ACTIVATION
MEASUREMENTS..........................................................................104
3.3 ANALYSIS OF BINDING
PROPERTIES......................................................................121
3.3.1 ANION BINDING PROPERTIES OF IMIDAZOLIUM-AZAANGULENIUM-BASED
RECEPTORS 124
3.3.2 SELF-AGGREGATION BEHAVIOR OF THE RECEPTORS
.............................
126
3.3.3 AZAANGULENIUM-BASED RECEPTORS BRIDGED WITH APMI U N
ITS...........................131
3.3.4 AZAANGULENIUM-TWEEZERS AS RECEPTORS
...........................................................
142
4
SUMMARY...............................................................................................
150
4.1 SOLVENTS FOR THE ABSORPTION OF C02 FROM FLUE OR BIOGAS
.........................
150
4.2 MULTINUCLEAR IMIDAZOLIUM SALTS FOR THE CHEMICAL ACTIVATION OF C02..
154
4.3 ANALYSIS OF BINDING PROPERTIES
....................................................................
156
4.4
OUTLOOK.............................................................................................................
160
5
ZUSAMMENFASSUNG..........................................................................................
162
5.1 LOESUNGSMITTEL FUER DIE ABSORPTION VON C02 AUS RAUCH- UND BIOGAS ....
162
5.2 MEHRKEMIGE IMIDAZOLIUMSALZE FUER DIE CHEMISCHE AKTIVIERUNG VON
C02
.........
..........................................................................................................
166
5.3 ANALYSE DER
ANIONENBINDUNGSEIGENSCHAFTEN............................................
169
5.4
AUSBLICK............................................................................................................
173
6 EXPERIMENTAL
SECTION......................................................................................175
6.1 GENERAL
INFORMATION.......................................................................................
175
6.1.1 CHEMICALS AND
TECHNIQUES................................................................................
175
6.1.2 ANALYSIS M
ETHODS...............................................................................................175
6.2 EXPERIMENTAL
PROCEDURES...............................................................................179
6.2.1 SYNTHESIS OF IMIDAZOLIUM
HALIDES.....................................................................
179
6.2.2 SYNTHESIS OF IMIDAZOLIUM
TETRAFLUOROBORATES..................................................184
6.2.3 SYNTHESIS OF IMIDAZOLIUM
ACETATES...................................................................
185
6.2.4 SYNTHESIS OF IMIDAZOLIUM
HEXAFLUOROPHOSPHATES........................................... 187
6.2.5 SYNTHESIS OF IMIDAZOLIUM
CARBOXYLATES...........................................................
190
6.2.6 REACTION OF NHCS WITH PHENYLISOCYANATE OR
DCC..........................................194
6.2.7 SYNTHESIS OF PAMAM
DENDRIMERS....................................................................
194
6.2.8 SYNTHESIS OF MULTINUCLEAR IMIDAZOLIUM SA
LTS..................................................198
6.2.9 SYNTHESIS OF MULTINUCLEAR IMIDAZOLIUM-AZATRIANGULENIUM SA
LTS..................200
6.3 EXPERIMENTAL ANALYSIS OF SUPRAMOLECULAR BINDING
AFFINITIES................229
6.3.1 DETERMINATION OF
SELF-AGGREGATION...................................................................229
6.3.2 DETERMINATION OF COMPLEX
STOICHIOMETRY........................................................230
6.3.3 DETERMINATION OF ASSOCIATION
CONSTANTS.........................................................231
7
APPENDIX...........................................................................................................233
7.1 COMPOUND
REGISTER........................................................................................
233
7.2 INITIAL WEIGHTS FOR THE DETERMINATION OF THE SUPRAMOLECULAR ANION
BINDING
AFFINITIES.........................................................................................
235
7.2.1 INITIAL WEIGHTS FOR THE DETERMINATION OF THE SELF-AGGREGATION
.......................
235
7.2.2 INITIAL WEIGHTS FOR THE DETERMINATION OF COMPLEX STOICHIOMETRY
..................
236
7.2.3 INITIAL WEIGHTS FOR THE DETERMINATION OF ASSOCIATION CONSTANTS
....................
238
7.2.4 JOB PLOT ANALYSIS OF THE INVESTIGATED RECEPTORS
...............................................
243
7.2.5 BINDING ISOTHERMS OF THE INVESTIGATED RECEPTORS
............................................
251
7.3 SPECTRAL DATA - NMR AND MASS DATA OF SELECTED COMPOUNDS
................
264
8
REFERENCES........................................................................309
IN
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| language | German English |
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| spelling | Dommer, Sabine aut Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 vorgelegt von Sabine D. Dommer aus Nürnberg Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 Erlangen ; Nürnberg 2017 VII, 327 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Dissertation Friedrich-Alexander-Universität Erlangen-Nürnberg 2017 Kohlendioxid (DE-588)4031648-8 gnd rswk-swf Organisches Kation (DE-588)7576892-6 gnd rswk-swf Reduktion Chemie (DE-588)4277879-7 gnd rswk-swf Adsorption (DE-588)4000536-7 gnd rswk-swf Imidazolderivate (DE-588)4161308-9 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Organisches Kation (DE-588)7576892-6 s Imidazolderivate (DE-588)4161308-9 s Kohlendioxid (DE-588)4031648-8 s Adsorption (DE-588)4000536-7 s DE-604 Reduktion Chemie (DE-588)4277879-7 s DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029867113&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Dommer, Sabine Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 Kohlendioxid (DE-588)4031648-8 gnd Organisches Kation (DE-588)7576892-6 gnd Reduktion Chemie (DE-588)4277879-7 gnd Adsorption (DE-588)4000536-7 gnd Imidazolderivate (DE-588)4161308-9 gnd |
| subject_GND | (DE-588)4031648-8 (DE-588)7576892-6 (DE-588)4277879-7 (DE-588)4000536-7 (DE-588)4161308-9 (DE-588)4113937-9 |
| title | Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 |
| title_alt | Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 |
| title_auth | Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 |
| title_exact_search | Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 |
| title_full | Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 vorgelegt von Sabine D. Dommer aus Nürnberg |
| title_fullStr | Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 vorgelegt von Sabine D. Dommer aus Nürnberg |
| title_full_unstemmed | Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 vorgelegt von Sabine D. Dommer aus Nürnberg |
| title_short | Design, synthesis, and supramolecular properties of imidazolium-based organic cations for the absorption or reduction of CO2 |
| title_sort | design synthesis and supramolecular properties of imidazolium based organic cations for the absorption or reduction of co2 design synthese und supramolekulare eigenschaften von auf imidazolium basierenden organischen kationen zur absorption oder reduktion von co2 |
| title_sub | = Design, Synthese und supramolekulare Eigenschaften von auf Imidazolium basierenden organischen Kationen zur Absorption oder Reduktion von CO2 |
| topic | Kohlendioxid (DE-588)4031648-8 gnd Organisches Kation (DE-588)7576892-6 gnd Reduktion Chemie (DE-588)4277879-7 gnd Adsorption (DE-588)4000536-7 gnd Imidazolderivate (DE-588)4161308-9 gnd |
| topic_facet | Kohlendioxid Organisches Kation Reduktion Chemie Adsorption Imidazolderivate Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029867113&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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