Organic trace analysis:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin ; Boston
De Gruyter
[2017]
|
| Schriftenreihe: | De Gruyter graduate
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XII, 357 Seiten Illustrationen, Diagramme (farbig) |
| ISBN: | 9783110441147 3110441144 |
Internformat
MARC
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| 100 | 1 | |a Nießner, Reinhard |d 1951- |e Verfasser |0 (DE-588)141829591 |4 aut | |
| 245 | 1 | 0 | |a Organic trace analysis |c Niessner, Schäffer |
| 264 | 1 | |a Berlin ; Boston |b De Gruyter |c [2017] | |
| 264 | 4 | |c © 2017 | |
| 300 | |a XII, 357 Seiten |b Illustrationen, Diagramme (farbig) | ||
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Datensatz im Suchindex
| _version_ | 1804177764433002496 |
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| adam_text | CONTENTS
I
1.1
1.2
1.3
1.4
1.5
1.6
2
2.1
2.2
2.3
2.4
2.5
2.6
2.7
2.8
3
3.1
3.2
3.3
3.4
3.5
3.6
4
4.1
4.2
4.2.1
4.2.2
4.2.3
4.2.4
OVERVIEW * 1
GENERAL REMARKS * 1
WHAT DOES * ORGANIC TRACES* MEAN? * 1
IMPORTANCE OF ORGANIC TRACE ANALYSIS * 2
PECULIARITIES WITH ORGANIC TRACE ANALYSIS * 4
ESSENTIAL MATRICES IN ORGANIC TRACE ANALYSIS * 5
AIMS OF ORGANIC TRACE ANALYSIS * 7
FURTHER READING* 8
BIBLIOGRAPHY * 9
STATISTICAL EVALUATION * 10
GENERAL REMARKS * 10
CALIBRATION FUNCTION * 10
SENSITIVITY * 11
TYPES OF ERROR * 11
LIMIT OF DETECTION/LIMIT OF QUANTIFICATION
-----
14
PRECISION * 15
ACCURACY * 15
CORRELATION AND REGRESSION * 16
FURTHER READING* 18
QUALITY CONTROL STRATEGIES * 19
GENERAL REMARKS * 19
ARTIFICIALLY GENERATED MATRIX SURROGATES * 19
ADDITION OF AN INTERNAL STANDARD * 21
VALIDATION BY APPLYING INDEPENDENT ANALYTICAL METHODS
VALIDATION BY REFERENCE MATERIAL *
26
QC BY APPLYING GOOD LABORATORY PRACTICES * 30
FURTHER READING* 31
BIBLIOGRAPHY * 31
SAMPLING OF ORGANIC TRACE CONTAMINANTS * 33
GENERAL REMARKS * 33
SAMPLING FROM ORGANISMS * 35
GENERAL REMARKS * 35
ANIMAL TISSUE SAMPLES * 36
HUMAN SAMPLES * 42
PLANT SAMPLING* 44
4.3 TRACE GAS SAMPLING
-----
46
4.3.1 GENERAL REMARKS
-----
46
4.3.2 GAS GRAB SAMPLING* 47
4.4 RAIN, SURFACE WATER AND PARTICULATE MATTER SAMPLING* 48
4.4.1 GENERAL REMARKS * 48
4.4.2 RAIN
-----
49
4.4.3 SURFACE WATER, DEEP WATER, GROUNDWATER
-----
50
4.4.4 PARTICULATE MATTER SAMPLING
-----
52
4.5 SOIL AND SEDIMENT SAMPLING
-----
54
4.5.1 GENERAL REMARKS
-----
54
4.5.2 SOIL
-----
55
4.5.3 SEDIMENT
-----
57
4.6 DIFFUSION SAMPLING (PASSIVE SAMPLING)
-----
58
4.7 SAMPLING OF COLLOIDAL MATTER (HYDROSOL, AEROSOL) * 62
4.7.1 GENERAL REMARKS * 62
4.7.2 HYDROSOL SAMPLING
-----
63
4.7.3 AEROSOL SAMPLING
-----
67
4.8 SOURCES FOR ARTIFACT FORMATION
-----
69
4.8.1 GENERAL REMARKS * 69
4.8.2 SOURCES OF ARTIFACTS * 69
FURTHER READING
-----
71
BIBLIOGRAPHY * 71
5 SAMPLE TREATMENT BEFORE ANALYSIS * 76
5.1 GENERAL REMARKS
-----
76
5.2 SAMPLE PRETREATMENT (STABILIZATION AND STORAGE) * 76
BIBLIOGRAPHY
-----
78
6 ENRICHMENT AND SAMPLE CLEANUP * 79
6.1 GENERAL REMARKS * 79
6.2 LIQUID SAMPLES (WATER, BODY FLUIDS, BEVERAGES) * 79
6.2.1 LIQUID-LIQUID EXTRACTION
-----
79
6.2.2 PRE-CONCENTRATION AFTER LLE (EVAPORATION, FREEZE-DRYING)
-----
81
6.2.3 SOLID-PHASE EXTRACTION * 83
6.2.4 SOLID-PHASE MICROEXTRACTION * 87
6.2.5 DISPERSIVE LIQUID-LIQUID MICROEXTRACTION
-----
89
6.2.6 MICELLAR EXTRACTION
-----
90
6.2.7 HEADSPACE EXTRACTION * 92
6.2.8 PURGE AND TRAP EXTRACTION * 93
6.3 SOLID SAMPLES (PARTICULATE MATTER, SOIL, SEDIMENT, PLANT AND ANIMAL
MATERIAL)
-----
94
6.3.1 SOLID-LIQUID EXTRACTION * 95
6.3.2 ASSISTED SOLID-LIQUID EXTRACTION (SOXHLET, ASE, MICROWAVE
EXTRACTION, ULTRASONICATION, SUPERCRITICAL FLUID EXTRACTION) * 97
6.3.3 ENZYMATIC DIGESTION * 106
6.3.4 NON-EXTRACTABLE RESIDUES * 107
6.3.5 STEAM DISTILLATION * 108
6.3.6 SIZE FRACTIONATION OF DISPERSED SOLID MATTER
-----
110
6.4 GASEOUS SAMPLES AND AEROSOLS * 113
6.4.1 GENERAL REMARKS
-----
113
6.4.2 LIQUID ABSORPTION OF TRACE GASES * 113
6.4.3 SOLID ADSORPTION OF TRACE GASES * 114
6.4.4 FILTRATION * 115
6.4.5 DIFFUSION SAMPLING (DENUDER SAMPLING) * 117
6.4.6 SAMPLING BY CONDENSATION * 119
6.4.7 SIZE-RESOLVED PARTICLE (AEROSOL) SAMPLING* 120
FURTHER READING * 123
BIBLIOGRAPHY * 125
7 CHROMATOGRAPHY * 129
7.1 GENERAL REMARKS * 129
7.2 CHROMATOGRAPHIC SEPARATION * 130
7.2.1 ADSORPTION CHROMATOGRAPHY * 133
7.2.2 ION-EXCHANGE CHROMATOGRAPHY * 135
7.2.3 SIZE-EXCLUSION CHROMATOGRAPHY* 137
7.3 BASICS AND WORKING PRINCIPLES * 139
7.3.1 PARAMETERS TO ACHIEVE BEST RESOLVING POWER* 140
7.3.2 GENERAL RECOMMENDATIONS * 144
7.4 HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY * 145
7.4.1 GENERAL INFORMATION * 145
7.4.2 MOBILE PHASE (HPLC)
-----
145
7.4.3 STATIONARY-PHASE MATERIALS * 151
7.4.4 COLUMNS * 156
7.4.5 HPLC DETECTORS-----158
7.4.6 SEPARATION PARAMETERS IN HPLC
-----
168
7.4.7 DERIVATIZATION METHODS (PRE-COLUMN, POST-COLUMN) IN HPLC * 170
7.4.8 HYPHENATED TECHNIQUES (HPLC-MS, HPLC-NMR) * 173
7.5 GAS CHROMATOGRAPHY * 176
7.5.1 GENERAL REMARKS
-----
176
7.5.2 SEPARATION COLUMNS AND STATIONARY PHASES (GC) * 177
7.5.3 MOBILE PHASE * 179
7.5.4 ISOTHERMAL VERSUS TEMPERATURE-PROGRAMMED GC * 181
7.5.5 INJECTION TECHNIQUES FOR GC * 182
7.5.6 GC SEPARATIONS AT EXTREME TEMPERATURES * 182
7.5.7 DERIVATIZATION TECHNIQUES IN GC
-----
184
7.5.8 CHANGE OF STATE DURING GC SEPARATION (PYROLYSIS, CARBON SKELETON
FORMATION) * 185
7.5.9 ANALYTE DETECTION IN GC (ELECTRICAL, ELECTROCHEMICAL, OPTICAL) *
186
7.5.10 HYPHENATED TECHNIQUES (GC-MS)
-----
198
7.5.11 MULTIDIMENSIONAL GC SEPARATIONS (GC
X
GC) * 201
FURTHER READING
-----
204
BIBLIOGRAPHY * 206
8 CAPILLARY ELECTROPHORESIS (CE) * 208
8.1 GENERAL REMARKS * 208
8.2 WORKING PRINCIPLES
-----
208
8.2.1 INTERACTION OF CHARGED ANALYTE SPECIES WITH AN EXTERNAL ELECTRIC
FIELD
-----
208
8.2.2 ELECTROENDOSMOTIC FLOW
-----
209
8.2.3 CONTROL OF EOF
-----
211
8.2.4 FLOW DYNAMICS, EFFICIENCY AND RESOLUTION
-----
212
8.3 MODES OF CE OPERATION * 214
8.3.1 CZE
-----
214
8.3.2 CAPILLARY GEL ELECTROPHORESIS
-----
215
8.3.3 MICELLAR ELECTROKINETIC CAPILLARY CHROMATOGRAPHY* 216
8.3.4 CAPILLARY ISOELECTRIC FOCUSING* 217
8.3.5 CAPILLARY ISOTACHOPHORESIS * 218
8.4 SAMPLE INJECTION (CE) * 219
8.4.1 HYDRODYNAMIC INJECTION * 220
8.4.2 ELECTROKINETIC INJECTION * 221
8.5 SEPARATION PARAMETERS IN CE
-----
221
8.5.1 CAPILLARY PROPERTIES AND CONDITIONING* 221
8.5.2 TEMPERATURE EFFECT IN CE
-----
222
8.5.3 ELECTRIC FIELD IN CE
-----
223
8.6 DETECTION OF ANALYTES IN CE
-----
223
8.6.1 UV-VIS DETECTION IN CE
-----
224
8.6.2 FLUORESCENCE AND CHEMILUMINESCENCE DETECTION IN CE * 224
8.6.3 AMPEROMETRIC AND CONDUCTOMETRIC DETECTION IN CE
-----
225
8.6.4 HYPHENATED TECHNIQUES (CE-MS)
-----
225
8.6.5 INDIRECT DETECTION METHODS IN CE
-----
225
8.6.6 INCREASING THE SENSITIVITY OF DETECTION IN CE
-----
226
FURTHER READING
-----
227
BIBLIOGRAPHY* 227
9 MASS SPECTROMETRY * 229
9.1 INTRODUCTION * 229
9.2 BASIC EQUIPMENT * 229
9.3 IONIZATION IN MS * 230
9.3.1 HARD IONIZATION BY ELECTRON IMPACT* 231
9.3.2 SOFT IONIZATION * 232
9.4 SEPARATION OF
M/Z SPECIES * 239
9.4.1 ONE-DIMENSIONAL MASS SEPARATION * 239
9.4.2 TWO-DIMENSIONAL MASS SEPARATION * 241
9.4.3 THREE-DIMENSIONAL MASS SEPARATION BY ION TRAP MS * 244
9.5 MOLECULAR IMAGING BY MS * 247
FURTHER READING * 247
BIBLIOGRAPHY * 248
10 RECEPTOR-BASED BIOANALYSIS FOR MASS SCREENING * 250
10.1 GENERAL REMARKS * 250
10.2 NATURAL RECEPTORS (ENZYMES AND ANTIBODIES) * 251
10.3 WORKING PRINCIPLE OF ENZYMES (ENZYMATIC CATALYSIS, ENZYMATIC
INHIBITION) * 252
10.4 WORKING PRINCIPLE OF ANTIBODIES (IA, TEST FORMAT, MICROARRAY, DIP
STICK) * 254
10.5 PRINCIPLES OF EFFECT-DIRECTED ANALYSIS * 262
FURTHER READING * 264
BIBLIOGRAPHY * 265
11 SELECTED APPLICATIONS * 269
11.1 TRACE ANALYSIS OF POLYCYCLIC AROMATIC HYDROCARBONS (PAHS) * 269
11.1.1 GENERAL REMARKS (OCCURRENCE, PHYSICAL AND CHEMICAL
PROPERTIES) * 269
11.1.2 SAMPLING STRATEGIES FOR PAHS (WATER, AIR, SOIL, BODY FLUIDS) *
271
11.1.3 WET-CHEMICAL ANALYSIS (HPLC, THIN-LAYER CHROMATOGRAPHY) * 278
11.1.4 GC ANALYSIS OF PAH
-----
282
11.1.5 IMMUNOLOGICAL BIOANALYSIS OF PAHS * 284
11.1.6 IN SITU PAH ANALYSIS BY SPECTROSCOPIC TECHNIQUES (LASER
FLUORESCENCE, PHOTOELECTRON EMISSION)
-----
288
11.2 POLYCHLORINATED BIPHENYLS, DIBENZODIOXINS AND -FURANS
-----
293
11.2.1 GENERAL REMARKS ON OCCURRENCE AND IMPORTANCE * 293
11.2.2 SAMPLING STRATEGIES FOR POLYHALOGENATED AROMATIC
HYDROCARBONS * 297
11.2.3 GC ANALYSIS OF PCDDS/PCDFS AND PCBS
-----
299
11.2.4 BIOANALYTICAL METHODS FOR PCDD/PCDF AND PCB SCREENING * 304
11.3 ORGANOPHOSPHORUS COMPOUNDS * 310
11.3.1 GENERAL REMARKS ON OCCURRENCE AND IMPORTANCE * 310
11.3.2 SAMPLING STRATEGIES FOR OPS (WATER, SOIL, AIR, BODY FLUID, FOOD
AND NUTRACEUTICALS, LIVING TISSUE) * 314
11.3.3 GC ANALYSIS OF OPS
-----
318
11.3.4 WET-CHEMICAL ANALYSIS OF OPS (HPLC-MS, TLC, CAPILLARY
ELECTROPHORESIS) * 319
11.3.5 BIOANALYSIS OF OPS * 324
FURTHER READING: POLYCYCLIC AROMATIC HYDROCARBONS * 334
FURTHER READING: POLYCHLORINATED BIPHENYLS (PCBS), DIBENZODIOXINS
(PCDDS) AND -FURANS (PCDFS)
-----
335
FURTHER READING: ORGANOPHOSPHATES
-----
335
BIBLIOGRAPHY
-----
335
LIST OF ABBREVIATIONS* 347
INDEX* 351
|
| any_adam_object | 1 |
| author | Nießner, Reinhard 1951- Schäffer, Andreas 1955- |
| author_GND | (DE-588)141829591 (DE-588)1082260932 |
| author_facet | Nießner, Reinhard 1951- Schäffer, Andreas 1955- |
| author_role | aut aut |
| author_sort | Nießner, Reinhard 1951- |
| author_variant | r n rn a s as |
| building | Verbundindex |
| bvnumber | BV044449330 |
| classification_rvk | VG 6800 VG 6801 WK 2200 |
| classification_tum | CHE 208 |
| ctrlnum | (OCoLC)1005875886 (DE-599)DNB112102341X |
| dewey-full | 540 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 540 - Chemistry and allied sciences |
| dewey-raw | 540 |
| dewey-search | 540 |
| dewey-sort | 3540 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Biologie Chemie |
| format | Book |
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| id | DE-604.BV044449330 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T07:53:16Z |
| institution | BVB |
| institution_GND | (DE-588)10095502-2 |
| isbn | 9783110441147 3110441144 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-029850294 |
| oclc_num | 1005875886 |
| open_access_boolean | |
| owner | DE-703 DE-92 DE-634 DE-11 DE-83 DE-91G DE-BY-TUM |
| owner_facet | DE-703 DE-92 DE-634 DE-11 DE-83 DE-91G DE-BY-TUM |
| physical | XII, 357 Seiten Illustrationen, Diagramme (farbig) |
| publishDate | 2017 |
| publishDateSearch | 2017 |
| publishDateSort | 2017 |
| publisher | De Gruyter |
| record_format | marc |
| series2 | De Gruyter graduate |
| spelling | Nießner, Reinhard 1951- Verfasser (DE-588)141829591 aut Organic trace analysis Niessner, Schäffer Berlin ; Boston De Gruyter [2017] © 2017 XII, 357 Seiten Illustrationen, Diagramme (farbig) txt rdacontent n rdamedia nc rdacarrier De Gruyter graduate Organischer Schadstoff (DE-588)4172787-3 gnd rswk-swf Spurenanalyse (DE-588)4056593-2 gnd rswk-swf Umweltanalytik (DE-588)4282985-9 gnd rswk-swf Organischer Stoff (DE-588)4203832-7 gnd rswk-swf Organischer Stoff (DE-588)4203832-7 s Organischer Schadstoff (DE-588)4172787-3 s Spurenanalyse (DE-588)4056593-2 s DE-604 Umweltanalytik (DE-588)4282985-9 s Schäffer, Andreas 1955- Verfasser (DE-588)1082260932 aut Walter de Gruyter GmbH & Co. KG (DE-588)10095502-2 pbl Erscheint auch als Online-Ausgabe, PDF 978-3-11-044115-4 Erscheint auch als Online-Ausgabe, EPUB 978-3-11-043293-0 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029850294&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Nießner, Reinhard 1951- Schäffer, Andreas 1955- Organic trace analysis Organischer Schadstoff (DE-588)4172787-3 gnd Spurenanalyse (DE-588)4056593-2 gnd Umweltanalytik (DE-588)4282985-9 gnd Organischer Stoff (DE-588)4203832-7 gnd |
| subject_GND | (DE-588)4172787-3 (DE-588)4056593-2 (DE-588)4282985-9 (DE-588)4203832-7 |
| title | Organic trace analysis |
| title_auth | Organic trace analysis |
| title_exact_search | Organic trace analysis |
| title_full | Organic trace analysis Niessner, Schäffer |
| title_fullStr | Organic trace analysis Niessner, Schäffer |
| title_full_unstemmed | Organic trace analysis Niessner, Schäffer |
| title_short | Organic trace analysis |
| title_sort | organic trace analysis |
| topic | Organischer Schadstoff (DE-588)4172787-3 gnd Spurenanalyse (DE-588)4056593-2 gnd Umweltanalytik (DE-588)4282985-9 gnd Organischer Stoff (DE-588)4203832-7 gnd |
| topic_facet | Organischer Schadstoff Spurenanalyse Umweltanalytik Organischer Stoff |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029850294&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT nießnerreinhard organictraceanalysis AT schafferandreas organictraceanalysis AT walterdegruytergmbhcokg organictraceanalysis |