Characterisation methods in inorganic chemistry:
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| Hauptverfasser: | , |
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| Format: | Buch |
| Sprache: | English |
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Oxford
Oxford University Press
[2017]
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| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | xvi, 320 Seiten Illustrationen, Diagramme |
| ISBN: | 9780199654413 |
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Datensatz im Suchindex
| _version_ | 1804177730285076480 |
|---|---|
| adam_text | Titel: Characterisation methods in inorganic chemistry
Autor: Weller, Mark T
Jahr: 2017
Detailed Contents
Preface
About the Book
About the Online Resource Centre
Acknowledgements
Acronyms and abbreviations
v
vi
vii
viii
XV
CHAPTER1 Fundamental aspects of characterisation
methods in inorganic chemistry
1.1 Introduction 1
1.2 Units and energy unit conversions 2
1.2.1 Units of distance and atomic Separation 2
1.2.2 Wavelength, frequency, and energy 2
1.2.3 Electronvolts 2
1.2.4 Wavenumbers 3
1.2.5 NMR energy units 4
1.3 The electromagnetic spectrum and spectroscopy 4
1.3.1 The electromagnetic spectrum and transitions
between energy levels in atoms 5
1.3.2 The generation of electromagnetic radiation 5
1.4 Timescales of characterisation methods 6
1.4.1 Diffraction 6
1.4.2 Spectroscopic methods 7
1.4.3 Introduction to exchange processes 7
1.5 Fourier transforms in spectroscopy 9
1.6 Experimental considerations—information,
experimental times, and sample requirements 11
1.6.1 Quantities required and experimental times 11
1.6.2 Sample form and recovery H
1.6.3 Availability of instrumentation 11
1.6.4 Choosing a suitable technique 12
1.6.5 Research facilities and instrumentation 13
1.7 Layout of the book 18
Problems ig
Bibliography ig
CHAPTER 2 Diffraction methods and crystaliography
Fundamentals
2.1 Introduction to diffraction
2.2 Unit cells, lattices, and the description of
crystal structures
2.3 Lattice planes and Miller Índices
2.4 Relationship between Miller Índices and
cf-spacing
20
20
21
26
28
Advanced diffraction techniques
2.16 Powder X-ray diffraction
2.16.1 Analysis of PXD data from tetragonal and
hexagonal Systems
2.16.2 Crystallite size from PXD data
2.16.3 Neutron powder diffraction
2.16.4 PXD intensities and füll diffraction
profile analysis
29
31
31
33
33
35
35
36
2.5 Scattering of X-rays by crystalIine solids:
Bragg s law and the Bragg equation
2.6 The powder X-ray diffraction experimental
method
2.6.1 Sources of X-rays
2.6.2 Data collection
2.6.3 Experimental methods
2.7 Applications of powder X-ray diffraction
2.7.1 Phase identification
2.7.2 Forensic applications and phase identification
of unknowns
2.7.3 Determination of phase purity, following
reactions to completion, and phase diagrams 36
2.7.4 Phase changes and thermal expansión 37
2.7.5 Quantitative analysis and quality control 38
2.8 Powder X-ray diffraction data analysis 38
2.8.1 Indexing powder diffraction patterns from
cubic Systems 38
2.9 Lattice type and systematic absences 40
2.9.1 The origin of systematic absences 40
2.9.2 Indexing data from I- and
F-centred lattices
2.10 Extracting simple structural information using
PXD data from cubic materials
2.11 The single-crystal X-ray diffraction
technique—introduction
2.12 Reflection intensities and structure factors
in X-ray diffraction 46
2.13 Structure Solution from single-crystal X-ray
diffraction data 49
2.13.1 Obtaining suitable single crystals 49
2.13.2 Instrumentation and collection of
diffraction data 99
2.14 Solving the structure from single-crystal
diffraction data 50
2.14.1 The Patterson synthesis
2.14.2 Direct methods
2.14.3 Completing the structure
2.15 Crystallographic information from single-crystal
X-ray diffraction
Problems 55
57
57
41
44
45
53
53
57
59
60
62
2.17 Single-crystal diffraction
2.17.1 Single-crystal neutrón diffraction
2.17.2 Electron density and X-n maps
2.17.3 Amorphous materials, total diffraction,
and pair distribution function analysis
Bibliography
CHAPTER 3 Nuclear magnetic resonance (NMR)
spectroscopy
Fundamentals
3.1 Introduction to NMR spectroscopy
3.2 The basis of the NMR technique
3.2.1 Nuclear magnetic moments
3.2.2 Energy levels for NMR spectroscopy
3.2.3 Sensitivity of the NMR technique
3.2.4 Energy levels, frequencies, and the NMR nucleus
3.3 Experiment and Instrumentation
3.4 Chemical shifts
3.5 Chemical shift and environment
3.6 Intensities
3.7 First-order spin-spin coupling or scalar coupling
3.7.1 Origins of spin-spin coupling
3.7.2 First-order spin-spin coupling for
two heteronuclear I=Yi nuclei
3.7.3 Spin-spin coupling nomenclature, coupling
strengths, and interaction distances
3.7.4 First-order heteronuclear coupling in
AX„ Systems, n 1
3.7.5 Homonuclear coupling
3.7.6 First-order coupling to spin I lh nuclei
3.8 Magnitudes of coupling constants
3.9 Decoupling and decoupled spectra
3.10 Effects due to variations in natural
abundance—isotopomers
3.11 Introduction to fluxionality
Problems
Advanced topics
3.12 Factors determining chemlcal shift
3.12.1 Oxidation State, molecular ion Charge, and
electronegativity
3.12.2 Coordination number
3.12.3 Other influences on chemical shift
3.13 Trends in coupling constants
3.14 Second-order coupling
3.15 Chemical and magnetic equivalence and
inequivalence
3.16 Relaxation and relaxation times: quadrupolar
nuclei in NMR
3.17 The NMR timescale, site exchange,
and fluxionality
Detailed Contents xi
63 3.18 Advanced NMR techniques and experiments:
63 INEPT and COSY 102
63 3.18.1 INEPT 102
3.18.2 COSY NMR spectra 103
54 3.19 Solid-state NMR 105
65 3.20 Applications of MASNMR 107
3.21 Other advanced techniques in MASNMR 110
3.22 Quantitative NMR (qNMR) and analysis 110
Bibliography 111
66
66 CHAPTER 4 Vibrational spectroscopy
67
67
Fundamentáis
112
71
4.1
Introduction to vibrational spectroscopy
112
72
73
4.1.1 Underlying theory
112
4.1.2 Selection rules
113
74
4.1.3 Number of vibrational modes
114
75
4.1.4 Normal modes of Vibration
114
77
4.2
Experimental considerations
115
78
4.2.1 IR spectrometers
115
79
4.2.2 Raman spectrometers
116
4.2.3 IR and Raman sampling
117
79
4.2.4 IR and Raman microscopy
119
79
4.3
Qualitative considerations
119
4.3.1 X-H groups and hydrogen bonds
119
81
4.3.2 Functional groups in organometallic
complexes
120
82
4.3.3 IR data for common anions
121
85
4.3.4 Compounds and complexes containing
86
oxo and nitrido groups
121
87
4.3.5 Complexes with halide ligands
122
4.3.6 Complexes with carbonyl ligands
122
88
4.3.7 Complexes with dinitrogen as a ligand
4.3.8 Complexes with dioxygen as a ligand
124
124
90
4.3.9 Complexes with nitrosyl ligands
125
91
4.3.10 Complexes with Cyanide, cyanate,
thiocyanate, and selenocyanate ligands
125
93
4.3.11 Complexes with nitrite ligands
125
94
4.4
Applications of group theory to vibrational
94
spectroscopy
4.4.1 Symmetry Operations and symmetry
126
94
elements
126
95
4.4.2 Point groups
131
95
4.4.3 Determining point groups
131
95
4.4.4 Character tables
134
4.4.5 A more rigorous approach to
96
selection rules
4.4.6 Intensities
135
136
97
4.4.7 Mutual exclusión principie
4.4.8 Reducible and irreducible representations
136
137
99
4.4.9 Determining reducible and irreducible
representations for stretching modes, Fslr
4.4.10 Checking calculations
139
142
100
4.4.11 Carbonyl and dinitrogen complexes
143
xii Detailed Contents
4.4.12 Analysis of metal carbonyl IR spectra
4.4.13 Analysis of all vibrational modes, r„^
and
4.4.14 Labelling and assigning of vibrational modes
143
146
150
151
152
152
Problems
Advanced topics in vibrational spectroscopy
4.5 Advanced topics in Raman spectroscopy
4.5.1 Applications of Polarisation in
Raman spectroscopy 152
4.5.2 Advanced Raman techniques 153
4.6 Advanced applications of group theory in
vibrational spectroscopy 155
4.6.1 Direct producís—application to overtones and
combinations in vibrational spectroscopy 155
4.6.2 Direct products—application to selection rules 157
4.6.3 Descent of symmetry and correlation
diagrams— application to calcite and
aragonite IR spectra 157
4.6.4 for linear molecules 159
4.6.5 Fermi resonance 159
4.6.6 Protection Operators and symmetry
coordinates to visualise vibrational modes
Bibliography
CHARTER 5 Electronic absorption and wnisskMi
spectroscopy
160
162
5.1
5.2
5.3
5.4
5.5
Fundamentáis
Introduction
Experimental UV-vis spectroscopy
Types of electronic transitions in inorganic
Compounds and complexes
Selection rules and absorption intensities in
UV-vis spectroscopy
5.4.1 Spin selection rule
5.4.2 Dipole selection rules
5.4.3 Relaxation of selection rules
5.4.4 Typical UV-vis intensities in transition
metal Compounds
d-d electronic transitions in transition metal
complexes
5.6
5.6.5 Intervalence (or metal to metal) charge
transfer (IVCT) transitions
5.7 Intra-Iigand transitions
5.8 Electronic transitions in other inorganic
materials
5.9 f-f electronic transitions in lanthanides
Problems
Advanced topics
5.10 Configurations, terms, and levels
5.10.1 Hunds rules
5.10.2 Atomic terms for p*. d , and f
conñgurations
5.10.3 Ordering of levels with terms
5.11 Emission spectroscopy
5.12 Lanthanide emission spectra—atomic
spectra in Solution
5.12.1 Ligand-enhanced lanthanide luminescence
5.13 Advanced d-d spectroscopy
5.13.1 Octahedral and tctrahedral ground terms
5.13.2 F.xcited State terms
5.13.3 Racah parameters
5.13.4 Orgel diagrams
5.13.5 Tanabe-Sugano diagrams
5. i 3.6 Summary of the analysis of UV-vis spectra
from first row transition metal ions
5.14 Nephelauxetic effect
Bibliography
183
184
184
184
185
185
185
187
187
188
188
189
189
191
191
193
194
194
196
203
203
205
163
163
164
167
167
168
168
169
169
170
CHARTER 8 X-riy and piwto«ÍBCtroB spoctrocopy,
•Itctron microscopy, and Mttrxy disptrsi*« analysis
oi x-rsys
5.5.1 Common colours of transition metal complexes 170
5.5.2 d-d spectra of 3d element complexes 171
5.5.3 The spectrochemical series 177
Charge transfer transitions in transition metal
complexes and Compounds 179
5.6.1 Ligand to metal Charge transfer (LMCT)
transitions 179
5.6.2 Characterisation of pigments, semiconductora,
and band gaps 181
5.6.3 Metal to ligand Charge transfer (MI.CT)
transitions 182
5.6.4 Optical electronegativities 182
6.1
6.2
6.3
6.4
6.5
6.6
6.7
Introduction to photoelectron spectroscopy
X-ray photoelectron spectroscopy (XPS)
Techniques related to XPS
6.3.1 Electron spectroscopy for chemical analysis
(ESCA)
6.3.2 Auger spectroscopy with X-ray excitation
Ultraviolet photoelectron spectroscopy (UPS)
6.4.1 Experimental considerations
6.4.2 UPS spectrum of CO
6.4.3 Applications of UPS
X-ray absorption spectroscopy
6.5.1 X-ray absorption measurements: absorption
and relaxation processes
6.5.2 XANES
6.5.3 Pre-edge features
6.5.4 EXAFS
Introduction to electrón microscopy and
energy dispersive analysis of X-rays
Scanning electrón microscopy (SEM)
206
207
208
208
209
209
210
210
210
211
211
212
212
213
216
217
Detailed Contents xiii
6.7.1 Sample preparation and environmental
SEM (ESEM) 218
6.7.2 EDAXandEDS 218
6.7.3 Auger spectroscopy in electrón microscopy 219
6.8 Transmission electrón microscopy (TEM) 219
6.8.1 TEM sample preparation and mounting 220
6.8.2 Bright field image 220
6.8.3 Diffraction in TEM 220
Problems 221
Bibliography 221
CHAPTER 7 Mass spectrometry, chemical, and
thermal analysis techniques
7.1 Introduction: compositional and thermal
analysis 222
7.2 Mass spectrometry of inorganic Compounds 222
7.2.1 Experiment basis and Instrumentation 222
7.2.2 Interpretation of mass spectral data from
inorganic and organometallic Compounds 224
7.2.3 Example applications in inorganic chemistry 226
7.2.4 Combined mass spectrometry analysis
methods 227
7.3 CHN, sulfur, and oxygen analysis 228
7.4 Atomic absorption spectroscopy, flame
emission spectroscopy, and flame photometry 229
7.4.1 Atomic absorption spectroscopy 229
7.4.2 Flame emission spectroscopy and
flame photometry 230
7.4.3 ICP-MS 231
7.5 Thermal analysis 231
7.5.1 Thermogravimetric analysis 231
7.5.2 Differential thermal analysis and
differential scanning calorimetry 232
7.5.3 Combined thermal analysis and
mass spectrometry 233
7.5.4 Melting point apparatus and hot
stage microscopes 234
7.5.5 Other thermal analysis methods 234
Problems 235
Bibliography 236
CHAPTER 8 Magnstism
8.1 Magnetometry 237
8.1.1 Magnetic moment instrumentation 237
8.1.2 Initial analysis of experimental
magnetisation data 238
8.2 Interpretation of magnetic moment,
valúes 240
8.2.1 The spin-only formula 240
8.2.2 Qualitative treatment of orbital
contributions and temperature-dependent
paramagnetism 242
8.2.3 Spin-crossover complexes and temperature-
independent paramagnetism (TIP) 243
8.2.4 Orbital contributions to magnetic moments 243
8.3 Cooperative magnetism 248
Problems 249
Bibliography 250
CHARTER 9 Electron parwnapHc mmnca (EPR)
spectroscopy
9.1 Introduction to EPR spectroscopy 251
9.2 Experimental considerations for
EPR spectroscopy 251
9.3 Information available from EPR spectra 252
9.3.1 Theg-value 252
9.3.2 Hyperfine coupling constant, A 256
9.4 Limitations of EPR spectroscopy 258
9.5 Applications of EPR spectroscopy 259
9.5.1 Main group examples 259
9.5.2 Transition metal examples 259
9.5.3 S Vi Systems 263
Problems 263
Bibliography 265
CHARTER 18 Mössbauer spectioscopy «Hl
nuclear quadruple resonance (MSR)
spectroscopy
10.1 Mössbauer spectroscopy 266
10.1.1 Introduction to Mössbauer spectroscopy 266
10.1.2 Experimental requirements for Mössbauer
spectroscopy 266
10.1.3 Information available from Mössbauer
spectra 268
10.1.4 Elemental ränge in Mössbauer
spectroscopy 274
10.1.5 Applications of Mössbauer spectroscopy
to elements other than iron 275
10.2 Nuclear quadrupole resonance (NQR)
spectroscopy 276
10.2.1 Introduction to NQR spectroscopy 276
10.2.2 Experimental considerations for
NQR spectroscopy 276
10.2.3 Underlying NQR theory 276
10.2.4 Information determined from NQR
spectra 277
10.2.5 Range of elements for, and limitations of,
NQR spectroscopy 278
xiv Detailed Contents
10.2.6 Analysis of NQR data 278
Problems 279
Bibliography 281
CHAPTER11 Characterisation of inorganic
Compounds: example Problems with multiple
techniques
Problem 11.1 Multinuclear NMR spectroscopy and
mass spectrometry 282
Problem 11.2 Powder X-ray diffraction and
multinuclear NMR 283
Problem 11.3 Electronic spectroscopy and magnetism 284
Problem 11.4 UV-vis spectroscopy and magnetism 285
Problem 11.5 Powder X-ray diffraction and thermal
analysis/mass spectrometry 286
Problem 11.6 IR spectroscopy and chemical
composition analysis 287
Problem 11.7 Elemental analysis, IR and Raman
spectroscopy, EPR spectroscopy, and
magnetic data 288
Problem 11.8 Crystallography, EPR, EXAFS, and
technique timescales 288
Problem 11.9 Mössbauer spectroscopy, magnetic
moments, and electronic absorption
spectroscopy 289
Problem 11.10 Multinuclear NMR, IR and
Raman spectroscopies, and
main group chemistry 289
Appendix 1 Character tables 293
Appendix 2 Table of direct products 299
Appendix 3 Correlation tables 301
Appendix 4 Tanabe-Sugano diagrams and
Lever plots 305
Index 311
Formula index 317
|
| any_adam_object | 1 |
| author | Weller, Mark T. 1960- Young, Nigel 1938- |
| author_GND | (DE-588)1082004251 (DE-588)129615161 |
| author_facet | Weller, Mark T. 1960- Young, Nigel 1938- |
| author_role | aut aut |
| author_sort | Weller, Mark T. 1960- |
| author_variant | m t w mt mtw n y ny |
| building | Verbundindex |
| bvnumber | BV044429586 |
| classification_rvk | VG 5150 |
| ctrlnum | (OCoLC)1000314877 (DE-599)HBZHT019307795 |
| discipline | Chemie / Pharmazie |
| format | Book |
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| genre | (DE-588)4123623-3 Lehrbuch gnd-content |
| genre_facet | Lehrbuch |
| id | DE-604.BV044429586 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T07:52:43Z |
| institution | BVB |
| isbn | 9780199654413 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-029831008 |
| oclc_num | 1000314877 |
| open_access_boolean | |
| owner | DE-11 DE-19 DE-BY-UBM |
| owner_facet | DE-11 DE-19 DE-BY-UBM |
| physical | xvi, 320 Seiten Illustrationen, Diagramme |
| publishDate | 2017 |
| publishDateSearch | 2017 |
| publishDateSort | 2017 |
| publisher | Oxford University Press |
| record_format | marc |
| spelling | Weller, Mark T. 1960- Verfasser (DE-588)1082004251 aut Characterisation methods in inorganic chemistry Mark T. Weller, Nigel Young Oxford Oxford University Press [2017] © 2017 xvi, 320 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Fourier-Transformierte (DE-588)4798599-9 gnd rswk-swf Schwingungsspektroskopie (DE-588)4128960-2 gnd rswk-swf Infrarotspektroskopie (DE-588)4135411-4 gnd rswk-swf Koordinationslehre (DE-588)4133952-6 gnd rswk-swf Röntgenstrukturanalyse (DE-588)4137203-7 gnd rswk-swf Chemische Bindung (DE-588)4009843-6 gnd rswk-swf MAS-NMR-Spektroskopie (DE-588)4306914-9 gnd rswk-swf Charakter Topologie (DE-588)4392712-9 gnd rswk-swf Chemie (DE-588)4009816-3 gnd rswk-swf Spektroskopie (DE-588)4056138-0 gnd rswk-swf Charakterisierung (DE-588)4069926-2 gnd rswk-swf Kristallographie (DE-588)4033217-2 gnd rswk-swf Magnetische Kernresonanz (DE-588)4037005-7 gnd rswk-swf Übergangsmetallatom (DE-588)4406105-5 gnd rswk-swf Raman-Spektroskopie (DE-588)4176916-8 gnd rswk-swf Substanz (DE-588)4202257-5 gnd rswk-swf Punktgruppe (DE-588)4176373-7 gnd rswk-swf Pulvermethode (DE-588)4176353-1 gnd rswk-swf Einkristall (DE-588)4013901-3 gnd rswk-swf (DE-588)4123623-3 Lehrbuch gnd-content Chemie (DE-588)4009816-3 s Substanz (DE-588)4202257-5 s Charakterisierung (DE-588)4069926-2 s Spektroskopie (DE-588)4056138-0 s DE-604 Fourier-Transformierte (DE-588)4798599-9 s Kristallographie (DE-588)4033217-2 s Röntgenstrukturanalyse (DE-588)4137203-7 s Einkristall (DE-588)4013901-3 s Pulvermethode (DE-588)4176353-1 s Magnetische Kernresonanz (DE-588)4037005-7 s MAS-NMR-Spektroskopie (DE-588)4306914-9 s Schwingungsspektroskopie (DE-588)4128960-2 s Infrarotspektroskopie (DE-588)4135411-4 s Punktgruppe (DE-588)4176373-7 s Charakter Topologie (DE-588)4392712-9 s Raman-Spektroskopie (DE-588)4176916-8 s Chemische Bindung (DE-588)4009843-6 s Übergangsmetallatom (DE-588)4406105-5 s Koordinationslehre (DE-588)4133952-6 s Young, Nigel 1938- Verfasser (DE-588)129615161 aut HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029831008&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Weller, Mark T. 1960- Young, Nigel 1938- Characterisation methods in inorganic chemistry Fourier-Transformierte (DE-588)4798599-9 gnd Schwingungsspektroskopie (DE-588)4128960-2 gnd Infrarotspektroskopie (DE-588)4135411-4 gnd Koordinationslehre (DE-588)4133952-6 gnd Röntgenstrukturanalyse (DE-588)4137203-7 gnd Chemische Bindung (DE-588)4009843-6 gnd MAS-NMR-Spektroskopie (DE-588)4306914-9 gnd Charakter Topologie (DE-588)4392712-9 gnd Chemie (DE-588)4009816-3 gnd Spektroskopie (DE-588)4056138-0 gnd Charakterisierung (DE-588)4069926-2 gnd Kristallographie (DE-588)4033217-2 gnd Magnetische Kernresonanz (DE-588)4037005-7 gnd Übergangsmetallatom (DE-588)4406105-5 gnd Raman-Spektroskopie (DE-588)4176916-8 gnd Substanz (DE-588)4202257-5 gnd Punktgruppe (DE-588)4176373-7 gnd Pulvermethode (DE-588)4176353-1 gnd Einkristall (DE-588)4013901-3 gnd |
| subject_GND | (DE-588)4798599-9 (DE-588)4128960-2 (DE-588)4135411-4 (DE-588)4133952-6 (DE-588)4137203-7 (DE-588)4009843-6 (DE-588)4306914-9 (DE-588)4392712-9 (DE-588)4009816-3 (DE-588)4056138-0 (DE-588)4069926-2 (DE-588)4033217-2 (DE-588)4037005-7 (DE-588)4406105-5 (DE-588)4176916-8 (DE-588)4202257-5 (DE-588)4176373-7 (DE-588)4176353-1 (DE-588)4013901-3 (DE-588)4123623-3 |
| title | Characterisation methods in inorganic chemistry |
| title_auth | Characterisation methods in inorganic chemistry |
| title_exact_search | Characterisation methods in inorganic chemistry |
| title_full | Characterisation methods in inorganic chemistry Mark T. Weller, Nigel Young |
| title_fullStr | Characterisation methods in inorganic chemistry Mark T. Weller, Nigel Young |
| title_full_unstemmed | Characterisation methods in inorganic chemistry Mark T. Weller, Nigel Young |
| title_short | Characterisation methods in inorganic chemistry |
| title_sort | characterisation methods in inorganic chemistry |
| topic | Fourier-Transformierte (DE-588)4798599-9 gnd Schwingungsspektroskopie (DE-588)4128960-2 gnd Infrarotspektroskopie (DE-588)4135411-4 gnd Koordinationslehre (DE-588)4133952-6 gnd Röntgenstrukturanalyse (DE-588)4137203-7 gnd Chemische Bindung (DE-588)4009843-6 gnd MAS-NMR-Spektroskopie (DE-588)4306914-9 gnd Charakter Topologie (DE-588)4392712-9 gnd Chemie (DE-588)4009816-3 gnd Spektroskopie (DE-588)4056138-0 gnd Charakterisierung (DE-588)4069926-2 gnd Kristallographie (DE-588)4033217-2 gnd Magnetische Kernresonanz (DE-588)4037005-7 gnd Übergangsmetallatom (DE-588)4406105-5 gnd Raman-Spektroskopie (DE-588)4176916-8 gnd Substanz (DE-588)4202257-5 gnd Punktgruppe (DE-588)4176373-7 gnd Pulvermethode (DE-588)4176353-1 gnd Einkristall (DE-588)4013901-3 gnd |
| topic_facet | Fourier-Transformierte Schwingungsspektroskopie Infrarotspektroskopie Koordinationslehre Röntgenstrukturanalyse Chemische Bindung MAS-NMR-Spektroskopie Charakter Topologie Chemie Spektroskopie Charakterisierung Kristallographie Magnetische Kernresonanz Übergangsmetallatom Raman-Spektroskopie Substanz Punktgruppe Pulvermethode Einkristall Lehrbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029831008&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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