Verfügbarkeit: Analysis and development of a direct alcohol fuel cell system

Analysis and development of a direct alcohol fuel cell system:

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Bibliographische Detailangaben
1. Verfasser:	Reeb, Berthold Benedikt Lothar (VerfasserIn)
Format:	Abschlussarbeit Buch
Sprache:	English
Veröffentlicht:	München 2017
Schlagworte:	Hochschulschrift
Online-Zugang:	Inhaltsverzeichnis
Beschreibung:	xxiii, 163 Seiten Illustrationen, Diagramme
ISBN:	9783945380123

Internformat

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Datensatz im Suchindex

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adam_text	C ONTENTS C ON TEN TS V LIST O F F IGURES VIII LIST O F TABLES X V A B B REV IA TIO N S XV! P H Y SICA L C O N STA N TS X IX S YM B O LS X X 1 IN TRO D U CTIO N 1 2 F U N D AM EN TALS 4 2.1 FUEL C E L L S .......................................................................................................... 5 2.1.1 EFFICIENCY: FUEL CELL AND HEAT E N G IN E .............................................. 8 2.2 FUELS FOR FUEL C ELLS............................................................................................ 11 2.2.1 THERMODYNAMIC POTENTIALS IN ELECTROCHEMISTRY[ 1 - 3 ] .................... 13 2.2.2 KINETICS IN A FUEL C E L L ........................................................................ 16 2.3 KINETICS OF A DIRECT ETHANOL FUEL C E L L ......................................................... 23 2.4 CATALYSTS FOR A DIRECT ETHANOL FUEL C E L L ...................................................... 27 2.4.1 ETHANOL OXIDATION AT THE ANODE OF A DIRECT ETHANOL FUEL CELL . . 27 2.4.2 THE OXYGEN REDUCTION REACTION AT THE CATHODE OF A FUEL CELL . . 31 2.5 CONVERSION OF ETHANOL TO E LE C TRIC ITY ............................................................ 33 2.6 HIGHLY INTEGRATED DIRECT ETHANOL FUEL CELL SYSTEM AT INTERMEDIATE TEM PERATURES ............................................................................................................. 35 2.7 SYSTEM ANALYSIS - ELECTRIC VEHICLE WITH AN INTERMEDIATE TEMPERATURE- DIRECT ETHANOL FUEL C E L L ................................................................................ 37 2.7.1 BALANCE OF PLANT OF AN INTERMEDIATE TEMPERATURE DIRECT ETHANOL FUEL CELL SYSTEM ................................................................................... 38 2.8 MATERIALS FOR INTERMEDIATE TEMPERATURE FUEL C ELLS ..................................... 40 2.8.1 ELECTROLYTES AND M EMBRANES............................................................... 40 2.8.2 SUPPORTS FOR FUEL CELL C A TA LY S TS ...................................................... 45 3 E XP ERIM EN TA L 47 3.1 EXPERIMENTAL T ECHNIQUES................................................................................ 48 3.1.1 THERMOGRAVIMETRIC ANALYSIS ............................................................ 48 3.1.2 MASS SPECTROMETRIC D ETECTION ............................................................ 48 3.1.3 ELEMENTARY A N A LY S IS ........................................................................... 49 3.1.4 POWDER X-RAY DIFFRACTION .................................................................. 49 3.1.5 SCANNING ELECTRON MICROSCOPY AND ENERGY DISPERSE SPECTROSCOPY 51 3.1.6 ELECTROCHEMICAL IMPEDANCE SPECTROSCOPY ........................................ 52 3.1.7 ELECTROCHEMICAL CHARACTERIZATION M E TH O D S ..................................... 57 3.2 CHEMICALS, MATERIALS AND G A S E S ..................................................................... 61 3.3 SET-UP - ELECTROLYTE P REPARATIO N ..................................................................... 62 3.4 COMPOSITE ASIO.STIO.OEPP-PBI INTERMEDIATE TEMPERATURE-FUEL CELL MEM BRANE P RE P A RA TIO N ............................................................................................ 64 3.4.1 ALTERNATIVE COMPOSITE MEMBRANE PREPARATION ROUTE WITH THE 826 PBI S O LU TIO N ......................................................................................... 67 3.5 MEA PREPARATION WITH ASIO.ZTIO.ZPP-PBI M EM B RAN ES............................. 68 3.5.1 COMMERCIAL HT-PEM FUEL CELL-ELECTRODES ..................................... 68 3.5.2 NON-COMMERCIAL ELECTRODES FOR INTERMEDIATE TEMPERATURES .... 70 3.5.3 ALTERNATIVE ROUTES TO PREPARE AN ELECTROCATALYTIC ELECTRODE. . . . 71 3.6 SET-UP - T E S TS TA N D ............................................................................................ 73 4 R ESU LTS 76 4.1 CHARACTERIZATION OF THE ELECTROLYTE ASIO.5TIO.5PP ..................................... 77 4.1.1 X-RAY DIFFRACTION ANALYSIS OF ASIO.5TIO.5PP ..................................... 77 4.1.2 ELEMENTAL ANALYSIS OF ASIO.5TIO.5PP................................................. 78 4.1.3 SCANNING ELECTRON MICROSCOPY AND ENERGY DISPERSE SPECTROSCOPY OF A S IO .5 T IO .5 P P ................................................................................... 79 4.2 CHARACTERIZATION OF THE ASIO.STIO.SPP-PBI M EM B RAN ES............................. 80 4.2.1 SCANNING ELECTRON MICROSCOPY AND ENERGY DISPERSE SPECTROSCOPY OF A ASIO.STIO.OEPP-PBI M EM B RAN E.................................................... 80 4.2.2 THERMOGRAVIMETRIC ANALYSIS OF ASITIPP-PBI MEMBRANES WITHOUT PLASTICIZER .............................................................................................. 81 4.2.3 THERMOGRAVIMETRIC ANALYSIS OF A ASITIPP-PBI MEMBRANE WITH PLASTICIZER .............................................................................................. 84 4.3 CHARACTERIZATION OF THE PLATINUM-TIN C A TA LY S T ........................................... 86 4.3.1 X-RAY DIFFRACTION ANALYSIS OF THE UNSUPPORTED PLATINUM-TIN CAT ALYST ....................................................................................................... 86 4.3.2 SCANNING ELECTRON MICROSCOPY AND ENERGY DISPERSE SPECTROSCOPY OF THE UNSUPPORTED PLATINUM-TIN C A TA LY S T ............................. 87 4.4 CHARACTERIZATION OF THE PLATINUM-RHODIUM CATALYST ............................... 89 4.4.1 X-RAY DIFFRACTION ANALYSIS OF THE UNSUPPORTED PLATINUM-RHODIUM C A TA LY ST......................................................................................... 89 4.4.2 SCANNING ELECTRON MICROSCOPY AND ENERGY DISPERSE SPECTROSCOPY OF THE UNSUPPORTED PLATINUM-RHODIUM C ATALY ST .................... 90 4.5 CHARACTERIZATION OF THE PLATINUM-RUTHENIUM C A T A L Y S T ............................. 91 4.5.1 X-RAY DIFFRACTION ANALYSIS OF THE UNSUPPORTED PLATINUM-RUTHENIUM C A TALY ST........................................................................................ ... 91 4.5.2 SCANNING ELECTRON MICROSCOPY AND ENERGY DISPERSE SPECTROSCOPY OF THE UNSUPPORTED PLATINUM-RUTHENIUM CATALYST ................ 92 4.6 FUEL CELL T E S T S ................................................................................................. 94 4.6.1 ADVENT HT-PEM MEAS AS R EFEREN CE.............................................. 95 4.6.2 ASIO.STIO.SPP-PBI MEA WITH HT-PEM E LECTRODES...........................101 4.6.2.1 MEA CHARACTERISTICS AS H2-02-FUEL CELL AND AS DIRECT ETHANOL FUEL C E L L ....................................................... 101 4.6.2.2 VARIATION OF THE OPERATION TEMPERATURE AS H2-O2 EC . . 107 4.6.2.3 VARIATION OF THE HUMIDITY AS H2-O2 FUEL C ELL ................. 108 4.6.2.4 VARIATION OF THE OPERATION TEMPERATURE AS DIRECT ETHANOL FUEL C E LL....................................................................................112 4.6.3 CHARACTERIZATION OF THE A SIO.5T IO.5PP MEAS UP TO 2 5 0 C ........ 114 4.6.3.1 CHARACTERIZATION OF A P T-A S IO.5T IO.5P P MEA UP TO 250C 115 4.6.3.2 DETERMINATION OF THE ELECTROCHEMICAL ACTIVE SURFACE AREA (ECSA) OF A PT-ASIO.5TIO.5PP M E A ................................... 117 4.6.4 CHARACTERIZATION OF A PTSN-ASIO.5TIO.5PP MEA UP TO 250C . . . 118 4.6.5 CHARACTERIZATION OF A PTR H -A S IO.5T IO.5P P MEA UP TO 250C . . . 120 4.6.6 CHARACTERIZATION OF A PTRU-ASIO.5TIO.5PP MEA UP TO 250C . . . 122 5 D ISCU SSIO N 124 5.1 REPRODUCIBILITY AND S TAN D ARD IZATIO N ................................................................125 5.2 ASIO.STIO.SPP-PBI MEMBRANE ELECTRODE ASSEMBLIES.........................................125 5.3 CATALYSTS FOR THE ETHANOL OXIDATION R E A C TIO N ................................................. 131 6 SUM M ARY, C ONCLU SION S AND O U TLOOK 136 6.1 SUMMARY AND C ONCLUSIONS................................................................................. 137 6.2 O U TLO O K .................................................................................................................138 A D RAW IN GS AND SCH EM ES - T EST C ELL 139 B V APORIZER 143 C T H ERM O D Y N A M IC D A TA 144 R EFEREN CES 147 A CK N OW LED GEM EN TS 163
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spellingShingle	Reeb, Berthold Benedikt Lothar Analysis and development of a direct alcohol fuel cell system
subject_GND	(DE-588)4113937-9
title	Analysis and development of a direct alcohol fuel cell system
title_auth	Analysis and development of a direct alcohol fuel cell system
title_exact_search	Analysis and development of a direct alcohol fuel cell system
title_full	Analysis and development of a direct alcohol fuel cell system Berthold Benedikt Lothar Reeb
title_fullStr	Analysis and development of a direct alcohol fuel cell system Berthold Benedikt Lothar Reeb
title_full_unstemmed	Analysis and development of a direct alcohol fuel cell system Berthold Benedikt Lothar Reeb
title_short	Analysis and development of a direct alcohol fuel cell system
title_sort	analysis and development of a direct alcohol fuel cell system
topic_facet	Hochschulschrift
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