Introduction to polymer chemistry:
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| Format: | Buch |
| Sprache: | English |
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Boca Raton ; London ; New York
CRC Press, Taylor & Francis Group
[2017]
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| Ausgabe: | Fourth edition |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | xxvii, 560 Seiten Illustrationen, Diagramme |
| ISBN: | 9781498737616 |
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| 245 | 1 | 0 | |a Introduction to polymer chemistry |c Charles E. Carraher, Jr. |
| 246 | 1 | 3 | |a Polymer chemistry |
| 250 | |a Fourth edition | ||
| 264 | 1 | |a Boca Raton ; London ; New York |b CRC Press, Taylor & Francis Group |c [2017] | |
| 300 | |a xxvii, 560 Seiten |b Illustrationen, Diagramme | ||
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| 650 | 4 | |a Polymerization | |
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Datensatz im Suchindex
| _version_ | 1804177028584308736 |
|---|---|
| adam_text | Titel: Introduction to polymer chemistry
Autor: Carraher, Charles E
Jahr: 2017
Contents
Preface xv
Acknowledgments xvii
Author xix
How to Study Polymers xxi
Polymer Nomenclature xxiü
American Chemlstry Society Commlttee on Professional Training Requirements xxvil
Chapter 1 Introductlon to Polymers 1
1.1 Hlstoryof Polymers 1
1.2 Why Polymers? 11
1.3 Today s Marketplace 14
1.4 Environmental Assessment 17
1.4.1 Environmental Impact Assessment 19
1.4.2 Ecological Footprlnt 20
1.4.3 Life Cycle Assessment 20
1.5 Managlng Sustainability 21
Summary 23
Glossary 24
Exercises 25
Further Reading 25
General Encyclopedlas and Dictlonaries 26
Chapter 2 Polymer Structure (Morphology) 27
2.1 Stereochemlstryof Polymers 28
2.2 Molecular Interactlons 34
2.2.1 Glass Transition and Melt Transition 38
2.2.2 Secondary Structures 40
2.3 Polymer Crystals 41
2.4 Amorphous Bulk State 44
2.5 Polymer Structure-Property Relatlonships 45
2.6 Crystalline and Amorphous Combinations 47
2.7 Cross-Linking 49
Summary 50
Glossary 51
Exercises 52
Further Reading 53
Chapter 3 Molecular Weight of Polymers 55
3.1 Introductlon 55
3.2 Solubility 57
3.2.1 Basic Concepts 57
3.2.2 Theoretical Approaches to Solubility 58
3.3 Average Molecular Weight Valúes 60
3.4 Fractionation of Polydisperse Systems 63
v
vi Contents
3.5 Chromatography 64
3.5.1 General Chromatography 64
3.5.2 Ion-Exchange Chromatography 64
3.5.3 Affinity Chromatography 64
3.5.4 High-Performance Liquid Chromatography 65
3.5.5 Electrophoresis 65
3.5.6 Gel Permeation Chromatography 66
3.5.7 Size Exclusión Chromatography 66
3.6 Colligative Molecular Weights 67
3.6.1 Osmometry 67
3.6.2 End-Group Analysis 68
3.6.3 Ebulliometry and Cryometry 68
3.7 Light-Scattering Photometry 69
3.8 OtherTechniques 74
3.8.1 Ultracentrifugation 74
3.8.2 Mass Spectrometry 75
3.9 Viscometry 76
3.9.1 Solution Viscosity 76
3.9.2 Melted Polymer Viscosities 80
Summary 81
Glossary 82
Exercises 84
Further Reading 85
Chapter4 Naturally Occurring Polymers 87
4.1 Polysaccharides 89
4.2 Cellulose 91
4.2.1 Paper 95
4.2.2 Paper Recycling 98
4.3 Cellulose-Regenerating Processes 99
4.3.1 Dissolving and Precipitation of Cellulose 99
4.3.2 Wrinkle-Free Fabric 100
4.4 Estersand EthersofCellulose 102
4.4.1 Inorganic Esters 103
4.4.2 Organic Esters 103
4.4.3 Organic Ethers 105
4.5 Starch 106
4.6 Other Polysaccharides 109
4.6.1 Glycogen 109
4.6.2 Dextrans 110
4.6.3 Chitin 110
4.6.4 Chitosan 111
4.6.5 Heparin 112
4.6.6 Hyaluronic Acid 113
4.6.7 Chondroitin Sulfates 113
4.6.8 Arabinogalactans 113
4.6.9 Carrageenans, Agar, and Agarose 113
4.7 Proteins 114
4.7.1 Basics 114
4.7.2 Primary Structure 116
4.7.3 Secondary Structure 116
4.7.3.1 Keratins 118
4.7.3.2 Silk 120
4.7.3.3 Wool 123
Contents vii
4.7.4 Tertiary Structure 124
4.7.4.1 Globular Proteins 124
4.7.4.2 Fibrous Proteins 126
4.7.4.3 Elastin 127
4.7.4.4 Membrane Proteins 128
4.7.5 Quaternary Structure 128
4.8 NucleicAcids 130
4.8.1 Basics 130
4.8.2 Flow of Biological Information 134
4.8.3 Next Steps 136
4.9 Naturally Occurring Polyisoprenes and Other Synthetic Elastomers 137
4.9.1 Balloons 141
4.9.2 Resins 142
4.9.3 Rosin and Related Materials 143
4.10 Lignln 144
4.11 Melanins 145
4.12 Polymer Structure 147
4.13 Genetic Engineering 148
4.14 DNA Profiling 150
4.15 Asphalt 152
Summary 153
Glossary 154
Exercises 156
Further Reading 157
Chapter 5 Step-Reaction Polymerization (Polycondensation Reactions) 159
5.1 Comparison between Polymer Type and Kinetics of Polymerization 159
5.2 Introduction 164
5.3 Stepwise Kinetics 164
5.4 Polycondensation Mechanisms 169
5.5 Polyesters and Polycarbonates 170
5.6 Synthetic Polyamides 178
5.7 Polymides 185
5.8 Polybenzimidazoles and Related Polymers 186
5.9 Polyurethanes and Polyureas 187
5.10 Polysulfides 190
5.11 Polyethers 191
5.12 Polysulfones 193
5.13 Poly(Ether Ether Ketone) and Polyketones 194
5.14 Phenolic and Amino Plastics 195
5.15 Synthetic Routes 197
5.16 Liquid Crystals 199
5.17 Microfibers 201
Summary 202
Glossary 203
Exercises 204
Further Reading 206
Chapter 6 lonic Chain Reaction and Complex Coordination Polymerization (Addition Polymerization) 207
6.1 Cationic Polymerization 209
6.1.1 Kinetics of Cationic Polymerization 209
6.1.2 PolyCVinyl Isobutyl Ether) 211
6.1.3 Polyoxymethylene 212
viii Contents
6.1.4 Polyethylene Oxide) 212
6.1.5 Polyterpenes and Related Polymers 212
6.2 Anionic Polymerization 212
6.2.1 Kinetics of Anionic Polymerization 212
6.2.2 C/s-1,4-Polyisoprene 214
6.2.3 Living Polymers 214
6.3 Stereoregularity and Stereogeometry 215
6.4 Polymerization with ComplexCoordination Catalysts 216
6.5 Soluble Stereoregulating Catalysis 217
6.6 Polyethylenes 220
6.6.1 Introduction Polyethylenes 220
6.6.2 High-Density Polyethylene 224
6.6.3 Linear Low-Density Polyethylene 224
6.6.4 Very-Low-Density Polyethylene 226
6.6.5 Ultrahigh-Molecular-Weight Polyethylene 226
6.6.6 Ultralinear Polyethylene 226
6.6.7 Cross-Linked Polyethylene 226
6.6.8 Medium-Density Polyethylene 226
6.6.9 Polymethylene 227
6.6.10 Shopping Bags 227
6.7 Polypropylene 229
6.7.1 History 229
6.7.2 Stereospecific Structures 232
6.7.3 Early Production 233
6.7.4 Forms of Polypropylene 234
6.8 Polymers from 1,4-Dienes 235
6.8.1 Introduction 235
6.8.2 Butadiene Rubber 235
6.8.3 ABS 235
6.8.4 High-Impact Polystyrene 236
6.8.5 Polyisoprene 236
6.8.6 Polychloroprene 237
6.9 Polyisobutylene 237
6.10 Metathesis Reactions 238
6.11 Zwitterionic Polymerization 239
6.12 Isomerization Polymerization 239
6.13 Precipitation Polymerization 240
Summary 240
Glossary 241
Exercises 242
Further Reading 244
Chapter 7 Free Radical Chain Polymerization (Addition Polymerization) 245
7.1 Initiators for Free Radical Chain Polymerization 245
7.2 Mechanism for Free Radical Chain Polymerization 248
7.3 Chain Transfer 255
7.4 Polymerization Techniques 257
7.4.1 Bulk Polymerization 257
7.4.2 Suspension Polymerization 259
7.4.3 Solution Polymerization 259
7.4.4 Emulsion Polymerization 260
7.5 Fluorine-Containing Polymers 262
7.5.1 Polytetrafluoroethylene 262
7.5.2 Poly(Vinyl Fluoride) 264
7.5.3 Other Fluorine-Containing Polymers 265
Contents i*
7.6 Polystyrene 266
7.7 Poly(Vinyl Chloride) 268
7.8 Poly(Methyl Methacrylate) 271
7.9 Polyacrylonitrile 273
7.10 Solid-State Irradiation Polymerization 274
7.11 Plasma Polymerizations 274
Summary 275
Glossary 276
Exercises 277
Further Reading 278
Chapter8 Copolymerization 279
8.1 Kinetics of Copolymerization 280
8.2 TheQ-eScheme 283
8.3 Commercial Copolymers 284
8.4 Block Copolymers 284
8.5 Graft Copolymers 286
8.6 Elastomers 286
8.6.1 General 286
8.6.2 Thermoplastic Elastomers 288
8.6.3 SBR Copolymers 288
8.6.4 Sales and Flammability 289
8.7 Blends 289
8.7.1 General 289
8.7.2 Immisclble Blends 290
8.7.3 Immiscible Blends: Remainderof the Section on Immiscible Blends 290
8.7.4 Miscible Blends 291
8.8 Polymer Mixtures: IPNs and Alloys 293
8.9 Dendrites 293
8.10 lonomers 295
8.11 Fluoroelastomers 296
8.12 Nitrile Rubber 296
8.12.1 Laboratory Gloves 297
8.13 Acrylonitrile Butadiene Styrene Terpolymers 298
8.14 EPDM Rubber 299
Summary 300
Glossary 300
Exercises 301
Further Reading 302
Chapter 9 Organometallic and Metalloid Polymers 305
9.1 Introduction 305
9.2 Inorganic Reaction Mechanisms 306
9.3 Condensation Organometallic Polymers 309
9.4 Coordination Polymers 314
9.5 Addition Polymers 316
Summary 319
Glossary 320
Exercises 320
Further Reading 320
Chapter 10 Inorganic Polymers 323
10.1 Introduction 323
10.2 Portland Cement 323
10.3 Other Cements 326
X
Contents
10.4 Silicates 328
10.4.1 Network 330
10.4.2 Layer 331
10.4.3 Chain 332
10.5 Silicon Dioxide (Amorphous) 332
10.5.1 Kinds ofGlass 334
10.5.2 SafetyGlass 337
10.5.3 New Applications ofGlass 338
10.5.4 Seeing Glass Lenses 339
10.6 Sol-Gel 341
10.6.1 Aerogels 341
10.7 Silicon Dioxide (Crystalline Forms): Quartz Forms 343
10.8 Silicon Dioxide in Electronic Chips 345
10.9 Asbestos 345
10.10 Fly Ash and Aluminosilicates 346
10.11 Polymerie Carbon: Diamond 348
10.12 Polymerie Carbon: Graphite 350
10.13 Internal Cyclization: Carbon Fibers and Related Materials 351
10.14 Carbon Nanotubes 353
10.14.1 General 353
10.14.2 Structures 353
10.14.3 Properties 355
10.14.3.1 Electrica! 355
10.14.3.2 Mechanical 356
10.14.3.3 Field Emission 356
10.14.3.4 Flydrogen and Ion Storage 356
10.14.3.5 Chemical and Genetlc Probes 356
10.14.3.6 Analytical Tools 356
10.14.3.7 Superconductors 356
10.14.4 Health Issues 357
10.14.5 Potential 357
10.15 Bitumens 357
10.16 Carbon Black 358
10.17 Polysulfur 360
10.18 Ceramics 360
10.19 High-Temperature Superconductors 362
10.19.1 Discovery ofthe 123-Compound 362
10.19.2 Structure ofthe 123-Compound 362
10.20 Zeolites 363
Summary 364
Glossary 365
Exercises 366
Further Reading 366
Chapter 11 Reactions of Polymers 369
11.1 Reactions with Polyolefins and Polyenes 369
11.2 Reactions of Aromatic and Aliphatic Pendant Groups 370
11.3 Degradation 371
11.4 Cross-Linking 373
11.5 Reactivities of End Groups 373
11.6 Supramolecules and Self-Assembly 374
11.7 Transfer and Retention of Oxygen 377
11.8 Nature s Macromolecular Catalysts 381
Contents xi
11.9 Photosynthesis 385
11.9.1 General 385
11.9.2 Purple Photosynthetlc Bacteria 387
11.9.3 Green Sulfur Bacteria 388
11.10 Mechanisms of Physical Energy Absorption 388
11.11 Breakage of Polymerie Materials 390
Summary 392
Glossary 392
Exerci ses 393
Further Reading 394
Chapter 12 Testing and Spectrometric Characterization of Polymers 395
12.1 Spectronic Characterization of Polymers 396
12.1.1 Infrared Spectroscopy 396
12.1.2 Raman Spectroscopy 398
12.1.3 Nuclear Magnetic Resonance Spectroscopy 398
12.1.4 NMR Applications 400
12.1.5 Electron Paramagnetlc Resonance Spectroscopy 401
12.1.6 X-Ray Spectroscopy 401
12.2 Surface Characterization 401
12.2.1 Attenuated Total Reflectance 402
12.2.2 Auger Electron Spectroscopy and X-Ray Photoelectron Spectroscopy 402
12.2.3 Near-Fleld Scanning Optical Microscopy 403
12.2.4 Electron Microscopy 403
12.2.5 Scanning Probe Microscopy 403
12.2.6 Secondary Ion Mass Spectroscopy 406
12.2.7 Superresolution Fluorescence Microscopy 406
12.3 Amorphous Region Determinations 407
12.4 Thermal Analysis 407
12.5 Thermal Property Tests 409
12.5.1 Thermal Conductivity 409
12.5.2 Thermal Expansion 410
12.5.3 Glass Transition Temperatures 410
12.6 Flammability 410
12.7 Electrical Properties: Theory .410
12.8 Electric Measurements 412
12.9 Weatherability 413
12.10 Optical Property Tests 414
12.10.1 Index ofRefraction 414
12.10.2 Optical Clarity 415
12.10.3 Absorption and Reflectance 415
12.11 Chemical Resistance 415
Summary 416
Glossary 417
Exercises 418
Further Reading 419
Chapter 13 Rheology and Physical Tests 421
13.1 Rheology 421
13.1.1 Rheology and Physical Tests 424
13.1.2 Response Time 427
13.2 Typical Stress-Strain Behavior 427
13.3 Stress-Strain Relationships 429
xii Contents
13.4 Specific Physical Tests 431
13.4.1 Tensile Strength 431
13.4.2 Tensile Strength of Inorganicand Metallic Fibers and Whiskers 432
13.4.3 Hardness 433
13.4.4 Failure 433
Summary 434
Glossary 434
Exercises 435
Further Reading 436
Chapter 14 Additives 437
14.1 Fi Hers 437
14.2 Reinforcements 439
14.2.1 Fibers and Resins 440
14.2.2 Applications 441
14.3 Nanocomposites 444
14.4 Plasticizers 446
14.5 Antioxidants 448
14.6 Heat Stabilizers 448
14.7 Ultraviolet Stabilizers 449
14.8 Flame Retardants 449
14.9 Colorants 450
14.10 Curing Agents 451
14.11 Antistatic Agents: Antistats 451
14.12 Chemical Blowing Agents 452
14.13 Compatibilizers 452
14.14 Impact Modifiers 452
14.15 Processing Aids 453
14.16 Lubricants 453
14.17 Microorganism Inhibitors 453
Summary 453
Glossary 454
Exercises 455
Further Reading 456
Chapter 15 Synthesis of Reactants and Intermediates for Polymers 459
15.1 Monomer Synthesis from Basic Feedstocks 459
15.2 Reactants for Step-Reaction Polymerization 467
15.3 Synthesis of Vinyl Monomers 473
15.4 Search for Less Expensive Feedstocks 477
Summary 478
Glossary 478
Exercises 479
Further Reading 479
Chapter 16 Polymer Technology 481
16.1 Polymer Processing 481
16.1.1 General 481
16.1.2 Secondary Structures: Mesophases 483
Contents xiii
16.2 Fibers 485
16.2.1 Polymer Processing: Spinning and Fiber Production 485
16.2.1.1 Introduction 485
16.2.1.2 Melt Spinning 487
16.2.1.3 Dry Spinning 487
16.2.1.4 Wet Spinning 487
16.3 Elastomers 488
16.3.1 Elastomer Processing 488
16.4 Films and Sheets 490
16.4.1 Calendering 491
16.5 Polymerie Foams 491
16.6 Reinforced Plastics (Composites) and Laminates 491
16.6.1 Composites 491
16.6.2 Particle-Reinforced Composites: Large-Particle Composites 492
16.6.3 Fiber-Reinforced Composites 493
16.6.4 Processing of Fiber-Reinforced Composites 493
16.6.5 Structural Composites 494
16.6.6 Laminating 494
16.7 Molding 495
16.7.1 Injection Molding 496
16.7.2 Blow Molding 497
16.7.3 Rotational Molding 498
16.7.4 Compression and Transfer Molding 499
16.7.5 Thermoforming 500
16.8 Casting 500
16.9 Extrusión 500
16.9.1 Processing 501
16.9.2 Rainwear 502
16.10 Coatings 503
16.11 Adhesives 505
16.12 Conductive Polymerie Materials 510
16.12.1 Photoconductive and Photonic Polymers 510
16.12.2 Electrically Conductive Polymers 511
16.13 Drug Design and Activity 515
16.14 Synthetic Biomedical Polymers 517
16.15 Dental Materials 521
16.16 Emerging Polymers 523
16.17 Green Materials 527
Summary 533
Glossary 534
Exercises 535
Further Reading 536
Appendix A: Structures of Common Polymers 539
Appendix B: Symbols and Acronyms 543
Appendix C: Comments on Health 547
Appendix D: ISO 9000 and 14000 549
Appendix E: Web Information 551
Index 553
|
| any_adam_object | 1 |
| author | Carraher, Charles E. 1941- |
| author_GND | (DE-588)1031526080 |
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| discipline | Chemie / Pharmazie Chemie |
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| id | DE-604.BV044027760 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T07:41:34Z |
| institution | BVB |
| isbn | 9781498737616 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-029435101 |
| oclc_num | 992500640 |
| open_access_boolean | |
| owner | DE-29T DE-11 DE-634 DE-19 DE-BY-UBM |
| owner_facet | DE-29T DE-11 DE-634 DE-19 DE-BY-UBM |
| physical | xxvii, 560 Seiten Illustrationen, Diagramme |
| publishDate | 2017 |
| publishDateSearch | 2017 |
| publishDateSort | 2017 |
| publisher | CRC Press, Taylor & Francis Group |
| record_format | marc |
| spelling | Carraher, Charles E. 1941- (DE-588)1031526080 aut Introduction to polymer chemistry Charles E. Carraher, Jr. Polymer chemistry Fourth edition Boca Raton ; London ; New York CRC Press, Taylor & Francis Group [2017] xxvii, 560 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Polymers Polymerization Polymere (DE-588)4046699-1 gnd rswk-swf Makromolekulare Chemie (DE-588)4168684-6 gnd rswk-swf Polymerisation (DE-588)4046704-1 gnd rswk-swf Polymere (DE-588)4046699-1 s Makromolekulare Chemie (DE-588)4168684-6 s DE-604 Polymerisation (DE-588)4046704-1 s Erscheint auch als Online-Ausgabe 978-1-4987-3785-2 HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029435101&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Carraher, Charles E. 1941- Introduction to polymer chemistry Polymers Polymerization Polymere (DE-588)4046699-1 gnd Makromolekulare Chemie (DE-588)4168684-6 gnd Polymerisation (DE-588)4046704-1 gnd |
| subject_GND | (DE-588)4046699-1 (DE-588)4168684-6 (DE-588)4046704-1 |
| title | Introduction to polymer chemistry |
| title_alt | Polymer chemistry |
| title_auth | Introduction to polymer chemistry |
| title_exact_search | Introduction to polymer chemistry |
| title_full | Introduction to polymer chemistry Charles E. Carraher, Jr. |
| title_fullStr | Introduction to polymer chemistry Charles E. Carraher, Jr. |
| title_full_unstemmed | Introduction to polymer chemistry Charles E. Carraher, Jr. |
| title_short | Introduction to polymer chemistry |
| title_sort | introduction to polymer chemistry |
| topic | Polymers Polymerization Polymere (DE-588)4046699-1 gnd Makromolekulare Chemie (DE-588)4168684-6 gnd Polymerisation (DE-588)4046704-1 gnd |
| topic_facet | Polymers Polymerization Polymere Makromolekulare Chemie Polymerisation |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029435101&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT carrahercharlese introductiontopolymerchemistry AT carrahercharlese polymerchemistry |