Asymmetric synthesis in organophosphorus chemistry: synthetic methods, catalysis, and applications
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Elektronisch E-Book |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
[2017]
|
| Schlagworte: | |
| Online-Zugang: | FRO01 UBG01 UBR01 Volltext Inhaltsverzeichnis |
| Beschreibung: | Fundamentals of the Stereochemistry of Organophosphorus Compounds -- Asymmetric Synthesis of P-Chirogenic Phosphorus Compounds -- Phosphorus Compounds with Chiral Side-Chain Centers -- Asymmetric Catalysis with Metal Complexes -- Asymmetric Organocatalysis -- Asymmetric Biocatalysis. - Includes bibliographical references and index |
| Beschreibung: | 1 Online-Ressource (xiv, 376 Seiten) Illustrationen |
| ISBN: | 9783527341542 9783527341535 9783527341511 9783527341528 |
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| 245 | 1 | 0 | |a Asymmetric synthesis in organophosphorus chemistry |b synthetic methods, catalysis, and applications |c Oleg I. Kolodiazhnyi |
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| 500 | |a Fundamentals of the Stereochemistry of Organophosphorus Compounds -- Asymmetric Synthesis of P-Chirogenic Phosphorus Compounds -- Phosphorus Compounds with Chiral Side-Chain Centers -- Asymmetric Catalysis with Metal Complexes -- Asymmetric Organocatalysis -- Asymmetric Biocatalysis. - Includes bibliographical references and index | ||
| 650 | 7 | |a SCIENCE / Chemistry / Organic |2 bisacsh | |
| 650 | 4 | |a Chemie | |
| 650 | 4 | |a Organophosphorus compounds | |
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Datensatz im Suchindex
| _version_ | 1804176706972418048 |
|---|---|
| adam_text | CONTENTS
PREFACE XI
ABBREVIATIONS XIII
1 FUNDAMENTALS OF THE STEREOCHEMISTRY OF ORGANOPHOSPHORUS
COMPOUNDS 1
1.1 HISTORICAL BACKGROUND 1
1.2 SOME COMMON DEFINITIONS IN STEREOCHEMISTRY 4
1.3 DETERMINATION OF ENANTIOMER COMPOSITION 7
1.3.1 METHOD OF NUCLEAR MAGNETIC RESONANCE 8
1.3.1.1 CHIRAL SOLVATING AGENTS 8
1.3.1.2 COMPLEXES OF METALS (SHIFT REAGENTS) 10
1.3.1.3 CHIRAL DERIVATIZING AGENTS FOR NMR 11
1.3.2 CHROMATOGRAPHIC METHODS OF ANALYSIS 14
1.3.2.1 GAS CHROMATOGRAPHY 25
1.3.2.2 LIQUID CHROMATOGRAPHY 16
1.4 DETERMINATION OF THE ABSOLUTE CONFIGURATION 17
1.4.1 X-RAY CRYSTAL ANALYSIS 17
1.4.2 METHOD OF CHEMICAL CORRELATION 19
1.4.3 THE ASSIGNMENT OF ABSOLUTE CONFIGURATION BY NMR 19
1.5 ASYMMETRIC INDUCTION AND STEREOCHEMISTRY 24
1.5.1 ASYMMETRIC INDUCTION 24
1.5.2 ASYMMETRIC SYNTHESIS 25
1.5.3 ASYMMETRIC TRANSFORMATION 25
1.5.4 AN ENANTIOSELECTIVE REACTION 25
1.5.5 ENANTIOSELECTIVE SYNTHESIS 25
1.6 SUMMARY 26
REFERENCES 26
2 ASYMMETRIC SYNTHESIS OF P-CHIROGENIC PHOSPHORUS COMPOUNDS 35
2.1 INTRODUCTION 35
2.2 LOW-COORDINATED PHOSPHORUS COMPOUNDS 36
2.3 TRIVALENT TRICOORDINATED PHOSPHORUS COMPOUNDS 41
2.3.1 CONFIGURATION STABILITY OF P(III)-COMPOUNDS 41
2.3.2 ASYMMETRIC NUCLEOPHILIC SUBSTITUTION AT P (III) 43
2.3.2.1 SECONDARY ALCOHOLS AS CHIRAL AUXILIARIES 45
23.2.2 OPTICALLY ACTIVE AMINES AS CHIRAL AUXILIARIES 54
23.23 EPHEDRINE AS INDUCTOR OF CHIRALITY AT P(III) 58
2 3 3 ASYMMETRIC OXIDATION OF P(III) COMPOUNDS 67
2.3.4 ASYMMETRIC ELECTROPHILIC SUBSTITUTION AT P(III) 68
2.3.4.1 ASYMMETRIC MICHAELIS-ARBUZOV REACTION 70
2.4 PENTAVALENT P(IV)-PHOSPHORUS COMPOUNDS 71
2.4.1 INTRODUCTION 71
2.4.2 NUCLEOPHILIC SUBSTITUTION REACTIONS 72
2.4.2.1 NUCLEOPHILIC SUBSTITUTION AT P(IV) WITH CHIRAL ALCOHOL 74
2A.2.2 NUCLEOPHILIC SUBSTITUTION AT P(IV) WITH CHIRAL AMINES 78
2.5 CHIRAL P(V) AND P(VI) PHOSPHORUS COMPOUNDS 80
2.6 SUMMARY 86
REFERENCES 87
3 PHOSPHORUS COMPOUNDS WITH CHIRAL SIDE-CHAIN CENTERS 101
3.1 INTRODUCTION 101
3.2 ASYMMETRIC INDUCTION IN SIDE CHAINS 102
3.2.1 TRANSFER OF CHIRALITY FROM PHOSPHORUS TO OTHER CENTERS 103
3.2.1.1 CHIRAL PHOSPHORUS-STABILIZED ANIONS 103
3.2.1.2 1,2-ASYMMETRIC INDUCTION 105
3.2.1.3 1,4-ASYMMETRIC INDUCTION 107
3.3 ENANTIOSELECTIVE OLEFINATION 113
3.4 STEREOSELECTIVE ADDITION OF PHOSPHOROUS NUCLEOPHILES TO C=X BONDS
117
3.4.1 PHOSPHA-ALDOL REACTION 119
3.4.2 PHOSPHA-MANNICH REACTION 130
3.4.3 PHOSPHA-MICHAEL REACTION 142
3.5 ASYMMETRIC REDUCTION 147
3.6 ASYMMETRIC OXIDATION 152
3.7 C-MODIFICATION 156
3.8 ASYMMETRIC CYCLOADDITION 157
3.9 MULTIPLE STEREOSELECTIVITY 159
3.10 SUMMARY 169
REFERENCES 170
4 ASYMMETRIC CATALYSIS WITH METAL COMPLEXES 187
4.1 INTRODUCTION 187
4.2 ASYMMETRIC CATALYTIC HYDROGENATION AND OTHER REACTIONS OF
REDUCTION 188
4.2.1 HYDROGENATION OF C=C PHOSPHORUS COMPOUNDS 188
4.2.2 HYDROGENATION OF C= 0 PHOSPHORUS COMPOUNDS 200
4.3 ASYMMETRIC REDUCTION AND OXIDATION 203
4.3.1 REDUCTION OF C-O , C=N, AND C=C BONDS 204
4.3.2 ASYMMETRIC OXIDATION 210
4.4 ELECTROPHILIC ASYMMETRIC CATALYSIS 211
4.4.1 CATALYTIC ELECTROPHILIC SUBSTITUTION AT THE PHOSPHORUS ATOM 212
4.4.1.1 ALKYLATION AND ARYLATION OF P(III) COMPOUNDS 213
4.4.2 CATALYTIC ELECTROPHILIC SUBSTITUTION IN A SIDE CHAIN 217
4.4.2.1 ALKYLATION 217
4.4.2.2 HALOGENATION 219
4.4.2.3 AMINATION 221
4.5 NUCLEOPHILIC ASYMMETRIE CATALYSIS 223
4.5.1 ASYMMETRIE ADDITION OF PHOSPHORUS NUCLEOPHILES TO MULTIPLE BONDS
223
4.5.1.1 PHOSPHA-ALDOL REACTION 224
4.5.1.2 PHOSPHA-MANNICH REACTION 229
4.5.1.3 PHOSPHA-MICHAEL REACTION 232
4.6 CYCLOADDITION REACTIONS 237
4.7 SUMMARY 240
REFERENCES 241
5 ASYMMETRIC ORGANOCATALYSIS 253
5.1 INTRODUCTION 253
5.2 MODES FOR CATALYTIC ACTIVATION OF SUBSTRATES IN ASYMMETRIC
ORGANOCATALYSIS 254
5.3 PHOSPHA-ALDOL REACTION 258
5.3.1 CATALYSIS WITH CINCHONA ALKALOIDS 258
5.3.2 CATALYSIS WITH CINCHONA-THIOUREA 259
5.3.3 CATALYSIS BY OTHER ORGANOCATALYSTS 260
5.4 PHOSPHA-MANNICH REACTIONS 262
5.4.1 ORGANOCATALYSIS BY CINCHONA ALKALOIDS 262
5.4.2 ORGANOCATALYSIS BY IMINES 263
5.4.3 ORGANOCATALYSIS BY IMINIUM SALTS 265
5.4.4 ORGANOCATALYSIS BY CHIRAL BRONSTED ACIDS 265
5.5 PHOSPHA-MICHAEL REACTION 269
5.5.1 ORGANOCATALYSIS BY CINCHONA ALKALOIDS 269
5.5.2 ORGANOCATALYSIS BY THIOUREA 270
5.5.3 ORGANOCATALYSIS BY IMINIUM SALTS 272
5.5.4 ORGANOCATALYSIS BY N-HETEROCYCLIC CARBENES
274
5.5.5 ORGANOCATALYSIS USING PROLINE DERIVATIVES 274
5.6 ORGANOCATALYTIC ADDITION TO KETOPHOSPHONATES 282
5.6.1 PROLINE, AMINO ACIDS, AND THEIR DERIVATIVES 282
5.6.2 ORGANOCATALYSIS BY THIOUREA 288
5.7 PHOSPHA-HENRY REACTION 288
5.8 ORGANOCATALYTIC MODIFICATION OF P-YLIDS 290
5.9 ASYMMETRIC CATALYSIS WITH CHIRAL DIAMINES 292
5.10 MISCELLANEOUS 303
REFERENCES 305
6 ASYMMETRIC BIOCATALYSIS 315
6.1 INTRODUCTION 315
6.2 ENZYMATIC SYNTHESIS OF ORGANOPHOSPHORUS COMPOUNDS 315
6.2.1 KINETIC RESOLUTION OF HYDROXYPHOSPHONATES 316
6.2.2 RESOLUTION OF -HYDROXYPHOSPHONATES BY BIOCATALYTIC
TRANSESTERIFICATION 317
6.2.3 RESOLUTION OF -HYDROXYPHOSPHONATES BY BIOCATALYTIC HYDROLYSIS 319
6.2.4 DYNAMIC KINETIC RESOLUTION OF -HYDROXYPHOSPHONATES 323
6.2.5 RESOLUTION OF SS- AND OO-HYDROXYPHOSPHONATES 323
6.2.6 DYNAMIC KINETIC RESOLUTION OF SS-HYDROXYPHOSPHONATES 331
6.2.7 RESOLUTION OF AMINOPHOSPHONATES 332
6.3 BIOSYNTHESIS OF COMPOUNDS WITH C-P BOND 335
6.4 RESOLUTION OF P-CHIRAL PHOSPHORUS COMPOUNDS 337
6.5 MICROBIOLOGICAL SYNTHESIS OF CHIRAL ORGANOPHOSPHORUS COMPOUNDS 349
6.5.1 YEAST-CATALYZED SYNTHESIS 349
6.5.2 SYNTHESIS USING UNICELLULAR FUNGI 354
6.5.3 SYNTHESIS USING BACTERIA
356
6.6 SUMMARY 358
REFERENCES 358
INDEX 369
|
| any_adam_object | 1 |
| author | Kolodjažnyj, Oleg I. ca. 20. Jh |
| author_GND | (DE-588)1089273258 |
| author_facet | Kolodjažnyj, Oleg I. ca. 20. Jh |
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| author_sort | Kolodjažnyj, Oleg I. ca. 20. Jh |
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| dewey-full | 547/.07 |
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| dewey-ones | 547 - Organic chemistry |
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| dewey-search | 547/.07 |
| dewey-sort | 3547 17 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Electronic eBook |
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| illustrated | Not Illustrated |
| indexdate | 2024-07-10T07:36:27Z |
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| language | English |
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| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Kolodjažnyj, Oleg I. ca. 20. Jh. Verfasser (DE-588)1089273258 aut Asymmetric synthesis in organophosphorus chemistry synthetic methods, catalysis, and applications Oleg I. Kolodiazhnyi Weinheim Wiley-VCH [2017] 1 Online-Ressource (xiv, 376 Seiten) Illustrationen txt rdacontent c rdamedia cr rdacarrier Fundamentals of the Stereochemistry of Organophosphorus Compounds -- Asymmetric Synthesis of P-Chirogenic Phosphorus Compounds -- Phosphorus Compounds with Chiral Side-Chain Centers -- Asymmetric Catalysis with Metal Complexes -- Asymmetric Organocatalysis -- Asymmetric Biocatalysis. - Includes bibliographical references and index SCIENCE / Chemistry / Organic bisacsh Chemie Organophosphorus compounds Organophosphorus compounds / Synthesis Phosphororganische Verbindungen (DE-588)4076094-7 gnd rswk-swf Asymmetrische Synthese (DE-588)4135603-2 gnd rswk-swf Phosphororganische Verbindungen (DE-588)4076094-7 s Asymmetrische Synthese (DE-588)4135603-2 s DE-604 Erscheint auch als Druck-Ausgabe 978-3-527-34150-4 https://onlinelibrary.wiley.com/doi/book/10.1002/9783527341542 Verlag URL des Erstveröffentlichers Volltext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029249103&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Kolodjažnyj, Oleg I. ca. 20. Jh Asymmetric synthesis in organophosphorus chemistry synthetic methods, catalysis, and applications SCIENCE / Chemistry / Organic bisacsh Chemie Organophosphorus compounds Organophosphorus compounds / Synthesis Phosphororganische Verbindungen (DE-588)4076094-7 gnd Asymmetrische Synthese (DE-588)4135603-2 gnd |
| subject_GND | (DE-588)4076094-7 (DE-588)4135603-2 |
| title | Asymmetric synthesis in organophosphorus chemistry synthetic methods, catalysis, and applications |
| title_auth | Asymmetric synthesis in organophosphorus chemistry synthetic methods, catalysis, and applications |
| title_exact_search | Asymmetric synthesis in organophosphorus chemistry synthetic methods, catalysis, and applications |
| title_full | Asymmetric synthesis in organophosphorus chemistry synthetic methods, catalysis, and applications Oleg I. Kolodiazhnyi |
| title_fullStr | Asymmetric synthesis in organophosphorus chemistry synthetic methods, catalysis, and applications Oleg I. Kolodiazhnyi |
| title_full_unstemmed | Asymmetric synthesis in organophosphorus chemistry synthetic methods, catalysis, and applications Oleg I. Kolodiazhnyi |
| title_short | Asymmetric synthesis in organophosphorus chemistry |
| title_sort | asymmetric synthesis in organophosphorus chemistry synthetic methods catalysis and applications |
| title_sub | synthetic methods, catalysis, and applications |
| topic | SCIENCE / Chemistry / Organic bisacsh Chemie Organophosphorus compounds Organophosphorus compounds / Synthesis Phosphororganische Verbindungen (DE-588)4076094-7 gnd Asymmetrische Synthese (DE-588)4135603-2 gnd |
| topic_facet | SCIENCE / Chemistry / Organic Chemie Organophosphorus compounds Organophosphorus compounds / Synthesis Phosphororganische Verbindungen Asymmetrische Synthese |
| url | https://onlinelibrary.wiley.com/doi/book/10.1002/9783527341542 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029249103&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT kolodjaznyjolegi asymmetricsynthesisinorganophosphoruschemistrysyntheticmethodscatalysisandapplications |