Oxidation mechanisms of metallic carrier materials for gas separation membranes:
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| Format: | Abschlussarbeit Buch |
| Sprache: | English |
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Bochum
2015
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| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | [10] 148 Seiten Illustrationen, Diagramme |
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| 245 | 1 | 0 | |a Oxidation mechanisms of metallic carrier materials for gas separation membranes |c von Martin Schiek aus Köln |
| 264 | 1 | |a Bochum |c 2015 | |
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Datensatz im Suchindex
| _version_ | 1804176187358969856 |
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| adam_text | Index
1 Introduction 1
2 Fundamentals of Alumina-forming NiCrAl-base Alloys 6
3 Aims of the Studies 8
4 Theory of High Temperature Corrosion 9
4 1 Thermodynamics 9
411 Fundamentals 9
412 Dissociation Pressure 10
413 Oxidation in H2O/H2 and CO2/CO Mixtures 12
414 Ellingham Diagram 14
4 2 Oxidation Kinetics 15
421 Oxide Growth 15
422 Correlation between Oxide Thickness and Weight Change 17
4 3 Oxidation of Alloys 18
431 Transient Oxidation Stage 19
432 Internal Oxidation 21
4321 Internal Oxidation in the Absence of an External Oxide Scale 21
4322 Internal Oxidation in the Presence of an External Oxide Scale 27
433 Transition from Internal to External Oxidation 29
434 Maintenance of External Oxide Scale Growth 31
5 Experimental 33
5 1 Studied Materials 33
5 2 Sample Preparation 34
5 3 Oxidation Experiments 34
5 4 Test Parameters 35
5 5 Sample Characterization 36
551 SEM/EDX 37
552 XRD 37
553 GD-OES 38
554 SNMS 39
555 Fluorescence Spectroscopy 39
6 Results and Discussion 40
6 1 Oxidation Behavior of Alloy 602 CA 40
611 Phase Composition and Microstructure of Alloy 602 CA 40
612 Results of the Behavior in Ar-20%02 and FhO-Containing Gases 41
6121 Oxidation Kinetics 41
6122 Oxide Scale Formation 43
6123 Internal Oxidation and Carbide Depleted Zones 56
613 Discussion of the Behavior in Ar-20%02 and H20-Containing Gases 58
6131 External Chromia Scale Formation in Different Environments 58
6132 Incorporation of Titanium into Chromia Scales 60
6133 External Alumina Scale Formation 60
6 2 Oxidation Behavior of Haynes 214 71
621 Phase Composition and Microstructure of Haynes 214 71
622 Oxidation Behavior in Ar-20%02 74
6221 Oxidation Kinetics 74
6222 Oxide Scale Formation 77
6223 Formation of Precipitate Free Zone (PFZ) 83
623 Discussion of the Oxidation Behavior in Ar-20%02 87
6231 Time and Temperature Dependence of the Oxide Scale Morphology 87
6232 Effect of y -Precipitation on Oxidation Behavior 90
6233 Effect of Aging Treatments on Oxidation Behavior 92
62331 Oxidation Kinetics of Aged Haynes 214 92
62332 Oxide Scale Morphology
94
6234 Proposed Oxidation Mechanisms 96
624 Behavior of Haynes 214 in H20-Containing Gases Compared with Ar-20%02 103
6241 Behavior in Ar-7%H20 103
6242 Behavior in Ar-4%H2-7%H20 107
6243 Behavior in Ar-20%O2-7%H2O 112
625 Discussion of the Behavior in H20-containing Gases Compared to Ar-20%02 117
7 Effects of Alloy Composition Variation 121
8 Considerations Related to Material Geometry and Oxidation Behavior 126
9 Summary and Conclusion 129
10 References 133
Appendix A - Buoyancy Effect 145
Appendix B - Instantaneous Oxidation Rate Constant
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| author | Schiek, Martin 1986- |
| author_GND | (DE-588)1092711430 |
| author_facet | Schiek, Martin 1986- |
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| physical | [10] 148 Seiten Illustrationen, Diagramme |
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| spelling | Schiek, Martin 1986- Verfasser (DE-588)1092711430 aut Oxidation mechanisms of metallic carrier materials for gas separation membranes von Martin Schiek aus Köln Bochum 2015 [10] 148 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Dissertation Ruhr-Universität Bochum 2015 Nickellegierung (DE-588)4135870-3 gnd rswk-swf Aluminiumlegierung (DE-588)4001586-5 gnd rswk-swf Membran Verfahrenstechnik (DE-588)7749014-9 gnd rswk-swf Chromlegierung (DE-588)4220946-8 gnd rswk-swf Gastrennung (DE-588)4156082-6 gnd rswk-swf Oxidation (DE-588)4137187-2 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Nickellegierung (DE-588)4135870-3 s Chromlegierung (DE-588)4220946-8 s Aluminiumlegierung (DE-588)4001586-5 s Oxidation (DE-588)4137187-2 s Gastrennung (DE-588)4156082-6 s Membran Verfahrenstechnik (DE-588)7749014-9 s DE-604 Ruhr-Universität Bochum (DE-588)7409-3 dgg HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028949490&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Schiek, Martin 1986- Oxidation mechanisms of metallic carrier materials for gas separation membranes Nickellegierung (DE-588)4135870-3 gnd Aluminiumlegierung (DE-588)4001586-5 gnd Membran Verfahrenstechnik (DE-588)7749014-9 gnd Chromlegierung (DE-588)4220946-8 gnd Gastrennung (DE-588)4156082-6 gnd Oxidation (DE-588)4137187-2 gnd |
| subject_GND | (DE-588)4135870-3 (DE-588)4001586-5 (DE-588)7749014-9 (DE-588)4220946-8 (DE-588)4156082-6 (DE-588)4137187-2 (DE-588)4113937-9 |
| title | Oxidation mechanisms of metallic carrier materials for gas separation membranes |
| title_auth | Oxidation mechanisms of metallic carrier materials for gas separation membranes |
| title_exact_search | Oxidation mechanisms of metallic carrier materials for gas separation membranes |
| title_full | Oxidation mechanisms of metallic carrier materials for gas separation membranes von Martin Schiek aus Köln |
| title_fullStr | Oxidation mechanisms of metallic carrier materials for gas separation membranes von Martin Schiek aus Köln |
| title_full_unstemmed | Oxidation mechanisms of metallic carrier materials for gas separation membranes von Martin Schiek aus Köln |
| title_short | Oxidation mechanisms of metallic carrier materials for gas separation membranes |
| title_sort | oxidation mechanisms of metallic carrier materials for gas separation membranes |
| topic | Nickellegierung (DE-588)4135870-3 gnd Aluminiumlegierung (DE-588)4001586-5 gnd Membran Verfahrenstechnik (DE-588)7749014-9 gnd Chromlegierung (DE-588)4220946-8 gnd Gastrennung (DE-588)4156082-6 gnd Oxidation (DE-588)4137187-2 gnd |
| topic_facet | Nickellegierung Aluminiumlegierung Membran Verfahrenstechnik Chromlegierung Gastrennung Oxidation Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028949490&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT schiekmartin oxidationmechanismsofmetalliccarriermaterialsforgasseparationmembranes AT ruhruniversitatbochum oxidationmechanismsofmetalliccarriermaterialsforgasseparationmembranes |