Experimental electrochemistry: a laboratory textbook
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
[2019]
|
| Ausgabe: | 2., completely revised and enlarged edition |
| Schlagworte: | |
| Online-Zugang: | http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-33524-4/ Inhaltsverzeichnis |
| Beschreibung: | xx, 268 Seiten Illustrationen, Diagramme |
| ISBN: | 9783527335244 |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
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| 100 | 1 | |a Holze, Rudolf |d 1954- |e Verfasser |0 (DE-588)120422026 |4 aut | |
| 245 | 1 | 0 | |a Experimental electrochemistry |b a laboratory textbook |c Rudolf Holze |
| 250 | |a 2., completely revised and enlarged edition | ||
| 264 | 1 | |a Weinheim |b Wiley-VCH |c [2019] | |
| 264 | 4 | |c © 2019 | |
| 300 | |a xx, 268 Seiten |b Illustrationen, Diagramme | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 0 | 7 | |a Elektrochemie |0 (DE-588)4014241-3 |2 gnd |9 rswk-swf |
| 653 | |a Chemie | ||
| 653 | |a Chemistry | ||
| 653 | |a Electrochemical Analysis | ||
| 653 | |a Electrochemistry | ||
| 653 | |a Electronic Materials | ||
| 653 | |a Elektrochemie | ||
| 653 | |a Elektrochemische Analytik | ||
| 653 | |a Elektronische Materialien | ||
| 653 | |a Materials Science | ||
| 653 | |a Materialwissenschaften | ||
| 653 | |a Physikalische Chemie | ||
| 655 | 7 | |0 (DE-588)4127380-1 |a Praktikum |2 gnd-content | |
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| 856 | 4 | 0 | |u http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-33524-4/ |x Verlag |
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| 999 | |a oai:aleph.bib-bvb.de:BVB01-028726011 | ||
Datensatz im Suchindex
| _version_ | 1804175840611663872 |
|---|---|
| adam_text | CONTENTS
PREFACE
TO
THE
SECOND
EDITION
IX
PREFACE
TO
THE
FIRST
EDITION
XI
FOREWORD
TO
THE
SECOND
EDITION
XV
SYMBOLS
AND
ACRONYMS
XVII
1
INTRODUCTION:
AN
OVERVIEW
OF
PRACTICAL
ELECTROCHEMISTRY
1
PRACTICAL
HINTS
2
ELECTRODES
3
MEASURING
INSTRUMENTS
6
ELECTROCHEMICAL
CELLS
7
DATA
RECORDING
9
2
ELECTROCHEMISTRY
IN
EQUILIBRIUM
11
EXPERIMENT
2.1:
THE
ELECTROCHEMICAL
SERIES
11
EXPERIMENT
2.2:
STANDARD
ELECTRODE
POTENTIALS
AND
THE
MEAN
ACTIVITY
COEFFICIENT
15
EXPERIMENT
2.3:
PH
MEASUREMENTS
AND
POTENTIOMETRICALLY
INDICATED
TITRATIONS
20
EXPERIMENT
2.4:
REDOX
TITRATIONS
(CERIMETRY)
25
EXPERIMENT
2.5:
DIFFERENTIAL
POTENTIOMETRIC
TITRATION
27
EXPERIMENT
2.6:
POTENTIOMETRIC
MEASUREMENT
OF
THE
KINETICS
OF
THE
OXIDATION
OF
OXALIC
ACID
30
EXPERIMENT
2.7:
POLARIZATION
AND
DECOMPOSITION
VOLTAGE
34
EXPERIMENT
2.8:
A
SIMPLE
RELATIVE
HYDROGEN
ELECTRODE
39
3
ELECTROCHEMISTRY
WITH
FLOWING
CURRENT
43
EXPERIMENT
3.1:
ION
MOVEMENT
IN
AN
ELECTRIC
FIELD
44
EXPERIMENT
3.2:
PAPER
ELECTROPHORESIS
46
EXPERIMENT
3.3:
CHARGE
TRANSPORT
IN
ELECTROLYTE
SOLUTION
47
EXPERIMENT
3.4:
CONDUCTANCE
TITRATION
51
EXPERIMENT
3.5:
CHEMICAL
CONSTITUTION
AND
ELECTROLYTIC
CONDUCTANCE
54
EXPERIMENT
3.6:
FARADAY S
LAW
56
EXPERIMENT
3.7:
KINETICS
OF
ESTER
SAPONIFICATION
58
EXPERIMENT
3.8:
MOVEMENT
OF
IONS
AND
HITTORF
TRANSPORT
NUMBER
62
VI
CONTENTS
EXPERIMENT
3.9:
POLAROGRAPHIC
INVESTIGATION
OF
THE
ELECTROREDUCTION
OF
FORMALDEHYDE
68
EXPERIMENT
3.10:
GALVANOSTATIC
MEASUREMENT
OF
STATIONARY
CURRENT-POTENTIAL
CURVES
72
EXPERIMENT
3.11:
CYCLIC
VOLTAMMETRY
75
EXPERIMENT
3.12:
SLOW
SCAN
CYCLIC
VOLTAMMETRY
82
EXPERIMENT
3.13:
KINETIC
INVESTIGATIONS
WITH
CYCLIC
VOLTAMMETRY
86
EXPERIMENT
3.14:
NUMERICAL
SIMULATION
OF
CYCLIC
VOLTAMMOGRAMS
90
EXPERIMENT
3.15:
CYCLIC
VOLTAMMETRY
WITH
MICROELECTRODES
92
EXPERIMENT
3.16:
CYCLIC
VOLTAMMETRY
OF
ORGANIC
MOLECULES
96
EXPERIMENT
3.17:
CYCLIC
VOLTAMMETRY
IN
NONAQUEOUS
SOLUTIONS
102
EXPERIMENT
3.18:
CYCLIC
VOLTAMMETRY
WITH
SEQUENTIAL
ELECTRODE
PROCESSES
104
EXPERIMENT
3.19:
CYCLIC
VOLTAMMETRY
OF
AROMATIC
HYDROCARBONS
107
EXPERIMENT
3.20:
CYCLIC
VOLTAMMETRY
OF
ANILINE
AND
POLYANILINE
110
EXPERIMENT
3.21:
GALVANOSTATIC
STEP
MEASUREMENTS
115
EXPERIMENT
3.22:
CYCLIC
VOLTAMMETRY
OF
A
SUPERCAPACITOR
ELECTRODE
118
EXPERIMENT
3.23:
CHRONOAMPEROMETRY
121
EXPERIMENT
3.24:
CHRONOCOULOMETRY
122
EXPERIMENT
3.25:
ROTATING
DISK
ELECTRODE
124
EXPERIMENT
3.26:
ROTATING
RING-DISK
ELECTRODE
130
EXPERIMENT
3.27:
MEASUREMENT OF
ELECTRODE
IMPEDANCES
133
EXPERIMENT
3.28:
CORROSION
CELLS
136
EXPERIMENT
3.29:
AERATION
CELL
138
EXPERIMENT
3.30:
CONCENTRATION
CELL
139
EXPERIMENT
3.31:
SALT
WATER
DROP
EXPERIMENT
ACCORDING
TO
EVANS
141
EXPERIMENT
3.32:
PASSIVATION
AND
ACTIVATION
OF
AN
IRON
SURFACE
142
EXPERIMENT
3.33:
CYCLIC
VOLTAMMETRY
WITH
CORRODING
ELECTRODES
143
EXPERIMENT
3.34:
TAFEL
PLOT
OF
A
CORRODING
ELECTRODE
145
EXPERIMENT
3.35:
IMPEDANCE
OF
A
CORRODING
ELECTRODE
148
EXPERIMENT
3.36:
LINEAR
POLARIZATION
RESISTANCE
OF
A
CORRODING
ELECTRODE
150
EXPERIMENT
3.37:
OSCILLATING
REACTIONS
152
4
ANALYTICAL
ELECTROCHEMISTRY
155
EXPERIMENT
4.1:
ION-SENSITIVE
ELECTRODE
156
EXPERIMENT
4.2:
POTENTIOMETRICALLY
INDICATED
TITRATIONS
158
EXPERIMENT
4.3:
BIPOTENTIOMETRICALLY
INDICATED
TITRATION
163
EXPERIMENT
4.4:
CONDUCTOMETRICALLY
INDICATED
TITRATION
165
EXPERIMENT
4.5:
ELECTROGRAVIMETRY
167
EXPERIMENT
4.6:
COULOMETRIC
TITRATION
170
EXPERIMENT
4.7:
AMPEROMETRY
172
EXPERIMENT
4.8:
POLAROGRAPHY
(FUNDAMENTALS)
178
EXPERIMENT
4.9:
POLAROGRAPHY
(ADVANCED
METHODS)
182
EXPERIMENT
4.10:
ANODIC
STRIPPING
VOLTAMMETRY
183
EXPERIMENT
4.11:
ABRASIVE
STRIPPING
VOLTAMMETRY
186
EXPERIMENT
4.12:
POLAROGRAPHIC
ANALYSIS
OF
ANIONS
189
EXPERIMENT
4.13:
TENSAMMETRY
191
CONTENTS
VII
5
NONTRADITIONAL
ELECTROCHEMISTRY
197
EXPERIMENT
5.1:
UV-VIS
SPECTROSCOPY
197
EXPERIMENT
5.2:
SURFACE-ENHANCED
RAMAN
SPECTROSCOPY
200
EXPERIMENT
5.3:
SURFACE-ENHANCED
RAMAN
SPECTROSCOPY
OF
A
SELF-ASSEMBLED
MONOLAYER
203
EXPERIMENT
5.4:
INFRARED
SPECTROELECTROCHEMISTRY
205
EXPERIMENT
5.5:
ELECTROCHROMISM
207
EXPERIMENT
5.6:
RAMAN
SPECTROSCOPIC
MONITORING
OF
CHARGE/DISCHARGE
OF
AN
INTRINSICALLY
CONDUCTING
POLYANILINE
SUPERCAPACITOR
ELECTRODE
MATERIAL
209
6
ELECTROCHEMICAL
ENERGY
CONVERSION
AND
STORAGE
211
EXPERIMENT
6.1:
LEAD-ACID
ACCUMULATOR
211
EXPERIMENT
6.2:
DISCHARGE
BEHAVIOR
OF
NICKEL-CADMIUM
ACCUMULATORS
216
EXPERIMENT
6.3:
PERFORMANCE
DATA
OF
A
FUEL
CELL
218
EXPERIMENT
6.4:
CHARGING
SUPERCAPACITORS
221
EXPERIMENT
6.5:
DISCHARGING
SUPERCAPACITORS
224
EXPERIMENT
6.6:
ZINC-AIR
CELL
227
EXPERIMENT
6.7:
LITHIUM-ION BATTERY
228
EXPERIMENT
6.8:
LOW-TEMPERATURE
DISCHARGE
BEHAVIOR
OF
NICKEL-CADMIUM
ACCUMULATORS
230
EXPERIMENT
6.9:
DISCHARGE
BEHAVIOR
OF
NICKEL-CADMIUM
ACCUMULATORS
AT
CONSTANT
LOAD
233
EXPERIMENT
6.10:
IMPEDANCE
OF
A
BUTTON
CELL
234
EXPERIMENT
6.11:
POTENTIOSTATIC
POLARIZATION
CURVES
236
EXPERIMENT
6.12:
GALVANOSTATIC
POLARIZATION
CURVES
237
7
ELECTROCHEMICAL
PRODUCTION
241
EXPERIMENT
7.1:
CEMENTATION
REACTION
241
EXPERIMENT
7.2:
GALVANIC
COPPER
DEPOSITION
242
EXPERIMENT
7.3:
ELECTROCHEMICAL
OXIDATION
OF
ALUMINUM
244
EXPERIMENT
7.4:
KOLBE
ELECTROLYSIS
OF
ACETIC
ACID
245
EXPERIMENT
7.5:
ELECTROLYSIS
OF
ACETYL
ACETONE
247
EXPERIMENT
7.6:
ANODIC
OXIDATION
OF
MALONIC
ACID
DIETHYLESTER
250
EXPERIMENT
7.7:
INDIRECT
ANODIC
DIMERIZATION
OF
ACETOACETIC
ESTER
(3-OXO-BUTYRIC
ACID
ETHYL
ESTER)
251
EXPERIMENT
7.8:
ELECTROCHEMICAL
BROMINATION
OF
ACETONE
253
EXPERIMENT
7.9:
ELECTROCHEMICAL
IODINATION
OF
ETHANOL
255
EXPERIMENT
7.10:
ELECTROCHEMICAL
PRODUCTION
OF
POTASSIUM
PEROXODISULFATE
25
7
EXPERIMENT
7.11:
YIELD
OF
CHLOR-ALKALI
ELECTROLYSIS
ACCORDING
TO THE
DIAPHRAGM
PROCESS
258
APPENDIX
261
INDEX
263
|
| any_adam_object | 1 |
| author | Holze, Rudolf 1954- |
| author_GND | (DE-588)120422026 |
| author_facet | Holze, Rudolf 1954- |
| author_role | aut |
| author_sort | Holze, Rudolf 1954- |
| author_variant | r h rh |
| building | Verbundindex |
| bvnumber | BV043305231 |
| classification_rvk | VE 5100 VE 6300 VE 6301 |
| classification_tum | CHE 140f |
| ctrlnum | (OCoLC)1124790649 (DE-599)DNB1079289704 |
| dewey-full | 540 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 540 - Chemistry and allied sciences |
| dewey-raw | 540 |
| dewey-search | 540 |
| dewey-sort | 3540 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik Chemie |
| edition | 2., completely revised and enlarged edition |
| format | Book |
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| genre | (DE-588)4127380-1 Praktikum gnd-content |
| genre_facet | Praktikum |
| id | DE-604.BV043305231 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T07:22:41Z |
| institution | BVB |
| institution_GND | (DE-588)16179388-5 |
| isbn | 9783527335244 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-028726011 |
| oclc_num | 1124790649 |
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| owner_facet | DE-20 DE-703 DE-29T DE-91G DE-BY-TUM DE-11 DE-19 DE-BY-UBM DE-634 |
| physical | xx, 268 Seiten Illustrationen, Diagramme |
| publishDate | 2019 |
| publishDateSearch | 2019 |
| publishDateSort | 2019 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Holze, Rudolf 1954- Verfasser (DE-588)120422026 aut Experimental electrochemistry a laboratory textbook Rudolf Holze 2., completely revised and enlarged edition Weinheim Wiley-VCH [2019] © 2019 xx, 268 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Elektrochemie (DE-588)4014241-3 gnd rswk-swf Chemie Chemistry Electrochemical Analysis Electrochemistry Electronic Materials Elektrochemie Elektrochemische Analytik Elektronische Materialien Materials Science Materialwissenschaften Physikalische Chemie (DE-588)4127380-1 Praktikum gnd-content Elektrochemie (DE-588)4014241-3 s DE-604 Wiley-VCH (DE-588)16179388-5 pbl Erscheint auch als Online-Ausgabe, PDF 978-3-527-67628-6 Erscheint auch als Online-Ausgabe, EPUB 978-3-527-67629-3 http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-33524-4/ Verlag DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028726011&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Holze, Rudolf 1954- Experimental electrochemistry a laboratory textbook Elektrochemie (DE-588)4014241-3 gnd |
| subject_GND | (DE-588)4014241-3 (DE-588)4127380-1 |
| title | Experimental electrochemistry a laboratory textbook |
| title_auth | Experimental electrochemistry a laboratory textbook |
| title_exact_search | Experimental electrochemistry a laboratory textbook |
| title_full | Experimental electrochemistry a laboratory textbook Rudolf Holze |
| title_fullStr | Experimental electrochemistry a laboratory textbook Rudolf Holze |
| title_full_unstemmed | Experimental electrochemistry a laboratory textbook Rudolf Holze |
| title_short | Experimental electrochemistry |
| title_sort | experimental electrochemistry a laboratory textbook |
| title_sub | a laboratory textbook |
| topic | Elektrochemie (DE-588)4014241-3 gnd |
| topic_facet | Elektrochemie Praktikum |
| url | http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-33524-4/ http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028726011&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT holzerudolf experimentalelectrochemistryalaboratorytextbook AT wileyvch experimentalelectrochemistryalaboratorytextbook |