Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Straubing
Verlag Attenkofer
2015
|
| Schriftenreihe: | Nachwachsende Rohstoffe in Forschung und Praxis
12 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | xiv, 144 Seiten Illustrationen, Diagramme |
| ISBN: | 9783942742399 |
Internformat
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| 245 | 1 | 0 | |a Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products |c Abdallah Soubhy Ali Abdraboh |
| 264 | 1 | |a Straubing |b Verlag Attenkofer |c 2015 | |
| 300 | |a xiv, 144 Seiten |b Illustrationen, Diagramme | ||
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| 490 | 1 | |a Nachwachsende Rohstoffe in Forschung und Praxis |v 12 | |
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| adam_text | T
ABLE OF CONTENTS
DEDICATION AND ACKNOWLEDGEM
ENTS..................................................................................................VII
A
BSTRACT......................................................................................................................................................IX
TABLE OF
CONTENTS......................................................................................................................................XI
HISTORICAL P
ERSPECTIVE.............................................................................................................................
1
1
INTRODUCTION.......................................................................................
.
......
.
........................................
2
1.1 GLOBAL
CHALLENGES............................................................................................................................2
1.2 GLOBAL FACILITIES AND FEASIBILITY OF *GLOBAL BIOMASS*
.................................................................3
1.2.1 AGRICULTURAL RESIDUE AVAILABILITY IN E
GYPT.......................................................................
6
1.3 THE IDEA OF
BIO-REFINERY.................................................................................................................
8
1.4 CONCLUSION
...................................................................................................................................
11
2 O
BJECTIVES............................................................................................................................................
14
3 M ATERIALS AND M
ETHODS....................................................................................................................
16
3.1 MATERIAL
...................................................................................................................................
16
3.1.1 RAW MATERIALS
.......................
.
..........................................................................................
16
3.1.2
CHEMICALS...................................................................................
......................................16
3.2 EXPERIMENTAL
PROCEDURES............................................................................................................16
3.2.1 BIO-REFINERY
PROCEDURES....................................................................................................
16
3.2.1.1 MILLING
PROCESS..................................................................................................
16
3.2.1.2 EXTRACTION OF WAX
(DEWAXING).........................................................................
16
3.2.1.3 PRETREATMENT
PROCEDURE.....................................................................................18
3.2.1.4 RECOVERY OF PRODUCT
FRACTIONS..........................................................................18
3.2.1.4.1 SILICA FRACTION
RECOVERY..................................................................................18
3.2.1.4.2 HEMICELLULOSIC FRACTION
RECOVERY..................................................................18
3.2.1.4.3 LIGNIN FRACTION
RECOVERY................................................................................
18
3.2.1.4.4 CELLULOSIC FRACTION
RECOVERY..........................................................................19
3.3 ANALYTICS ......................................................
.
..............................
.
............................................
19
3.3.1 CHEMICAL ANALYSIS OF FEEDSTOCK AND
SOLIDS......................................................................19
3.3.2 MICROSCOPIC EXAMINATIONS AND
CHARACTERIZATION.............................................................
19
3.3.2.1 LIGHT
MICROSCOPY.............................................................................................20
3.3.2.2 SCANNING ELECTRON MICROSCOPE
(SEM)............................................................ 20
3.3.2.3 ENERGY DISPERSIVE X-RAY SPECTROSCOPY (EDX)
..............................................
20
3.3.3 X-RAY DIFFRACTOMETER (XRD) PATTERNS
..............................................................................
20
3.3.4 PARTICLE SIZE DISTRIBUTION ANALYSIS
(PSD).........................................................................20
3.3.5 THERMO-GRAVIMETRIC ANALYSIS (TGA-DSC)
......
.
.................................................... 20
3.3.6 FOURIER-TRANSFORM INFRARED SPECTROSCOPY
(FTIR)........................................................
.
21
3.3.7 ANALYSES OF DEWAXED EXTRACTS
............................
21
3.3.7.1 DETERMINATION OF ALKANES AND PALMITATES
.......................................................
21
3.3.7.2 DETERMINATION OF FREE FATTY
ACIDS......................................................................21
3.3.7.3 DETERMINATION OF TOTAL F ATTY ACIDS
...................................................................
21
3.3.7.4 DETERMINATION OF FREE
ALCOHOLS.........................................................................21
3.3.7.5
DETERMINATION OF TOTAL ALCOHOLS AND
HYDROXYACIDS........................................22
3.3.7.6 DETERMINATION OF
STEROLS.................................................................................
22
3.3.8 GC-MS
METHODS...............................................................................................................22
3.3.9 SUGARS, INHIBITORS AND FERMENTATION PRODUCTS QUANTIFICATION BY
HPLC.........................23
3.3.10 ENZYME
ASSAYS..................................................................................................................
24
3.3.10.1 BRADFORD * S TEST FOR PROTEIN
DETERMINATION....................................................... 24
3.3.10.2 MEASUREMENT OF CELLULASE ACTIVITIES (FPU ASSAY)
...........................................
24
3.4 BIO-CONVERSION PROCESSES (SACCHARIFICATION AND
FERMENTATION)............................................25
3.4.1 ENZYMATIC SACCHARIFICATION FOR THE INSOLUBLE RESIDUE (CELLULOSE
FRACTION)......................25
3.4.2 ENZYME LEVELS, TOTAL SOLID LOAD (TS) AND
SACCHARIFICATION...................................... 25
3.4.3 FERMENTATION
PROCESSES....................................................................................................26
3.4.3.1
MICROORGANISMS..............................................................................................
26
3.4.3.2
INOCULUM............................................................................................................26
3.4.3.3 ETHANOL
FERMENTATION......................................................................................
26
3.4.3.3.1 CULTIVATION MEDIUM *CONTROL MEDIA*
........................................................... 26
3.4.3.3.2 ETHANOL FERMENTATION
MEDIA..........................................................................26
3.4.3.3.1 PRE-TEST ON C-SOURCE
CONSUMPTION................................................................28
3.4.3.3.2 SIMULTANEOUS SACCHARIFICATION AND FERMENTATION (SSF) OF
PRETREATED RICE
STRAW (CELLULOSIC
FRACTION)..............................................................................
28
3.4.3.3.3 PARTIALLY SEPARATED HYDROLYSIS AND FERMENTATION P SHF
.............................
28
3.4.3.4 EPS
FERMENTATION............................................................................................29
3.4.3.4.1 CONTROL CULTIVATION MEDIUM FOR EPS CULTIVATION MEDIUM USING
PRODUCTION
BY
S. ROLFSII
.....................................................................................................29
3.4.3.4.2 EPS FERMENTATION
PROCESS..............................................................................
29
3.4.3.4.3 EPS FERMENTATION
PRODUCTS...........................................................................31
4 FEEDSTOCK ANALYSIS OF EGYPTIAN RICE
STRAW.................................................................................32
4.1 RICE STRAW
STRUCTURE....................................................................................................................32
4.2 LIGNOCELLULOSIC STRUCTURE OF RICE
STRAW.....................................................................................
32
4.3 EXTRACTIVES AND INORGANIC
PROFILES............................................................................................35
4.4 RESULTS OF FEEDSTOCK
ANALYSIS......................................................................................................36
4.4.1 MICROSCOPIC
ANALYSIS........................................................................................................
36
4.4.2 ELEMENTAL ANALYSIS OF RICE STRAW
.....................................................................................
37
4.4.3 STRUCTURAL
COMPOSITION.....................................................................................................39
4.5 SUMMARY AND
CONCLUSION.....................................................................................
.
....................
41
5 BIO-REFINERY AND -CONVERSION PROCESSES OF THE EGYPTIAN RICE STRAW
................................
42
5.1 PRETREATMENT STRATEGIES FOR THE LIGNOCELLULOSIC
BIOMASS........................................................42
5.2 BIO-REFINERY CONCEPT AND PROCEDURE
......................................
.
................................................
45
5.2.1
MILLING...............................................................................................................................
45
5.2.2 EXTRACTION OF WAX
(DEWAXING)................................................................
46
5.2.3
PRETREATMENT......................................................................................................................
46
5.2.3.1 PRETREATMENT
PROCEDURE...................................................................................48
5.2.4 RECOVERY OF PRODUCT
FRACTIONS..........................................................................................49
* SILICA FRACTION
RECOVERY...............................................................................................
49
* HEMICELLULOSIC FRACTION
RECOVERY...............................................................................
49
* LIGNIN FRACTION
RECOVERY.............................................................................................
49
* CELLULOSIC FRACTION
RECOVERY........................................................................................49
5.2.5 BIO-CONVERSION
PROCESSES................................................................................................
49
5
.3 RESULTS AND DISCUSSION OF THE BIO-REFINERY CONCEPT OF RICE STRAW
.........................................
50
5.3.1 MASS BALANCE OF ALL BIO-REFINERY
STEPS............................................................................50
5.3.2 REDUCING SUGARS BALANCE OF ALL BIO-REFINERY
STEPS..........................................................51
5.4 SUMMARY AND CONCLUSION OF
BIO-REFINERY.................................................................................52
6 BIOGENIC W AX AND STEROLS AS BIO-REFINERY
BY-PRODUCTS........................................................54
6.1
INTRODUCTION..................................................................................................................................54
6.1.1 COMPOSITION OF PLANT WAX
LAYERS....................................................................................
54
6.1.2 GC-MS ANALYSIS FOR CHARACTERIZATION OF WAX COMPOUNDS
.........
...................................
56
6.2 EXTRACTION PROCEDURES APPLIED FOR DEWAXING
..........................................................................
57
6.3 RESULTS AND
DISCUSSION................................................................................................................
57
6.3.1 MICROSCOPIC
EXAMINATION................................................................................................
57
6.3.2 RECOVERY OF EXTRACTIVES BY THE DIFFERENT EXTRACTION SYSTEMS
........................................
59
6.3.2.1 OVERALL EXTRACTIVES
YIELDS.................................................................................
59
6.3.2.2 TOTAL AND FREE FATTY
ACIDS..................................................................................60
6.3.2.3 EXTRACTION OF
ALKANES.......................................................................................
62
6.3.2.4 TOTAL AND FREE FATTY ALCOHOLS
...........................................................................
63
6.3.2.5 EXTRACTION OF
PHYTOSTEROLS.................................................................................64
6.4 SUMMARY AND
CONCLUSION...........................................................................................................65
7 BIOGENIC SILICA AS VALUABLE PRODUCT FROM RICE STRAW
.............................................................
68
7.1
INTRODUCTION..................................................................................................................................68
7.2 RESULTS AND DISCUSSION OF SILICA FRACTION
ANALYSIS....................................................................69
7.2.1 SEM OF RICE
STRAW............................................................................................................69
7.2.2 CHARACTERIZATION OF SILICA PRODUCED FROM RICE STRAW
.....................................................
70
7.2.2.1 SEM AND PARTICLE SIZE DISTRIBUTION
(PSD)................................... 70
12.2.2
FT-IR
SPECTRUM................................................................................................71
7.2.2.3 RECOVERY OF SILICA AND SEM-EDX SPECTROMETRIE DATA
....................................
73
7.3 SUMMARY AND
CONCLUSION...........................................................................................................74
8 CELLULOSIC FIBERS AS REFINERY PRODUCTS FROM RICE STRAW
.........................................................76
8.1
INTRODUCTION..................................................................................................................................76
8.2 RESULTS
..................................................................................................................................
77
8.2.1 RECOVERY OF CELLULOSIC FRACTIONS FROM RICE
STRAW...........................................................77
8.2.2 FOURIER-TRANSFORM INFRARED SPECTROSCOPY (FTIR)
...........................................................
77
8.2.3 DSC AND TGA
ANALYSIS..............................................................................
79
8.2.4 SEM OF CELLULOSIC
FRACTION...............................................................................................
80
8.2.5 CRYSTALLINITY AND PARTICLE
SIZE..........................................................................................81
8.3 SUMMARY AND
CONCLUSION...........................................................................................................83
9 CELLULOSIC ETHANOL PRODUCTION FROM PRETREATED RICE STRA W
.................................................86
9.1
INTRODUCTION..................................................................................................................................86
9.2 RESULTS AND
DISCUSSIONS...............................................................................................................
89
9.2.1 PRE-TEST ON C-SOURCE
CONSUMPTION..................................................................................89
9.2.2 SACCHARIFICATION AND FERMENTATION PROCESS OF PRETREATED RICE STRAW
..............................
91
9
.2.2.1 ENZYME
ACTIVITIES..............................................................................................
92
9.2.2.2 ENZYMES
LEVEL...................................................................................................92
9.2.2.3 TOTAL SOLID
LOAD..................................................................................................95
9.2.2A SIMULTANEOUS SACCHARIFICATION AND FERMENTATION (SSE)
.................................
97
9.2.3 SSE USING OKARA AS AN ALTERNATIVE
N-SOURCE....................................................................98
9.2.3.1 CHARACTERIZATION OF OKARA
...................................
98
9.2.3.2 ESTABLISHMENT OF FERMENTATION MEDIA USING PRETREATED RICE STRAW
AND OKARA AS
ALTERNATIVE
N-SOURCE..........................................................................................
99
9.2.3.3 ETHANOL FERMENTATION BY VARYING THE OKARA CONCENTRATIONS USED
.................
104
9.3
CONCLUSIONS................................................................................................................................
108
10 EXOPOLYSACCHARIDE *SCLEROGLUCAN* PRODUCTION FROM RICE STRAW BY
SCLEROTIUM ROLFSII
.............................................................................................................................................................110
10.1
INTRODUCTION.................................................................................................................................110
10.2 RESULTS AND
DISCUSSION...............................................................................................................
114
10.2.1 ESP-F
ERMENTATION...........................................................................................................114
10.2.2 PARTIAL-SEPARATION AND HYDROLYSIS FOLLOWED BY FERMENTATION (P
SHF)
........................
117
10.3 SUMMARY AND
CONCLUSION..........................................................................................................121
11 SUM M
ARY...........................................................................................................................................122
12 R
EFERENCES..........................................................................................................................................124
LIST OF FIGU
RES.......................................................................................................................................
132
LIST OF T A B
LE...........................................................................................................................................136
LIST OF
ABBREVIATIONS...........................................................................................................................140
CURRICULUM VITAE
144
|
| any_adam_object | 1 |
| author | Abdraboh, Abdallah Soubhy Ali 1980- |
| author_GND | (DE-588)108400822X |
| author_facet | Abdraboh, Abdallah Soubhy Ali 1980- |
| author_role | aut |
| author_sort | Abdraboh, Abdallah Soubhy Ali 1980- |
| author_variant | a s a a asa asaa |
| building | Verbundindex |
| bvnumber | BV043299829 |
| classification_tum | CIT 945d CIT 647d CIT 680d |
| ctrlnum | (OCoLC)951252977 (DE-599)BVBBV043299829 |
| discipline | Chemie-Ingenieurwesen Biotechnologie |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV043299829 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T07:22:34Z |
| institution | BVB |
| isbn | 9783942742399 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-028720742 |
| oclc_num | 951252977 |
| open_access_boolean | |
| owner | DE-M49 DE-BY-TUM DE-91 DE-BY-TUM DE-12 DE-91S DE-BY-TUM DE-634 |
| owner_facet | DE-M49 DE-BY-TUM DE-91 DE-BY-TUM DE-12 DE-91S DE-BY-TUM DE-634 |
| physical | xiv, 144 Seiten Illustrationen, Diagramme |
| publishDate | 2015 |
| publishDateSearch | 2015 |
| publishDateSort | 2015 |
| publisher | Verlag Attenkofer |
| record_format | marc |
| series | Nachwachsende Rohstoffe in Forschung und Praxis |
| series2 | Nachwachsende Rohstoffe in Forschung und Praxis |
| spelling | Abdraboh, Abdallah Soubhy Ali 1980- Verfasser (DE-588)108400822X aut Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products Abdallah Soubhy Ali Abdraboh Straubing Verlag Attenkofer 2015 xiv, 144 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Nachwachsende Rohstoffe in Forschung und Praxis 12 Dissertation Technische Universität München 2015 Bioraffinerie (DE-588)7742513-3 gnd rswk-swf Bioreaktor (DE-588)4006780-4 gnd rswk-swf Lignocellulosehaltiger Rohstoff (DE-588)4206021-7 gnd rswk-swf Strohverarbeitung (DE-588)4396665-2 gnd rswk-swf Reis (DE-588)4049271-0 gnd rswk-swf Cellulosegewinnung (DE-588)4391003-8 gnd rswk-swf Biokraftstoff (DE-588)4145658-0 gnd rswk-swf Herstellung (DE-588)4159653-5 gnd rswk-swf Biokonversion (DE-588)4145610-5 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Bioraffinerie (DE-588)7742513-3 s Reis (DE-588)4049271-0 s Strohverarbeitung (DE-588)4396665-2 s Lignocellulosehaltiger Rohstoff (DE-588)4206021-7 s Biokonversion (DE-588)4145610-5 s Biokraftstoff (DE-588)4145658-0 s Herstellung (DE-588)4159653-5 s Cellulosegewinnung (DE-588)4391003-8 s DE-604 Bioreaktor (DE-588)4006780-4 s b DE-604 Nachwachsende Rohstoffe in Forschung und Praxis 12 (DE-604)BV035709535 12 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028720742&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Abdraboh, Abdallah Soubhy Ali 1980- Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products Nachwachsende Rohstoffe in Forschung und Praxis Bioraffinerie (DE-588)7742513-3 gnd Bioreaktor (DE-588)4006780-4 gnd Lignocellulosehaltiger Rohstoff (DE-588)4206021-7 gnd Strohverarbeitung (DE-588)4396665-2 gnd Reis (DE-588)4049271-0 gnd Cellulosegewinnung (DE-588)4391003-8 gnd Biokraftstoff (DE-588)4145658-0 gnd Herstellung (DE-588)4159653-5 gnd Biokonversion (DE-588)4145610-5 gnd |
| subject_GND | (DE-588)7742513-3 (DE-588)4006780-4 (DE-588)4206021-7 (DE-588)4396665-2 (DE-588)4049271-0 (DE-588)4391003-8 (DE-588)4145658-0 (DE-588)4159653-5 (DE-588)4145610-5 (DE-588)4113937-9 |
| title | Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products |
| title_auth | Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products |
| title_exact_search | Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products |
| title_full | Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products Abdallah Soubhy Ali Abdraboh |
| title_fullStr | Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products Abdallah Soubhy Ali Abdraboh |
| title_full_unstemmed | Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products Abdallah Soubhy Ali Abdraboh |
| title_short | Bio-refinery and -conversion of lignocellulosic rice straw to produce biofuel and high valuable by-products |
| title_sort | bio refinery and conversion of lignocellulosic rice straw to produce biofuel and high valuable by products |
| topic | Bioraffinerie (DE-588)7742513-3 gnd Bioreaktor (DE-588)4006780-4 gnd Lignocellulosehaltiger Rohstoff (DE-588)4206021-7 gnd Strohverarbeitung (DE-588)4396665-2 gnd Reis (DE-588)4049271-0 gnd Cellulosegewinnung (DE-588)4391003-8 gnd Biokraftstoff (DE-588)4145658-0 gnd Herstellung (DE-588)4159653-5 gnd Biokonversion (DE-588)4145610-5 gnd |
| topic_facet | Bioraffinerie Bioreaktor Lignocellulosehaltiger Rohstoff Strohverarbeitung Reis Cellulosegewinnung Biokraftstoff Herstellung Biokonversion Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028720742&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV035709535 |
| work_keys_str_mv | AT abdrabohabdallahsoubhyali biorefineryandconversionoflignocellulosicricestrawtoproducebiofuelandhighvaluablebyproducts |