Solid-state NMR: basic principles & practice
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| Format: | Elektronisch E-Book |
| Sprache: | English |
| Veröffentlicht: |
[New York, N.Y.] (222 East 46th Street, New York, NY 10017)
Momentum Press
2012
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| Schlagworte: | |
| Online-Zugang: | FAW01 FAW02 Volltext |
| Beschreibung: | Title from PDF t.p. (viewed on September 13, 2012) Includes bibliographical references and index Preface -- About the authors -- 1. Introduction -- 1.1 The utility of NMR -- 1.2 A preview of solid-state NMR spectra -- 1.3 The solid state -- 1.4 Polymorphism, solvates, co-crystals & host:guest systems -- 1.5 NMR of solids & the periodic table -- 2. Basic NMR concepts for solids -- 2.1 Nuclear spin magnetization -- 2.2 Tensors -- 2.3 Shielding -- 2.4 Indirect coupling -- 2.5 Dipolar coupling -- 2.6 Quadrupolar coupling -- 2.7 Magic-angle spinning -- 2.8 Relaxation -- 3. Spin-1/2 nuclei: a practical guide -- 3.1 Introduction -- 3.2 The vector model & the rotating frame of reference -- 3.3 The components of an NMR experiment -- 3.4 Cross polarization -- 3.5 High-resolution spectra from 1H (& 19F) -- 4. Quantum mechanics of solid-state NMR -- 4.1 Introduction -- 4.2 The Hamiltonians of NMR -- 4.3 The density matrix -- 4.4 Density operator treatments of simple NMR experiments -- 4.5 The density matrix for coupled spins -- 4.6 Euler angles & spherical tensors -- 4.7 Additional analytical tools -- 5. Going further with spin-1/2 solid-state NMR -- 5.1 Introduction -- 5.2 Linewidths in solid-state NMR -- 5.3 Exploiting indirect (J) couplings in solids -- 5.4 Spectral correlation experiments -- 5.5 Homonuclear decoupling -- 5.6 Using correlation experiments for spectral assignment -- 5.7 Further applications -- 6. Quadrupolar nuclei -- 6.1 Introduction -- 6.2 Characteristics of first-order quadrupolar spectra -- 6.3 First-order energy levels & spectra -- 6.4 Second-order zero-asymmetry cases -- 6.5 Spectra for cases with non-zero asymmetry: central transition -- 6.6 Recording one-dimensional spectra of quadrupolar nuclei -- 6.7 Manipulating the quadrupolar effect -- 6.8 Spectra for integral spins -- 7. Relaxation, exchange & quantitation -- 7.1 Introduction -- 7.2 Relaxation -- 7.3 Exchange -- 7.4 Quantitative NMR -- 7.5 Paramagnetic systems -- 8. Analysis & interpretation -- 8.1 Introduction -- 8.2 Quantitative measurement of anisotropies -- 8.3 Measurement of dipolar couplings -- 8.4 Quantifying indirect (J) couplings -- 8.5 Tensor interplay -- 8.6 Effects of quadrupolar nuclei on spin-1/2 spectra -- 8.7 Quantifying relationships between tensors -- 8.8 NMR crystallography -- Appendices -- A. The spin properties of spin-1/2 nuclides -- B. The spin properties of quadrupolar nuclides -- C. Liouville space, relaxation & exchange -- C.1 Introduction to Liouville space -- C.2 Application to relaxation -- C.3 Application to chemical exchange -- D. Introduction to solid-state NMR simulation -- D.1 Specifying the spin system -- D.2 Specifying the powder sampling -- D.3 Specifying the pulse sequence -- D.4 Efficiency of calculation -- Index Nuclear magnetic resonance (NMR) has proved to be a uniquely powerful and versatile spectroscopy, and no modern university chemistry department or industrial chemistry laboratory is complete without a suite of NMR spectrometers. The phenomenon of nuclear spin may seem an odd basis for an analytical tool, but it is the relative isolation of the nuclear spin from its surroundings that makes it an ideal noninterfering probe of the electronic environment. Different sites are clearly identified by their chemical shifts, while J couplings in 1H spectra provide connectivity information. The combination of these two complementary interactions, plus the formidable array of different NMR experiments developed since the arrival of Fourier transform NMR in 1966, has revolutionized the practice of chemistry |
| Beschreibung: | 1 electronic text (xiv, 276 p.) |
| ISBN: | 1606503529 9781606503522 |
Internformat
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| 500 | |a Includes bibliographical references and index | ||
| 500 | |a Preface -- About the authors -- | ||
| 500 | |a 1. Introduction -- 1.1 The utility of NMR -- 1.2 A preview of solid-state NMR spectra -- 1.3 The solid state -- 1.4 Polymorphism, solvates, co-crystals & host:guest systems -- 1.5 NMR of solids & the periodic table -- | ||
| 500 | |a 2. Basic NMR concepts for solids -- 2.1 Nuclear spin magnetization -- 2.2 Tensors -- 2.3 Shielding -- 2.4 Indirect coupling -- 2.5 Dipolar coupling -- 2.6 Quadrupolar coupling -- 2.7 Magic-angle spinning -- 2.8 Relaxation -- | ||
| 500 | |a 3. Spin-1/2 nuclei: a practical guide -- 3.1 Introduction -- 3.2 The vector model & the rotating frame of reference -- 3.3 The components of an NMR experiment -- 3.4 Cross polarization -- 3.5 High-resolution spectra from 1H (& 19F) -- | ||
| 500 | |a 4. Quantum mechanics of solid-state NMR -- 4.1 Introduction -- 4.2 The Hamiltonians of NMR -- 4.3 The density matrix -- 4.4 Density operator treatments of simple NMR experiments -- 4.5 The density matrix for coupled spins -- 4.6 Euler angles & spherical tensors -- 4.7 Additional analytical tools -- | ||
| 500 | |a 5. Going further with spin-1/2 solid-state NMR -- 5.1 Introduction -- 5.2 Linewidths in solid-state NMR -- 5.3 Exploiting indirect (J) couplings in solids -- 5.4 Spectral correlation experiments -- 5.5 Homonuclear decoupling -- 5.6 Using correlation experiments for spectral assignment -- 5.7 Further applications -- | ||
| 500 | |a 6. Quadrupolar nuclei -- 6.1 Introduction -- 6.2 Characteristics of first-order quadrupolar spectra -- 6.3 First-order energy levels & spectra -- 6.4 Second-order zero-asymmetry cases -- 6.5 Spectra for cases with non-zero asymmetry: central transition -- 6.6 Recording one-dimensional spectra of quadrupolar nuclei -- 6.7 Manipulating the quadrupolar effect -- 6.8 Spectra for integral spins -- | ||
| 500 | |a 7. Relaxation, exchange & quantitation -- 7.1 Introduction -- 7.2 Relaxation -- 7.3 Exchange -- 7.4 Quantitative NMR -- 7.5 Paramagnetic systems -- | ||
| 500 | |a 8. Analysis & interpretation -- 8.1 Introduction -- 8.2 Quantitative measurement of anisotropies -- 8.3 Measurement of dipolar couplings -- 8.4 Quantifying indirect (J) couplings -- 8.5 Tensor interplay -- 8.6 Effects of quadrupolar nuclei on spin-1/2 spectra -- 8.7 Quantifying relationships between tensors -- 8.8 NMR crystallography -- | ||
| 500 | |a Appendices -- A. The spin properties of spin-1/2 nuclides -- B. The spin properties of quadrupolar nuclides -- C. Liouville space, relaxation & exchange -- C.1 Introduction to Liouville space -- C.2 Application to relaxation -- C.3 Application to chemical exchange -- D. Introduction to solid-state NMR simulation -- D.1 Specifying the spin system -- D.2 Specifying the powder sampling -- D.3 Specifying the pulse sequence -- D.4 Efficiency of calculation -- Index | ||
| 500 | |a Nuclear magnetic resonance (NMR) has proved to be a uniquely powerful and versatile spectroscopy, and no modern university chemistry department or industrial chemistry laboratory is complete without a suite of NMR spectrometers. The phenomenon of nuclear spin may seem an odd basis for an analytical tool, but it is the relative isolation of the nuclear spin from its surroundings that makes it an ideal noninterfering probe of the electronic environment. Different sites are clearly identified by their chemical shifts, while J couplings in 1H spectra provide connectivity information. The combination of these two complementary interactions, plus the formidable array of different NMR experiments developed since the arrival of Fourier transform NMR in 1966, has revolutionized the practice of chemistry | ||
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| 650 | 4 | |a Chemie | |
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Datensatz im Suchindex
| _version_ | 1804175549739827200 |
|---|---|
| any_adam_object | |
| author | Apperley, David C. |
| author_facet | Apperley, David C. |
| author_role | aut |
| author_sort | Apperley, David C. |
| author_variant | d c a dc dca |
| building | Verbundindex |
| bvnumber | BV043120638 |
| classification_rvk | VG 9500 |
| collection | ZDB-4-EBA |
| ctrlnum | (OCoLC)809804677 (DE-599)BVBBV043120638 |
| dewey-full | 543.0877 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543.0877 |
| dewey-search | 543.0877 |
| dewey-sort | 3543.0877 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Electronic eBook |
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| id | DE-604.BV043120638 |
| illustrated | Not Illustrated |
| indexdate | 2024-07-10T07:18:04Z |
| institution | BVB |
| isbn | 1606503529 9781606503522 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-028544829 |
| oclc_num | 809804677 |
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| physical | 1 electronic text (xiv, 276 p.) |
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| publisher | Momentum Press |
| record_format | marc |
| spelling | Apperley, David C. Verfasser aut Solid-state NMR basic principles & practice David C. Apperley, Robin K. Harris & Paul Hodgkinson [New York, N.Y.] (222 East 46th Street, New York, NY 10017) Momentum Press 2012 1 electronic text (xiv, 276 p.) txt rdacontent c rdamedia cr rdacarrier Title from PDF t.p. (viewed on September 13, 2012) Includes bibliographical references and index Preface -- About the authors -- 1. Introduction -- 1.1 The utility of NMR -- 1.2 A preview of solid-state NMR spectra -- 1.3 The solid state -- 1.4 Polymorphism, solvates, co-crystals & host:guest systems -- 1.5 NMR of solids & the periodic table -- 2. Basic NMR concepts for solids -- 2.1 Nuclear spin magnetization -- 2.2 Tensors -- 2.3 Shielding -- 2.4 Indirect coupling -- 2.5 Dipolar coupling -- 2.6 Quadrupolar coupling -- 2.7 Magic-angle spinning -- 2.8 Relaxation -- 3. Spin-1/2 nuclei: a practical guide -- 3.1 Introduction -- 3.2 The vector model & the rotating frame of reference -- 3.3 The components of an NMR experiment -- 3.4 Cross polarization -- 3.5 High-resolution spectra from 1H (& 19F) -- 4. Quantum mechanics of solid-state NMR -- 4.1 Introduction -- 4.2 The Hamiltonians of NMR -- 4.3 The density matrix -- 4.4 Density operator treatments of simple NMR experiments -- 4.5 The density matrix for coupled spins -- 4.6 Euler angles & spherical tensors -- 4.7 Additional analytical tools -- 5. Going further with spin-1/2 solid-state NMR -- 5.1 Introduction -- 5.2 Linewidths in solid-state NMR -- 5.3 Exploiting indirect (J) couplings in solids -- 5.4 Spectral correlation experiments -- 5.5 Homonuclear decoupling -- 5.6 Using correlation experiments for spectral assignment -- 5.7 Further applications -- 6. Quadrupolar nuclei -- 6.1 Introduction -- 6.2 Characteristics of first-order quadrupolar spectra -- 6.3 First-order energy levels & spectra -- 6.4 Second-order zero-asymmetry cases -- 6.5 Spectra for cases with non-zero asymmetry: central transition -- 6.6 Recording one-dimensional spectra of quadrupolar nuclei -- 6.7 Manipulating the quadrupolar effect -- 6.8 Spectra for integral spins -- 7. Relaxation, exchange & quantitation -- 7.1 Introduction -- 7.2 Relaxation -- 7.3 Exchange -- 7.4 Quantitative NMR -- 7.5 Paramagnetic systems -- 8. Analysis & interpretation -- 8.1 Introduction -- 8.2 Quantitative measurement of anisotropies -- 8.3 Measurement of dipolar couplings -- 8.4 Quantifying indirect (J) couplings -- 8.5 Tensor interplay -- 8.6 Effects of quadrupolar nuclei on spin-1/2 spectra -- 8.7 Quantifying relationships between tensors -- 8.8 NMR crystallography -- Appendices -- A. The spin properties of spin-1/2 nuclides -- B. The spin properties of quadrupolar nuclides -- C. Liouville space, relaxation & exchange -- C.1 Introduction to Liouville space -- C.2 Application to relaxation -- C.3 Application to chemical exchange -- D. Introduction to solid-state NMR simulation -- D.1 Specifying the spin system -- D.2 Specifying the powder sampling -- D.3 Specifying the pulse sequence -- D.4 Efficiency of calculation -- Index Nuclear magnetic resonance (NMR) has proved to be a uniquely powerful and versatile spectroscopy, and no modern university chemistry department or industrial chemistry laboratory is complete without a suite of NMR spectrometers. The phenomenon of nuclear spin may seem an odd basis for an analytical tool, but it is the relative isolation of the nuclear spin from its surroundings that makes it an ideal noninterfering probe of the electronic environment. Different sites are clearly identified by their chemical shifts, while J couplings in 1H spectra provide connectivity information. The combination of these two complementary interactions, plus the formidable array of different NMR experiments developed since the arrival of Fourier transform NMR in 1966, has revolutionized the practice of chemistry SCIENCE / Chemistry / Analytic bisacsh Nuclear magnetic resonance spectroscopy fast NMR-Spektroskopie gnd Festkörper gnd Chemie Nuclear magnetic resonance spectroscopy NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Festkörper (DE-588)4016918-2 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 s Festkörper (DE-588)4016918-2 s 1\p DE-604 Harris, Robin K. Sonstige oth Hodgkinson, Paul Sonstige oth Erscheint auch als Druckausgabe 1-60650-350-2 Erscheint auch als Druckausgabe 978-1-60650-350-8 http://search.ebscohost.com/login.aspx?direct=true&scope=site&db=nlebk&db=nlabk&AN=501147 Aggregator Volltext 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Apperley, David C. Solid-state NMR basic principles & practice SCIENCE / Chemistry / Analytic bisacsh Nuclear magnetic resonance spectroscopy fast NMR-Spektroskopie gnd Festkörper gnd Chemie Nuclear magnetic resonance spectroscopy NMR-Spektroskopie (DE-588)4075421-2 gnd Festkörper (DE-588)4016918-2 gnd |
| subject_GND | (DE-588)4075421-2 (DE-588)4016918-2 |
| title | Solid-state NMR basic principles & practice |
| title_auth | Solid-state NMR basic principles & practice |
| title_exact_search | Solid-state NMR basic principles & practice |
| title_full | Solid-state NMR basic principles & practice David C. Apperley, Robin K. Harris & Paul Hodgkinson |
| title_fullStr | Solid-state NMR basic principles & practice David C. Apperley, Robin K. Harris & Paul Hodgkinson |
| title_full_unstemmed | Solid-state NMR basic principles & practice David C. Apperley, Robin K. Harris & Paul Hodgkinson |
| title_short | Solid-state NMR |
| title_sort | solid state nmr basic principles practice |
| title_sub | basic principles & practice |
| topic | SCIENCE / Chemistry / Analytic bisacsh Nuclear magnetic resonance spectroscopy fast NMR-Spektroskopie gnd Festkörper gnd Chemie Nuclear magnetic resonance spectroscopy NMR-Spektroskopie (DE-588)4075421-2 gnd Festkörper (DE-588)4016918-2 gnd |
| topic_facet | SCIENCE / Chemistry / Analytic Nuclear magnetic resonance spectroscopy NMR-Spektroskopie Festkörper Chemie |
| url | http://search.ebscohost.com/login.aspx?direct=true&scope=site&db=nlebk&db=nlabk&AN=501147 |
| work_keys_str_mv | AT apperleydavidc solidstatenmrbasicprinciplespractice AT harrisrobink solidstatenmrbasicprinciplespractice AT hodgkinsonpaul solidstatenmrbasicprinciplespractice |