Beryllium: environmental analysis and monitoring
Gespeichert in:
Format: | Elektronisch E-Book |
---|---|
Sprache: | English |
Veröffentlicht: |
Cambridge
Royal Society of Chemistry
c2009
|
Schlagworte: | |
Online-Zugang: | FAW01 FAW02 Volltext |
Beschreibung: | Introduction: Purpose or Background-- Methods-- Summary. Chapter 1: Overview of Beryllium Sampling and Analysis. Introduction-- Background-- Beryllium Sources-- Industrial Uses-- Health Risks-- Natural Versus Anthropogenic-- Carcinogenicity-- Acute Beryllium Disease-- Chronic Beryllium Disease-- Occupational Exposure Limits-- History-- Current Limits-- Trends-- Impact of U.S. Department of Energy Beryllium Rule-- Environmental Remediation-- Sampling Overview-- Air Sampling-- Surface Sampling-- Dermal Sampling-- Soil Sampling-- Analysis Overview: Summary of Current Techniques-- Need for Improved Performance-- Need for Real-Time Monitoring-- Goals of This Book (Summary). Chapter 2: Air Sampling. Introduction-- Purpose of Air Sampling and Choice of Strategy-- Sampling for Compliance with a Limit Value-- Sampling to Determine the Effectiveness of Control Measures-- Sampling to Identify a Group Range of Exposures-- Identification of a Homogenous Exposure Group (HEG)-- - Determining the Range of Exposures of a HEG-- Sampling for Prospective Health Studies-- Methods of Air Sampling-- Properties and Behaviors of Aerosols-- Sources of Beryllium Aerosols-- Sampling for Non-volatile Aerosols Using Filters-- Size-selective Sampling-- Inhalable Sampling-- Respirable Sampling-- High-volume Sampling-- Sampling for Volatile Aerosols-- Sampling for Ultrafine Aerosols-- Metrics for Ultrafine Particles-- Analytical Considerations for Selecting a Sampling Method-- Retrospective Exposure Assessments-- Determining a Job-exposure Matrix (JEM)-- Cumulative vs Peak Exposures in Assessing Exposure Histories-- Summary. Chapter 3: Successful Surface Sampling for Beryllium. Introduction-- Background-- Wipe Sampling - Dry, Wet, Alcohol-- Bulk Sampling - Sweep, Vacuum, HEPA Sock-- Methods-- Sampling Safety-- Planning Meetings - Before and During Sampling Campaigns-- Communication-- Personal Factors-- Personal Protection Equipment (PPE)-- Protecting the Sampler-- - Protecting the Sample-- Sample Planning - Avoiding Surprises and Delays-- Getting Organized - The Plan - Large or Small-- Sampling Campaign Type, Scope and Strategy-- Detailed Sampling Plan and Agreement to Follow-- Sampling Safety Plan Included-- Include Site History in Plan-- Possible Interferences Identified-- Time Line & Locations of Beryllium Work-- Time Line & Locations of Interferences Work-- Beryllium in Naturally Occurring Materials-- Recordkeeping-- Chain-Of-Custody-- Oversight - Method - Assignments - Reports - Forms-- Locations of Sample Points and Number of Samples - How Determined-- Random Selection Sample Points-- Biased Sample Points-- Sampling Techniques and Requirements Detailed-- Photography Requirements and Permits-- Analysis of Samples - Pre-Qualifying and Selection of the Laboratory-- Quality Control Measures-- Data Reduction Format-- Final Report Parameters-- Cost Considerations - What is Desired vs. What is Needed-- Sampling Supplies-- Consumables-- - Hand Tools-- Power Equipment, Cords and Work Carts-- Sampling Team Needs - Lunches and Other Logistics-- Trash and Waste Collection and Disposal-- Surface Sampling - When To Do What and Why-- Regulatory Requirements for Sampling-- Sampling Methods-- Surface Clean, Dusty or Dirty-- Wipe vs. Bulk-- Dry Wipe vs. Wet Wipe vs. Alcohol Wipe-- Bulk Sampling-- Determining Surface Area-- Recordkeeping and Photography-- Protection of Sample Process and Samples from Contamination-- Obtaining the Sample-- Sampling for Release of Items from Radiologically Contaminated Areas-- Summary. Chapter 4: Sample Dissolution Reagents for Beryllium. Introduction: Background-- Methods of Sample Preparation in Geological Media-- Beryllium Ores-- Soils and Silicates-- Methods of Sample Preparation for Occupational Hygiene Samples-- Workplace Air Samples-- Surface Samples-- Bulk Samples-- Summary. Chapter 5: Heating Sources for Beryllium Sample Preparation. Introduction-- Purpose of Heating-- - Kinetics of Dissolution-- Issues with Particulates-- Issues with Speciation-- Methods-- Mechanical Agitation-- Limitations/Requirements-- Advantages-- Examples (Soils)-- Thermal Heating-- Limitations/Requirements-- Advantages-- Examples (Ashing, Hot Acid, Hot Ammoniumbifluoride)-- Sonication-- Limitations/Requirements-- Advantages-- Examples-- Microwave-- Limitations/Requirements-- Advantages-- Examples (Combine with Acid for ICP)-- Selected Comparisons-- Filters-- Comparison of Heating Methods on Recovery for Ammonium Bifluoride Dissolution-- Soils-- Summary. Chapter 6: Inductively Coupled Plasma Atomic Emission Spectrometry And Inductively Coupled Plasma Mass Spectrometry. Introduction-- Background-- Concept of ICP analysis and AES and MS detection-- Methods - Preparation of Samples-- Methods Available-- Analytical Considerations for Selecting a Sample Preparation Method-- Challenges with Beryllium Samples for Analysis by ICP-AES or ICP-MS-- Quality Control/Quality Assurance-- - Methods - Analysis by ICP-AES-- Instrumentation (tentative)-- Selection of Line (Intensity, Detection Limit)-- Interferences (Background, Spectral, Suppression)-- Need to Know Other Constituents-- How to Correct (Different Wavelength, Correction Factor)-- Sensitivity-- Matrix Effects-- Analytical Methods-- Considerations when Working with Beryllium-- Methods - Analysis by ICP/MS-- Instrumentation-- The Mass Spectrum-- Interferences-- Sensitivity-- Matrix Effects-- Analytical Methods-- Considerations when Working with Beryllium-- Tables/Charts: Summary of Prep Methods-- Spectrum with Example of Potential Interferences. Summary. Chapter 7: Analysis by Non-Plasma Sources. Introduction-- Background-- Methods-- Atomic Absorption-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- UV-Visible-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- Fluorescence-- Methodology-- Detection Limits-- Interferences and Limitations-- - Applications-- Electrochemistry-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- Laser Induced Breakdown Spectroscopy (LIBS)-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- Summary. Chapter 8: Data Reporting & Communications. Introduction-- Background-- Terminology-- Data Censoring-- Challenges in Evaluating Censored Data-- Other Fundamental Concepts-- Methods-- Evaluation Based on Individual Data Points-- Laboratory Reporting Limits-- Basis, Pros and Cons-- Evaluation Based on Data Sets-- Data/Measurement Quality Objectives-- Basis, Pros and Cons-- Uncensored Data-- What It Is-- When It May Be Useful-- When Not to Use It-- Considerations for Laboratories and Clients-- Project Planning-- Laboratory Integration in Project Design Decisions-- Quality Control-- Quality Assurance-- Beryllium Data Reporting-- Preparation (Before Analysis)-- Instrumentation-- Qualities of Reported Data-- - Quantitation as a Substitute for Uncertainty Reporting-- Communicating Results-- Laboratory to Client-- Data Evaluation-- Communication to Managers and Stakeholders-- Summary. Chapter 9: Applications, Future Trends, and Opportunities. Applications of Current Technologies-- Uses of Analytical Measurements-- Diagnostic Sampling-- Exposure Assessment-- Exposure Surveillance-- Data Evaluation-- Data Quality Objectives-- Data Sets Versus Data Points-- Precision/Bias Versus Uncertainty Budgets-- Future Trends and Opportunities-- Drivers for Change-- Occupational Exposure Limits-- Real-Time Monitoring-- Size-Selective Sampling-- Technology Improvements-- Sampling-- Analysis-- Data Evaluation-- Exposure-- Assessment Strategies-- Summary This comprehensive book describes all aspects of the current sampling and analysis techniques for trace-level beryllium in the workplace |
Beschreibung: | 1 Online-Ressource |
ISBN: | 1847559670 9781847559678 |
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500 | |a Introduction: Purpose or Background-- Methods-- Summary. Chapter 1: Overview of Beryllium Sampling and Analysis. Introduction-- Background-- Beryllium Sources-- Industrial Uses-- Health Risks-- Natural Versus Anthropogenic-- Carcinogenicity-- Acute Beryllium Disease-- Chronic Beryllium Disease-- Occupational Exposure Limits-- History-- Current Limits-- Trends-- Impact of U.S. Department of Energy Beryllium Rule-- Environmental Remediation-- Sampling Overview-- Air Sampling-- Surface Sampling-- Dermal Sampling-- Soil Sampling-- Analysis Overview: Summary of Current Techniques-- Need for Improved Performance-- Need for Real-Time Monitoring-- Goals of This Book (Summary). Chapter 2: Air Sampling. Introduction-- Purpose of Air Sampling and Choice of Strategy-- Sampling for Compliance with a Limit Value-- Sampling to Determine the Effectiveness of Control Measures-- Sampling to Identify a Group Range of Exposures-- Identification of a Homogenous Exposure Group (HEG)-- | ||
500 | |a - Determining the Range of Exposures of a HEG-- Sampling for Prospective Health Studies-- Methods of Air Sampling-- Properties and Behaviors of Aerosols-- Sources of Beryllium Aerosols-- Sampling for Non-volatile Aerosols Using Filters-- Size-selective Sampling-- Inhalable Sampling-- Respirable Sampling-- High-volume Sampling-- Sampling for Volatile Aerosols-- Sampling for Ultrafine Aerosols-- Metrics for Ultrafine Particles-- Analytical Considerations for Selecting a Sampling Method-- Retrospective Exposure Assessments-- Determining a Job-exposure Matrix (JEM)-- Cumulative vs Peak Exposures in Assessing Exposure Histories-- Summary. Chapter 3: Successful Surface Sampling for Beryllium. Introduction-- Background-- Wipe Sampling - Dry, Wet, Alcohol-- Bulk Sampling - Sweep, Vacuum, HEPA Sock-- Methods-- Sampling Safety-- Planning Meetings - Before and During Sampling Campaigns-- Communication-- Personal Factors-- Personal Protection Equipment (PPE)-- Protecting the Sampler-- | ||
500 | |a - Protecting the Sample-- Sample Planning - Avoiding Surprises and Delays-- Getting Organized - The Plan - Large or Small-- Sampling Campaign Type, Scope and Strategy-- Detailed Sampling Plan and Agreement to Follow-- Sampling Safety Plan Included-- Include Site History in Plan-- Possible Interferences Identified-- Time Line & Locations of Beryllium Work-- Time Line & Locations of Interferences Work-- Beryllium in Naturally Occurring Materials-- Recordkeeping-- Chain-Of-Custody-- Oversight - Method - Assignments - Reports - Forms-- Locations of Sample Points and Number of Samples - How Determined-- Random Selection Sample Points-- Biased Sample Points-- Sampling Techniques and Requirements Detailed-- Photography Requirements and Permits-- Analysis of Samples - Pre-Qualifying and Selection of the Laboratory-- Quality Control Measures-- Data Reduction Format-- Final Report Parameters-- Cost Considerations - What is Desired vs. What is Needed-- Sampling Supplies-- Consumables-- | ||
500 | |a - Hand Tools-- Power Equipment, Cords and Work Carts-- Sampling Team Needs - Lunches and Other Logistics-- Trash and Waste Collection and Disposal-- Surface Sampling - When To Do What and Why-- Regulatory Requirements for Sampling-- Sampling Methods-- Surface Clean, Dusty or Dirty-- Wipe vs. Bulk-- Dry Wipe vs. Wet Wipe vs. Alcohol Wipe-- Bulk Sampling-- Determining Surface Area-- Recordkeeping and Photography-- Protection of Sample Process and Samples from Contamination-- Obtaining the Sample-- Sampling for Release of Items from Radiologically Contaminated Areas-- Summary. Chapter 4: Sample Dissolution Reagents for Beryllium. Introduction: Background-- Methods of Sample Preparation in Geological Media-- Beryllium Ores-- Soils and Silicates-- Methods of Sample Preparation for Occupational Hygiene Samples-- Workplace Air Samples-- Surface Samples-- Bulk Samples-- Summary. Chapter 5: Heating Sources for Beryllium Sample Preparation. Introduction-- Purpose of Heating-- | ||
500 | |a - Kinetics of Dissolution-- Issues with Particulates-- Issues with Speciation-- Methods-- Mechanical Agitation-- Limitations/Requirements-- Advantages-- Examples (Soils)-- Thermal Heating-- Limitations/Requirements-- Advantages-- Examples (Ashing, Hot Acid, Hot Ammoniumbifluoride)-- Sonication-- Limitations/Requirements-- Advantages-- Examples-- Microwave-- Limitations/Requirements-- Advantages-- Examples (Combine with Acid for ICP)-- Selected Comparisons-- Filters-- Comparison of Heating Methods on Recovery for Ammonium Bifluoride Dissolution-- Soils-- Summary. Chapter 6: Inductively Coupled Plasma Atomic Emission Spectrometry And Inductively Coupled Plasma Mass Spectrometry. Introduction-- Background-- Concept of ICP analysis and AES and MS detection-- Methods - Preparation of Samples-- Methods Available-- Analytical Considerations for Selecting a Sample Preparation Method-- Challenges with Beryllium Samples for Analysis by ICP-AES or ICP-MS-- Quality Control/Quality Assurance-- | ||
500 | |a - Methods - Analysis by ICP-AES-- Instrumentation (tentative)-- Selection of Line (Intensity, Detection Limit)-- Interferences (Background, Spectral, Suppression)-- Need to Know Other Constituents-- How to Correct (Different Wavelength, Correction Factor)-- Sensitivity-- Matrix Effects-- Analytical Methods-- Considerations when Working with Beryllium-- Methods - Analysis by ICP/MS-- Instrumentation-- The Mass Spectrum-- Interferences-- Sensitivity-- Matrix Effects-- Analytical Methods-- Considerations when Working with Beryllium-- Tables/Charts: Summary of Prep Methods-- Spectrum with Example of Potential Interferences. Summary. Chapter 7: Analysis by Non-Plasma Sources. Introduction-- Background-- Methods-- Atomic Absorption-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- UV-Visible-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- Fluorescence-- Methodology-- Detection Limits-- Interferences and Limitations-- | ||
500 | |a - Applications-- Electrochemistry-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- Laser Induced Breakdown Spectroscopy (LIBS)-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- Summary. Chapter 8: Data Reporting & Communications. Introduction-- Background-- Terminology-- Data Censoring-- Challenges in Evaluating Censored Data-- Other Fundamental Concepts-- Methods-- Evaluation Based on Individual Data Points-- Laboratory Reporting Limits-- Basis, Pros and Cons-- Evaluation Based on Data Sets-- Data/Measurement Quality Objectives-- Basis, Pros and Cons-- Uncensored Data-- What It Is-- When It May Be Useful-- When Not to Use It-- Considerations for Laboratories and Clients-- Project Planning-- Laboratory Integration in Project Design Decisions-- Quality Control-- Quality Assurance-- Beryllium Data Reporting-- Preparation (Before Analysis)-- Instrumentation-- Qualities of Reported Data-- | ||
500 | |a - Quantitation as a Substitute for Uncertainty Reporting-- Communicating Results-- Laboratory to Client-- Data Evaluation-- Communication to Managers and Stakeholders-- Summary. Chapter 9: Applications, Future Trends, and Opportunities. Applications of Current Technologies-- Uses of Analytical Measurements-- Diagnostic Sampling-- Exposure Assessment-- Exposure Surveillance-- Data Evaluation-- Data Quality Objectives-- Data Sets Versus Data Points-- Precision/Bias Versus Uncertainty Budgets-- Future Trends and Opportunities-- Drivers for Change-- Occupational Exposure Limits-- Real-Time Monitoring-- Size-Selective Sampling-- Technology Improvements-- Sampling-- Analysis-- Data Evaluation-- Exposure-- Assessment Strategies-- Summary | ||
500 | |a This comprehensive book describes all aspects of the current sampling and analysis techniques for trace-level beryllium in the workplace | ||
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[et al.], editors</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Cambridge</subfield><subfield code="b">Royal Society of Chemistry</subfield><subfield code="c">c2009</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">1 Online-Ressource</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">c</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">cr</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a">Introduction: Purpose or Background-- Methods-- Summary. Chapter 1: Overview of Beryllium Sampling and Analysis. 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Chapter 3: Successful Surface Sampling for Beryllium. Introduction-- Background-- Wipe Sampling - Dry, Wet, Alcohol-- Bulk Sampling - Sweep, Vacuum, HEPA Sock-- Methods-- Sampling Safety-- Planning Meetings - Before and During Sampling Campaigns-- Communication-- Personal Factors-- Personal Protection Equipment (PPE)-- Protecting the Sampler-- </subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a"> - Protecting the Sample-- Sample Planning - Avoiding Surprises and Delays-- Getting Organized - The Plan - Large or Small-- Sampling Campaign Type, Scope and Strategy-- Detailed Sampling Plan and Agreement to Follow-- Sampling Safety Plan Included-- Include Site History in Plan-- Possible Interferences Identified-- Time Line & Locations of Beryllium Work-- Time Line & Locations of Interferences Work-- Beryllium in Naturally Occurring Materials-- Recordkeeping-- Chain-Of-Custody-- Oversight - Method - Assignments - Reports - Forms-- Locations of Sample Points and Number of Samples - How Determined-- Random Selection Sample Points-- Biased Sample Points-- Sampling Techniques and Requirements Detailed-- Photography Requirements and Permits-- Analysis of Samples - Pre-Qualifying and Selection of the Laboratory-- Quality Control Measures-- Data Reduction Format-- Final Report Parameters-- Cost Considerations - What is Desired vs. What is Needed-- Sampling Supplies-- Consumables-- </subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a"> - Hand Tools-- Power Equipment, Cords and Work Carts-- Sampling Team Needs - Lunches and Other Logistics-- Trash and Waste Collection and Disposal-- Surface Sampling - When To Do What and Why-- Regulatory Requirements for Sampling-- Sampling Methods-- Surface Clean, Dusty or Dirty-- Wipe vs. Bulk-- Dry Wipe vs. Wet Wipe vs. Alcohol Wipe-- Bulk Sampling-- Determining Surface Area-- Recordkeeping and Photography-- Protection of Sample Process and Samples from Contamination-- Obtaining the Sample-- Sampling for Release of Items from Radiologically Contaminated Areas-- Summary. Chapter 4: Sample Dissolution Reagents for Beryllium. Introduction: Background-- Methods of Sample Preparation in Geological Media-- Beryllium Ores-- Soils and Silicates-- Methods of Sample Preparation for Occupational Hygiene Samples-- Workplace Air Samples-- Surface Samples-- Bulk Samples-- Summary. Chapter 5: Heating Sources for Beryllium Sample Preparation. 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Introduction-- Background-- Terminology-- Data Censoring-- Challenges in Evaluating Censored Data-- Other Fundamental Concepts-- Methods-- Evaluation Based on Individual Data Points-- Laboratory Reporting Limits-- Basis, Pros and Cons-- Evaluation Based on Data Sets-- Data/Measurement Quality Objectives-- Basis, Pros and Cons-- Uncensored Data-- What It Is-- When It May Be Useful-- When Not to Use It-- Considerations for Laboratories and Clients-- Project Planning-- Laboratory Integration in Project Design Decisions-- Quality Control-- Quality Assurance-- Beryllium Data Reporting-- Preparation (Before Analysis)-- Instrumentation-- Qualities of Reported Data-- </subfield></datafield><datafield tag="500" ind1=" " ind2=" "><subfield code="a"> - Quantitation as a Substitute for Uncertainty Reporting-- Communicating Results-- Laboratory to Client-- Data Evaluation-- Communication to Managers and Stakeholders-- Summary. Chapter 9: Applications, Future Trends, and Opportunities. 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genre | 1\p (DE-588)4143413-4 Aufsatzsammlung gnd-content |
genre_facet | Aufsatzsammlung |
id | DE-604.BV043096967 |
illustrated | Not Illustrated |
indexdate | 2024-07-10T07:17:19Z |
institution | BVB |
isbn | 1847559670 9781847559678 |
language | English |
oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-028521159 |
oclc_num | 429670528 |
open_access_boolean | |
owner | DE-1046 DE-1047 |
owner_facet | DE-1046 DE-1047 |
physical | 1 Online-Ressource |
psigel | ZDB-4-EBA ZDB-4-EBA FAW_PDA_EBA |
publishDate | 2009 |
publishDateSearch | 2009 |
publishDateSort | 2009 |
publisher | Royal Society of Chemistry |
record_format | marc |
spelling | Beryllium environmental analysis and monitoring Mike Brisson... [et al.], editors Cambridge Royal Society of Chemistry c2009 1 Online-Ressource txt rdacontent c rdamedia cr rdacarrier Introduction: Purpose or Background-- Methods-- Summary. Chapter 1: Overview of Beryllium Sampling and Analysis. Introduction-- Background-- Beryllium Sources-- Industrial Uses-- Health Risks-- Natural Versus Anthropogenic-- Carcinogenicity-- Acute Beryllium Disease-- Chronic Beryllium Disease-- Occupational Exposure Limits-- History-- Current Limits-- Trends-- Impact of U.S. Department of Energy Beryllium Rule-- Environmental Remediation-- Sampling Overview-- Air Sampling-- Surface Sampling-- Dermal Sampling-- Soil Sampling-- Analysis Overview: Summary of Current Techniques-- Need for Improved Performance-- Need for Real-Time Monitoring-- Goals of This Book (Summary). Chapter 2: Air Sampling. Introduction-- Purpose of Air Sampling and Choice of Strategy-- Sampling for Compliance with a Limit Value-- Sampling to Determine the Effectiveness of Control Measures-- Sampling to Identify a Group Range of Exposures-- Identification of a Homogenous Exposure Group (HEG)-- - Determining the Range of Exposures of a HEG-- Sampling for Prospective Health Studies-- Methods of Air Sampling-- Properties and Behaviors of Aerosols-- Sources of Beryllium Aerosols-- Sampling for Non-volatile Aerosols Using Filters-- Size-selective Sampling-- Inhalable Sampling-- Respirable Sampling-- High-volume Sampling-- Sampling for Volatile Aerosols-- Sampling for Ultrafine Aerosols-- Metrics for Ultrafine Particles-- Analytical Considerations for Selecting a Sampling Method-- Retrospective Exposure Assessments-- Determining a Job-exposure Matrix (JEM)-- Cumulative vs Peak Exposures in Assessing Exposure Histories-- Summary. Chapter 3: Successful Surface Sampling for Beryllium. Introduction-- Background-- Wipe Sampling - Dry, Wet, Alcohol-- Bulk Sampling - Sweep, Vacuum, HEPA Sock-- Methods-- Sampling Safety-- Planning Meetings - Before and During Sampling Campaigns-- Communication-- Personal Factors-- Personal Protection Equipment (PPE)-- Protecting the Sampler-- - Protecting the Sample-- Sample Planning - Avoiding Surprises and Delays-- Getting Organized - The Plan - Large or Small-- Sampling Campaign Type, Scope and Strategy-- Detailed Sampling Plan and Agreement to Follow-- Sampling Safety Plan Included-- Include Site History in Plan-- Possible Interferences Identified-- Time Line & Locations of Beryllium Work-- Time Line & Locations of Interferences Work-- Beryllium in Naturally Occurring Materials-- Recordkeeping-- Chain-Of-Custody-- Oversight - Method - Assignments - Reports - Forms-- Locations of Sample Points and Number of Samples - How Determined-- Random Selection Sample Points-- Biased Sample Points-- Sampling Techniques and Requirements Detailed-- Photography Requirements and Permits-- Analysis of Samples - Pre-Qualifying and Selection of the Laboratory-- Quality Control Measures-- Data Reduction Format-- Final Report Parameters-- Cost Considerations - What is Desired vs. What is Needed-- Sampling Supplies-- Consumables-- - Hand Tools-- Power Equipment, Cords and Work Carts-- Sampling Team Needs - Lunches and Other Logistics-- Trash and Waste Collection and Disposal-- Surface Sampling - When To Do What and Why-- Regulatory Requirements for Sampling-- Sampling Methods-- Surface Clean, Dusty or Dirty-- Wipe vs. Bulk-- Dry Wipe vs. Wet Wipe vs. Alcohol Wipe-- Bulk Sampling-- Determining Surface Area-- Recordkeeping and Photography-- Protection of Sample Process and Samples from Contamination-- Obtaining the Sample-- Sampling for Release of Items from Radiologically Contaminated Areas-- Summary. Chapter 4: Sample Dissolution Reagents for Beryllium. Introduction: Background-- Methods of Sample Preparation in Geological Media-- Beryllium Ores-- Soils and Silicates-- Methods of Sample Preparation for Occupational Hygiene Samples-- Workplace Air Samples-- Surface Samples-- Bulk Samples-- Summary. Chapter 5: Heating Sources for Beryllium Sample Preparation. Introduction-- Purpose of Heating-- - Kinetics of Dissolution-- Issues with Particulates-- Issues with Speciation-- Methods-- Mechanical Agitation-- Limitations/Requirements-- Advantages-- Examples (Soils)-- Thermal Heating-- Limitations/Requirements-- Advantages-- Examples (Ashing, Hot Acid, Hot Ammoniumbifluoride)-- Sonication-- Limitations/Requirements-- Advantages-- Examples-- Microwave-- Limitations/Requirements-- Advantages-- Examples (Combine with Acid for ICP)-- Selected Comparisons-- Filters-- Comparison of Heating Methods on Recovery for Ammonium Bifluoride Dissolution-- Soils-- Summary. Chapter 6: Inductively Coupled Plasma Atomic Emission Spectrometry And Inductively Coupled Plasma Mass Spectrometry. Introduction-- Background-- Concept of ICP analysis and AES and MS detection-- Methods - Preparation of Samples-- Methods Available-- Analytical Considerations for Selecting a Sample Preparation Method-- Challenges with Beryllium Samples for Analysis by ICP-AES or ICP-MS-- Quality Control/Quality Assurance-- - Methods - Analysis by ICP-AES-- Instrumentation (tentative)-- Selection of Line (Intensity, Detection Limit)-- Interferences (Background, Spectral, Suppression)-- Need to Know Other Constituents-- How to Correct (Different Wavelength, Correction Factor)-- Sensitivity-- Matrix Effects-- Analytical Methods-- Considerations when Working with Beryllium-- Methods - Analysis by ICP/MS-- Instrumentation-- The Mass Spectrum-- Interferences-- Sensitivity-- Matrix Effects-- Analytical Methods-- Considerations when Working with Beryllium-- Tables/Charts: Summary of Prep Methods-- Spectrum with Example of Potential Interferences. Summary. Chapter 7: Analysis by Non-Plasma Sources. Introduction-- Background-- Methods-- Atomic Absorption-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- UV-Visible-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- Fluorescence-- Methodology-- Detection Limits-- Interferences and Limitations-- - Applications-- Electrochemistry-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- Laser Induced Breakdown Spectroscopy (LIBS)-- Methodology-- Detection Limits-- Interferences and Limitations-- Applications-- Summary. Chapter 8: Data Reporting & Communications. Introduction-- Background-- Terminology-- Data Censoring-- Challenges in Evaluating Censored Data-- Other Fundamental Concepts-- Methods-- Evaluation Based on Individual Data Points-- Laboratory Reporting Limits-- Basis, Pros and Cons-- Evaluation Based on Data Sets-- Data/Measurement Quality Objectives-- Basis, Pros and Cons-- Uncensored Data-- What It Is-- When It May Be Useful-- When Not to Use It-- Considerations for Laboratories and Clients-- Project Planning-- Laboratory Integration in Project Design Decisions-- Quality Control-- Quality Assurance-- Beryllium Data Reporting-- Preparation (Before Analysis)-- Instrumentation-- Qualities of Reported Data-- - Quantitation as a Substitute for Uncertainty Reporting-- Communicating Results-- Laboratory to Client-- Data Evaluation-- Communication to Managers and Stakeholders-- Summary. Chapter 9: Applications, Future Trends, and Opportunities. Applications of Current Technologies-- Uses of Analytical Measurements-- Diagnostic Sampling-- Exposure Assessment-- Exposure Surveillance-- Data Evaluation-- Data Quality Objectives-- Data Sets Versus Data Points-- Precision/Bias Versus Uncertainty Budgets-- Future Trends and Opportunities-- Drivers for Change-- Occupational Exposure Limits-- Real-Time Monitoring-- Size-Selective Sampling-- Technology Improvements-- Sampling-- Analysis-- Data Evaluation-- Exposure-- Assessment Strategies-- Summary This comprehensive book describes all aspects of the current sampling and analysis techniques for trace-level beryllium in the workplace SCIENCE / Chemistry / Inorganic bisacsh Chemie Beryllium Sampling Beryllium Analysis Umweltprobe (DE-588)4222155-9 gnd rswk-swf Probenahme (DE-588)4047319-3 gnd rswk-swf Beryllium (DE-588)4144824-8 gnd rswk-swf Chemische Analyse (DE-588)4009840-0 gnd rswk-swf 1\p (DE-588)4143413-4 Aufsatzsammlung gnd-content Beryllium (DE-588)4144824-8 s Umweltprobe (DE-588)4222155-9 s Chemische Analyse (DE-588)4009840-0 s 2\p DE-604 Probenahme (DE-588)4047319-3 s 3\p DE-604 Brisson, Mike Sonstige oth http://search.ebscohost.com/login.aspx?direct=true&scope=site&db=nlebk&db=nlabk&AN=519278 Aggregator Volltext 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
spellingShingle | Beryllium environmental analysis and monitoring SCIENCE / Chemistry / Inorganic bisacsh Chemie Beryllium Sampling Beryllium Analysis Umweltprobe (DE-588)4222155-9 gnd Probenahme (DE-588)4047319-3 gnd Beryllium (DE-588)4144824-8 gnd Chemische Analyse (DE-588)4009840-0 gnd |
subject_GND | (DE-588)4222155-9 (DE-588)4047319-3 (DE-588)4144824-8 (DE-588)4009840-0 (DE-588)4143413-4 |
title | Beryllium environmental analysis and monitoring |
title_auth | Beryllium environmental analysis and monitoring |
title_exact_search | Beryllium environmental analysis and monitoring |
title_full | Beryllium environmental analysis and monitoring Mike Brisson... [et al.], editors |
title_fullStr | Beryllium environmental analysis and monitoring Mike Brisson... [et al.], editors |
title_full_unstemmed | Beryllium environmental analysis and monitoring Mike Brisson... [et al.], editors |
title_short | Beryllium |
title_sort | beryllium environmental analysis and monitoring |
title_sub | environmental analysis and monitoring |
topic | SCIENCE / Chemistry / Inorganic bisacsh Chemie Beryllium Sampling Beryllium Analysis Umweltprobe (DE-588)4222155-9 gnd Probenahme (DE-588)4047319-3 gnd Beryllium (DE-588)4144824-8 gnd Chemische Analyse (DE-588)4009840-0 gnd |
topic_facet | SCIENCE / Chemistry / Inorganic Chemie Beryllium Sampling Beryllium Analysis Umweltprobe Probenahme Beryllium Chemische Analyse Aufsatzsammlung |
url | http://search.ebscohost.com/login.aspx?direct=true&scope=site&db=nlebk&db=nlabk&AN=519278 |
work_keys_str_mv | AT brissonmike berylliumenvironmentalanalysisandmonitoring |