The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Hamburg
TuTech Innovation
2015
|
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | 186 S. Ill., graph. Darst. |
| ISBN: | 9783941492929 |
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TABLE OF CONTENTS:
ACKNOWLEDGEMENTS
SHORT SUMMARY
KURZZUSAMMENFASSUNG
1. INTRODUCTION
1.1. MOTIVATION
1.1.1. REFERENCES
1.2. OBJECTIVES AND STRUCTURE
2. STATE-OF-THE-ART OF THE SCIENCE AND TECHNOLOGY
2.1. MANUFACTURING TECHNOLOGIES FOR FIBER-REINFORCED COMPOSITES
2.1.1. PREPREG METHODS
2.1.2. FILAMENT WINDING
2.1.3. PULTRUSION
2.1.4. INJECTION PROCESSES VIA A MOLD
2.1.5. INFUSION PROCESSES VIA A VACUUM BAG
2.1.6. REFERENCES
2.2. FIBER REINFORCEMENTS FOR EPOXY RESIN SYSTEMS
2.2.1. WOVEN FABRICS
2.2.2. UNIDIRECTIONAL FABRICS
2.2.3. MULTIAXIAL FABRICS
2.2.4. PREFORMS
2.2.5. FIBER SIZING
2.2.6. REFERENCES
HTTP://D-NB.INFO/1072579928
2.3. EPOXY RESIN SYSTEMS FOR FIBER-REINFORCED COMPOSITES 24
2.3.1. EPOXY RESINS 24
2.3.2. CURING AGENTS FOR EPOXY RESINS 26
2.3.2.1. AMINE CURING AGENTS 26
2.3.2.2. ANHYDRIDE CURING AGENTS 26
2.3.3. EPOXY RESIN SYSTEMS 28
2.3.4 REFERENCES 29
2.4. TOUGHENING OF EPOXY RESINS 30
2.4.1. DIFFERENTIATION BETWEEN TOUGHENING AND INCREASING
FLEXIBILITY 30
2.4.2. REACTIVE LIQUID RUBBERS 30
2.4.3. CORE-SHELL RUBBER PARTICLES 32
2.4.4. THERMOPLASTIC PARTICLES 33
2.4.5. SELF-ORGANIZING BLOCK COPOLYMERS 34
2.4.6. REFERENCES 35
2.5. MODIFICATION OF EPOXY RESINS WITH SI0
2
NANOPARTICLES 37
2.5.1. SI0
2
NANOPARTICLES 37
2.5.2. PROPERTY IMPROVEMENTS OF CURED BULK RESIN
SYSTEMS 40
2.5.3. PROPERTY IMPROVEMENTS OF CURED BULK
HYBRID RESIN SYSTEMS 41
2.5.4. PROPERTY IMPROVEMENTS OF FIBER-REINFORCED
COMPOSITES 43
2.5.5. REFERENCES 47
3. MATERIALS, SAMPLE PREPARATION AND CHARACTERIZATION 50
3.1. EPOXY RESIN SYSTEM 50
2
3.2. CARBON FIBER REINFORCEMENT 50
3.3. SAMPLE PREPARATION AND CHARACTERIZATION 50
4. RESULTS AND DISCUSSION 51
4.1. PROPERTY IMPROVEMENTS OFEPOXY RESINS MODIFIED WITH SI0
2
NANOPARTICLES 51
PREPUBLISHED AS
"EPOXY RESIN COMPOSITES WITH SURFACE-MODIFIED SILICON DIOXIDE
NANOPARTICLES: A REVIEW"
IN JOURNAL OF APPLIED POLYMER SCIENCE 130, PAGES 1421-1428, 2013
4.1.1. ABSTRACT 51
4.1.2. INTRODUCTION 51
4.1.3. DISCUSSION 54
4.1.3.1. AMINE-CURED EPOXY RESINS 54
4.1.3.2. ANHYDRIDE-CURED EPOXY RESINS 59
4.1.3.3. COMPARISON BETWEEN DIFFERENT TYPES OF HARDENERS 63
4.1.4. CONCLUSIONS 65
4.1.5. REFERENCES 66
4.2. PROPERTY IMPROVEMENTS OFEPOXY RESINS MODIFIED WITH SI0
2
NANOPARTICLES AND ELASTOMERS (HYBRID SYSTEMS) 69
PREPUBLISHED AS
"EPOXY RESINS MODIFIED WITH ELASTOMERS AND SURFACE-MODIFIED
SILICA NANOPARTICLES: FEATURE ARTICLE"
IN POLYMER 54, PAGES 4790-4797, 2013
4.2.1. ABSTRACT 69
4.2.2. INTRODUCTION 69
4.2.3. DISCUSSION 72
3
4.2.3.1. EPOXY RESINS MODIFIED WITH REACTIVE LIQUID RUBBERS
(CTBNS) AND SILICA NANOPARTICLES, AMINE CURED 72
4.2.3.2. EPOXY RESINS MODIFIED WITH STYRENE-BUTADIENE RUBBER
(SBR) AND SILICA NANOPARTICLES, AMINE CURED 75
4.2.3.3. EPOXY RESINS MODIFIED WITH REACTIVE LIQUID RUBBERS
(CTBNS) AND SILICA NANOPARTICLES, ANHYDRIDE CURED 75
4.2.3.4. EPOXY RESINS MODIFIED WITH SILICA NANOPARTICLES, CURED
WITH AMINES AND AMINO-FUNCTIONAL REACTIVE LIQUID
RUBBERS (ATBNS) 77
4.2.3.5. EPOXY RESINS MODIFIED WITH CORE-SHELL ELASTOMERS
(CSRS) AND SILICA NANOPARTICLES, AMINE CURED 78
4.2.3.6. EPOXY RESINS MODIFIED WITH CORE-SHELL ELASTOMERS
(CSRS) AND SILICA NANOPARTICLES, ANHYDRIDE CURED 81
4.2.3.7. SHORT OVERVIEW OF IMPROVEMENTS ACHIEVED 82
4.2.3.8. SYNERGY OR NO SYNERGY? 83
4.2.4. CONCLUSIONS 85
4.2.5. REFERENCES 86
4.3. PROPERTY IMPROVEMENTS OF FIBER-REINFORCED COMPOSITES BASED ON
EPOXY RESINS MODIFIED WITH SI0
2
NANOPARTICLES 89
PREPUBLISHED AS
IMPROVING MECHANICAL PROPERTIES OF FIBER-REINFORCED COMPOSITES
BASED ON EPOXY RESINS CONTAINING INDUSTRIAL SURFACE-MODIFIED SILICA
NANOPARTICLES: REVIEW AND OUTLOOK"
IN JOURNAL OF COMPOSITE MATERIALS 49, PAGES 53-63, 2015
4.3.1. ABSTRACT 89
4.3.2. INTRODUCTION 89
4.3.3. DISCUSSION 93
4.3.3.1. GLASS FIBER-REINFORCED EPOXY RESIN COMPOSITES 93
4.3.3.2. CARBON FIBER-REINFORCED EPOXY RESIN COMPOSITES 97
4.3.3.3. COMPARISION BETWEEN BULK AND LAMINATE PROPERTY
IMPROVEMENTS 101
4.3.3.4. MECHANISMS OF TOUGHENING 102
4.3.3.5. HOW MUCH SILICA NANOPARTIDES DO YOU REALLY
NEED - AND WHERE? 103
4.3.4. CONCLUSIONS 104
4.3.5. REFERENCES 105
4.4. PROPERTY IMPROVEMENTS OF FIBER-REINFORCED COMPOSITES BASED ON
EPOXY RESINS MODIFIED WITH S/0
2
NANOPARTIDES AND ELASTOMERS
(HYBRID SYSTEMS) 109
PREPUBLISHED AS
"REVIEW: FIBER-REINFORCED COMPOSITES BASED ON EPOXY RESINS
MODIFIED WITH ELASTOMERS AND SURFACE-MODIFIED SILICA
NANOPARTIDES"'
IN JOURNAL OF MATERIALS SCIENCE 49, PAGES 2391-2402, 2014
4.4.1. ABSTRACT 109
4.4.2. INTRODUCTION 109
4.4.3. DISCUSSION 113
4.4.3.1. GLASS FIBER-REINFORCED EPOXY RESIN COMPOSITES 114
4.4.3.2. CARBON FIBER-REINFORCED EPOXY RESIN COMPOSITES 118
4.4.3.3. MECHANISMS FOR PROPERTY IMPROVEMENTS OF HYBRID
EPOXY RESIN SYSTEMS 121
4.4.3.4. THE TRANSFER OF IMPROVED BULK RESIN PROPERTIES INTO
THE FIBER-REINFORCED COMPOSITE 122
4.4.4. CONCLUSIONS 126
4.4.5. REFERENCES 126
4.5. FIBER-REINFORCED COMPOSITES WITH EPOXY RESIN MODIFIED WITH
REACTIVE LIQUID RUBBER AND SI0
2
NANOPARTIDES 131
PREPUBLISHED AS
5
"CARBON FIBER-REINFORCED COMPOSITES USING AN EPOXY RESIN MATRIX MODIFIED
WITH REACTIVE LIQUID RUBBER AND SILICA NANOPARTICLES"
IN COMPOSITES SCIENCE AND TECHNOLOGY 105, PAGES 86-95, 2014
4.5.1. ABSTRACT
131
4.5.2. INTRODUCTION
131
4.5.3. EXPERIMENTAL
135
4.5.3.1. MATERIALS
135
4.5.3.2.
BULK SAMPLE PREPARATION
136
4.5.3.3.
LAMINATE PREPARATION
136
4.5.3.4. BULK SAMPLE TESTING
136
4.5.3.5. LAMINATE TESTING
137
4.5.4. RESULTS AND DISCUSSION
138
4.5.4.1. BULK RESIN PROPERTIES
138
4.5.4.2. LAMINATE PROPERTIES
142
4.5.4.3. MICROSCOPICAL INVESTIGATIONS
149
4.5.4.4. FORMATION OF NANOSILICA AGGLOMERATES
152
4.5.5. CONCLUSIONS AND OUTLOOK 156
4.5.6. REFERENCES
157
5. SUMMARY AND OUTLOOK 160
5.1. SUMMARY AND OUTLOOK 160
5.2. ZUSAMMENFASSUNG UND AUSBLICK 162
6. BIBLIOGRAPHY 166
APPENDIX 1: PUBLICATIONS 181
APPENDIX 2: CV 185
6 |
| any_adam_object | 1 |
| author | Sprenger, Stephan |
| author_facet | Sprenger, Stephan |
| author_role | aut |
| author_sort | Sprenger, Stephan |
| author_variant | s s ss |
| building | Verbundindex |
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| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 540 - Chemistry and allied sciences |
| dewey-raw | 540 |
| dewey-search | 540 |
| dewey-sort | 3540 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik |
| format | Thesis Book |
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| spelling | Sprenger, Stephan Verfasser aut The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof Stephan Sprenger Hamburg TuTech Innovation 2015 186 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Zugl.: Bayreuth, Univ., Diss., 2015 Nanopartikel (DE-588)4333369-2 gnd rswk-swf Härten (DE-588)4139793-9 gnd rswk-swf Siliciumdioxid (DE-588)4077447-8 gnd rswk-swf Epoxidharz (DE-588)4070891-3 gnd rswk-swf Bruchzähigkeit (DE-588)4008393-7 gnd rswk-swf Faserverstärkter Kunststoff (DE-588)4128805-1 gnd rswk-swf Faserverbundwerkstoffe Epoxidharze SiO2-Nanopartikel Übertragungsfaktor Ermüdungsverhalten Bruchzähigkeit (DE-588)4113937-9 Hochschulschrift gnd-content Epoxidharz (DE-588)4070891-3 s Siliciumdioxid (DE-588)4077447-8 s Nanopartikel (DE-588)4333369-2 s Härten (DE-588)4139793-9 s DE-604 Faserverstärkter Kunststoff (DE-588)4128805-1 s Bruchzähigkeit (DE-588)4008393-7 s X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=5296304&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028151444&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Sprenger, Stephan The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof Nanopartikel (DE-588)4333369-2 gnd Härten (DE-588)4139793-9 gnd Siliciumdioxid (DE-588)4077447-8 gnd Epoxidharz (DE-588)4070891-3 gnd Bruchzähigkeit (DE-588)4008393-7 gnd Faserverstärkter Kunststoff (DE-588)4128805-1 gnd |
| subject_GND | (DE-588)4333369-2 (DE-588)4139793-9 (DE-588)4077447-8 (DE-588)4070891-3 (DE-588)4008393-7 (DE-588)4128805-1 (DE-588)4113937-9 |
| title | The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof |
| title_auth | The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof |
| title_exact_search | The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof |
| title_full | The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof Stephan Sprenger |
| title_fullStr | The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof Stephan Sprenger |
| title_full_unstemmed | The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof Stephan Sprenger |
| title_short | The effects of SiO2 nanoparticles in toughened epoxy resins and fiber-reinforced composites made thereof |
| title_sort | the effects of sio2 nanoparticles in toughened epoxy resins and fiber reinforced composites made thereof |
| topic | Nanopartikel (DE-588)4333369-2 gnd Härten (DE-588)4139793-9 gnd Siliciumdioxid (DE-588)4077447-8 gnd Epoxidharz (DE-588)4070891-3 gnd Bruchzähigkeit (DE-588)4008393-7 gnd Faserverstärkter Kunststoff (DE-588)4128805-1 gnd |
| topic_facet | Nanopartikel Härten Siliciumdioxid Epoxidharz Bruchzähigkeit Faserverstärkter Kunststoff Hochschulschrift |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=5296304&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028151444&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT sprengerstephan theeffectsofsio2nanoparticlesintoughenedepoxyresinsandfiberreinforcedcompositesmadethereof |