Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Aachen
Shaker
2015
|
| Schriftenreihe: | Schriftenreihe des IME
36 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Zsfassung in dt. und engl. Sprache |
| Beschreibung: | XXXII, 107 S. , S. XXIV-XXXVII Ill., graph. Darst. |
| ISBN: | 9783844032949 |
Internformat
MARC
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| 245 | 1 | 0 | |a Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries |c Honggang Wang |
| 264 | 1 | |a Aachen |b Shaker |c 2015 | |
| 300 | |a XXXII, 107 S. , S. XXIV-XXXVII |b Ill., graph. Darst. | ||
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| 500 | |a Zsfassung in dt. und engl. Sprache | ||
| 502 | |a Zugl.: Aachen, Techn. Hochsch., Diss., 2014 | ||
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| 653 | |a Automotive Li-ion batteries | ||
| 653 | |a Cobalt | ||
| 653 | |a Nickel | ||
| 653 | |a Lithium | ||
| 653 | |a Hydrometallurgy | ||
| 653 | |a Recycling | ||
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Datensatz im Suchindex
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| adam_text | TABLE OF CONTENTS
TABLE OF CONTENTS
TABLE OF CONTENTS I
LIST OF FIGURES ILL
LIST OF TABLES VIII
ABBREVIATIONS X
ABSTRACT XI
KURZFASSUNG XII
EXTENDED ABSTRACT XIII
1 INTRODUCTION -1-
2 STATE OF TECHNOLOGY - 2 -
21 FUNDAMENTAL OF AUTOMOTIVE U ION BATTERIES - 2 -
2 11 INTRODUCTION OF AUTOMOTIVE LI-ION BATTERIES. . - 2 -
21.2 CONSTRUCTION OF LITHIUM-ION BATTERIES IN SINGLE CELL AND MODULE - 5
-
2 13 VALUE OF SPENT AUTOMOTIVE LI-ION BATTERIES -11-
2 2 RECYCLING CONCEPTS OF AUTOMOTIVE LI-ION BATTERIES. -13 -
2 2.1 DIRECTIVES REGARDING TO THE LI-ION BATTERIES RECYCLING IN EUROPE
-13 -
2 2 2 REVIEW OF LI-ION BATTERIES RECYCLING METHODS AT INDUSTRIAL SCALE
-15 -
2 2.3 HYDROMETALLURGICAL LI-ION BATTERIES RECYCLING METHODS TESTED ONLY
AT LAB SCALE. - 23 -
2 3 LEACHING -26-
2 3.1 GENERAL REMARKS -26-
2 3.2 KINETIC MODELLING - 26 -
2.3.3 THERMOCHEMICAL MODELLING ... - 28 -
2 4 CU CEMENTATION .... -30-
2 5 METAL PRECIPITATION FROM LEACHING SOLUTION -32-
2.5.1 METAL HYDROXIDE PRECIPITATION . . . - 32 -
2 5 2 METAL SULPHIDE PRECIPITATION - 34 -
2 5.3 FUNDAMENTALS OF FE PRECIPITATION - 37 -
2.6 SOLVENT EXTRACTION -39-
2 61 MECHANISM AND PROCEDURE OF SOLVENT EXTRACTION - 40 -
262 SOLVENT
EXTRACTION
EQUILIBRIUM -41-
2 6 3 EXTRACTANTS IN THE SOLVENT EXTRACTION PROCESS - 42 -
2 7 LITHIUM MARKET PRIMARY RESOURCES, APPLICATIONS AND PRODUCTION -44-
2 8 COMPARISON OF PYRO- AND HYDROMETALLURGICAL PROCESS - 46 -
2 9 GENERAL ASSESSMENT AND MOTIVATION OF THIS WORK -48-
3 EXPERIMENTAL METHODOLOGY -49-
31 PRE-TREATMENT OF SPENT AUTOMOTIVE LI-ION BATTERIES -49-
3 2 CHARACTERISATION OF THE ELECTRODE POWDER. . . - 50 -
I
HTTP://D-NB.INFO/1063731178
TABLE OF CONTENTS
3 3 DESIGN OF METALLURGICAL RECYCLING PROCESS .-52-
3 4 LEACHING EXPERIMENTS -55-
3 5 SOLUTION REFINING. .. .-57-
3 5 1 CU CEMENTATION WITH FE POWDER - 57 -
3 5 2 CU PRECIPITATION AS SULPHIDE - 58 -
3 5 3 FE AND AL PRECIPITATION BY PH ADJUSTMENT.... - 60 -
3 5 4 SOLVENT EXTRACTION - 60 -
3.6 CATHODE METAL PRECIPITATION WITH HYDROXIDE, CARBONATE AND SULPHIDE
METHODS.. -62 -
3 7 LI
2
C0
3
CRYSTALLISATION/PRECIPITATION . - 64 -
4 RESULTS AND DISCUSSION - 65 *
4.1 LEACHING REACTIONS ... - 65 -
4 11 LEACHING IN SULPHURIC ACID MEDIA ... - 66 -
4.1 2 LEACHING KINETICS - 70 -
413 VERIFICATION
EXPERIMENTS ..-78-
4.1 4 PURITY AND MORPHOLOGY OF FILTERED GRAPHITE - 79 -
4 2 SOLUTION REFINING - 80 -
4 2 1 CU RECOVERY VIA CU CEMENTATION - 80 -
4 2 2 CU RECOVERY VIA SULPHIDE PRECIPITATION . ... - 86 -
4 2.3 FE AND AL PRECIPITATION BY PH ADJUSTMENT ... . - 89 -
4 2 4 PURIFICATION OF LEACHING SOLUTION BY SOLVENT EXTRACTION - 91 -
4 3 CATHODE METAL (CO, NI, MN) PRECIPITATION - 94 -
4 3.1 CATHODE METAL HYDROXIDE PRECIPITATION , .-94-
4 3 2 CATHODE METAL CARBONATE PRECIPITATION - 96 -
433 METAL SULPHIDE
PRECIPITATION -97-
4 4 L12CO3 CRYSTALLISATION/PRECIPITATION .... -99-
4 5 EVALUATION OF RECYCLING PRODUCTS AND EFFICIENCY ... -101-
5 CONCLUSIONS -104-
6 OUTLOOK OF FUTURE WORK DIRECTIONS -106 *
7 LITERATURE XXIV
8 APPENDIX XXVIII
81 PH-TIME, EH-TIME DIAGRAMS FOR LEACHING EXPERIMENTS XXVIII
8.2 PH-TIME AND EH-TIME DIAGRAMS FOR COPPER CEMENTATION EXPERIMENTS ...
.XXIX
8 3 EH-PH DIAGRAMS FOR CO, MN, NI, CU AND AL XXXI
8 4 PH AND EH BY ADDED NAOH AND WOJCOJMOSS IN CATHODE METAL
PRECIPITATION XXXIV
8.5 XRD DIAGRAM OF RAW MATERIAL AND LIST OF IDENTIFIED PHASES. ... ...
XXXV
8 6 SEM PHOTOS OF LEACHING RESIDUAL (GRAPHITE) UNDER DIFFERENT LEACHING
CONDITIONS XXXVI
11
|
| any_adam_object | 1 |
| author | Wang, Honggang |
| author_GND | (DE-588)1065324731 |
| author_facet | Wang, Honggang |
| author_role | aut |
| author_sort | Wang, Honggang |
| author_variant | h w hw |
| building | Verbundindex |
| bvnumber | BV042599814 |
| classification_rvk | ZN 8730 |
| ctrlnum | (OCoLC)911136978 (DE-599)BVBBV042599814 |
| discipline | Elektrotechnik / Elektronik / Nachrichtentechnik |
| format | Thesis Book |
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| id | DE-604.BV042599814 |
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| indexdate | 2024-07-10T07:05:36Z |
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| isbn | 9783844032949 |
| language | English |
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| spelling | Wang, Honggang Verfasser (DE-588)1065324731 aut Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries Honggang Wang Aachen Shaker 2015 XXXII, 107 S. , S. XXIV-XXXVII Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Schriftenreihe des IME 36 Zsfassung in dt. und engl. Sprache Zugl.: Aachen, Techn. Hochsch., Diss., 2014 Kraftfahrzeugbatterie (DE-588)4165422-5 gnd rswk-swf Nassmetallurgie (DE-588)4123820-5 gnd rswk-swf Metall (DE-588)4038860-8 gnd rswk-swf Recycling (DE-588)4076573-8 gnd rswk-swf Lithiumcarbonat (DE-588)4378397-1 gnd rswk-swf Grafit (DE-588)4158067-9 gnd rswk-swf Lithium-Ionen-Akkumulator (DE-588)7681721-0 gnd rswk-swf Automotive Li-ion batteries Cobalt Nickel Lithium Hydrometallurgy Recycling (DE-588)4113937-9 Hochschulschrift gnd-content Kraftfahrzeugbatterie (DE-588)4165422-5 s Lithium-Ionen-Akkumulator (DE-588)7681721-0 s Grafit (DE-588)4158067-9 s Metall (DE-588)4038860-8 s Lithiumcarbonat (DE-588)4378397-1 s Recycling (DE-588)4076573-8 s Nassmetallurgie (DE-588)4123820-5 s DE-604 Schriftenreihe des IME 36 (DE-604)BV016981907 36 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028032902&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Wang, Honggang Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries Schriftenreihe des IME Kraftfahrzeugbatterie (DE-588)4165422-5 gnd Nassmetallurgie (DE-588)4123820-5 gnd Metall (DE-588)4038860-8 gnd Recycling (DE-588)4076573-8 gnd Lithiumcarbonat (DE-588)4378397-1 gnd Grafit (DE-588)4158067-9 gnd Lithium-Ionen-Akkumulator (DE-588)7681721-0 gnd |
| subject_GND | (DE-588)4165422-5 (DE-588)4123820-5 (DE-588)4038860-8 (DE-588)4076573-8 (DE-588)4378397-1 (DE-588)4158067-9 (DE-588)7681721-0 (DE-588)4113937-9 |
| title | Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries |
| title_auth | Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries |
| title_exact_search | Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries |
| title_full | Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries Honggang Wang |
| title_fullStr | Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries Honggang Wang |
| title_full_unstemmed | Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries Honggang Wang |
| title_short | Development of a high efficient hydrometallurgical recycling process for automotive Li-ion batteries |
| title_sort | development of a high efficient hydrometallurgical recycling process for automotive li ion batteries |
| topic | Kraftfahrzeugbatterie (DE-588)4165422-5 gnd Nassmetallurgie (DE-588)4123820-5 gnd Metall (DE-588)4038860-8 gnd Recycling (DE-588)4076573-8 gnd Lithiumcarbonat (DE-588)4378397-1 gnd Grafit (DE-588)4158067-9 gnd Lithium-Ionen-Akkumulator (DE-588)7681721-0 gnd |
| topic_facet | Kraftfahrzeugbatterie Nassmetallurgie Metall Recycling Lithiumcarbonat Grafit Lithium-Ionen-Akkumulator Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028032902&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV016981907 |
| work_keys_str_mv | AT wanghonggang developmentofahighefficienthydrometallurgicalrecyclingprocessforautomotiveliionbatteries |