Polymer surface characterization:
Gespeichert in:
| Weitere Verfasser: | |
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| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin ; Boston, Mass.
<<De>> Gruyter
2014
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| Schriftenreihe: | De Gruyter graduate
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| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben |
| Beschreibung: | XIV, 292 S. Ill., graph. Darst. 24 cm |
| ISBN: | 3110275082 9783110275087 |
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CONTENTS
PREFACE * X
CONTRIBUTING AUTHORS XIII
STEFANIA COMETA AND LUIGIA SABBATINI
1 INTRODUCTORY REMARKS ON POLYMERS AND POLYMER SURFACES * 1
1.1 WHY POLYMERS? 1
1.1.1 GENERALITY 1
1.1.2 SYNTHESIS 1
1.1.3 CLASSIFICATION AND NOMENCLATURE 3
1.1.4 MORPHOLOGY AND PROPERTIES 4
1.2 WHY TO INVESTIGATE A POLYMER SURFACE? 8
1.2.1 NATURE AND DYNAMICS OF POLYMER SURFACES * 9
1.2.1.1 VIBRATIONAL DYNAMICS OF MACROMOLECULES 9
1.2.1.2 CHANGES IN THERMODYNAMIC PROPERTIES ON THE SURFACE *10
1.2.1.3 ROTATION OF FUNCTIONAL GROUPS ON POLYMER BACKBONES IN RESPONSE
TO DIFFERENT ENVIRONMENTAL CONDITIONS *13
1.2.1.4 SURFACE INTERDIFFUSION OR SEGREGATION OF COPOLYMERS OR POLYMER
BLENDS 17
1.2.2 SURFACE MODIFICATION OF POLYMERS 18
1.2.2.1 IMPROVEMENT OF WETTABILITY 18
1.2.2.2 IMPROVEMENT OF POROSITY OR ROUGHENING 19
1.2.2.3 IMPROVEMENT OF ADHESION 23
1.2.2.4 INTERACTION OF POLYMER WITH BIOLOGICAL ENVIRONMENT:
BIOCOMPATIBILITY 25
1.2.2.5 IMPROVEMENT OF CONDUCTIVITY 26
1.2.3 POSSIBILITY OF PREDICTING POLYMER PERFORMANCES BY SURFACE
CHARACTERIZATION TECHNIQUES 28
REFERENCES 30
BEAT A. KELLER
2 INVESTIGATION OF POLYMER SURFACES BY TIME-OF-FLIGHT SECONDARY ION
MASS SPECTROMETRY*39
2.1 INTRODUCTION 39
2.1.1 ANALYSIS OF SURFACES 39
2.1.2 THE SIMS PROCESS: A DETAILED APPROACH OF THEORY AND
INSTRUMENTS 40
2.1.2.1 SPUTTER PROCESS AND SSIMS APPROACH 41
2.1.2.2 MASS ANALYZER SYSTEMS 43
2.1.2.3 ION SOURCES AND PRIMARY IONS 43
2.1.2.4 SURFACE IONIZATION ION GUNS 44
HTTP://D-NB.INFO/1031968768
VIII *
CONTENTS
2.1.2.5 DUOPLASMATRON AND GAS ION SOURCES 45
2.1.2.6 LIQUID METAL ION GUNS 45
2.1.2.7 GAS CLUSTER ION SOURCES 46
2.1.2.8 HIGH-RESOLUTION ION IMAGES OBTAINED FROM CLUSTER LMIG SOURCES
2.2 TOF-SIMS INVESTIGATIONS OF POLYMER MATERIALS 49
2.2.1 GENERAL REMARKS 49
2.2.2 POLYMERS 49
2.2.2.1 POLYDIMETHYLSILOXANE 51
2.2.2.2 POLYSTYRENE 52
2.2.2.3 POLYACRYLATES 53
2.2.2.4 FLUORINATED POLYMERS 53
2.2.2.5 POLY(ETHYLENETEREPHTHALATE) 55
2.2.2.6 POLYETHYLENE GLYCOL 55
2.2.2.7 SPECTRA LIBRARIES AND G-SIMS APPROACH 55
2.2.2.8 MULTIVARIATE ANALYSIS AND PRINCIPAL COMPONENT ANALYSIS 57
2.2.3 POLYMER, ADDITIVES 58
2.2.4 COPOLYMERS 59
2.2.5 MULTICOMPONENT POLYMERS (POLYMER BLENDS) 62
2.2.6 PLASMA MODIFICATION AND DEPOSITION * 63
2.2.7 OTHER APPLICATIONS 65
REFERENCES 66
ELVIRA DE GIGLIO, NICOLETTA DITARANTO, AND LUIGIA SABBATINI
3 POLYMER SURFACE CHEMISTRY: CHARACTERIZATION BY XPS * 73
3.1 INTRODUCTION 73
3.2 PHOTOELECTRON SPECTROSCOPY: A BRIEF HISTORY 74
3.2.1 BASIC PRINCIPLES 74
3.2.2 SPECTROSCOPIC AND X-RAY NOTATIONS 76
3.3 INSTRUMENTATION 76
3.3.1 VACUUM SYSTEM 78
3.3.2 X-RAY SOURCES 78
3.3.2.1 DUAL MG/AL ANODE X-RAY TUBE 78
3.3.2.2 MONOCHROMATIC SOURCE 79
3.3.2.3 SYNCHROTRON RADIATION SOURCE * 79
3.3.3 ENERGY ANALYZERS 79
3.3.4 DETECTORS 81
3.3.5 CHARGE COMPENSATION 81
3.3.6 SMALL-AREA XPS: IMAGING AND MAPPING 82
3.3.7 AMBIENT-PRESSURE PHOTOELECTRON SPECTROSCOPY 83
3.4 CHEMICAL INFORMATION FROM XPS 83
3.5 CHEMICAL SHIFT AND ITS SIGNIFICANCE IN THE ANALYSIS OF POLYMERS 8
3.6 CHEMICAL DERIVATIZATION TECHNIQUES IN CONJUNCTION WITH XPS 89
3.7 POLYMERS SURFACE SEGREGATION 93
CONTENTS *
IX
3.8 POLYMERS PHYSICAL TREATMENTS/GRAFTING 98
3.9 POLYMERS AGING 104
REFERENCES 107
FITIPPO MANGOLINI AND ANTONELLA ROSSI
4 ATTENUATED TOTAL REFLECTION-FOURIER TRANSFORM INFRARED
SPECTROSCOPY: A POWERFUL TOOL FOR INVESTIGATING POLYMER SURFACES
AND INTERFACES *113
4.1 PRINCIPLES OF FOURIER TRANSFORM INFRARED SPECTROSCOPY *113
4.2 THEORY OF ATTENUATED TOTAL REFLECTION FTIR SPECTROSCOPY 114
4.2.1 PROPAGATION OF IR RADIATION THROUGH A PLANAR INTERFACE BETWEEN
TWO ISOTROPIC MEDIA 114
4.2.2 PROPAGATION OF IR RADIATION THROUGH STRATIFIED MEDIA 118
4.2.3 PENETRATION DEPTH AND EFFECTIVE THICKNESS *121
4.2.3.1 PENETRATION DEPTH IN ATR/FTIR
SPECTROSCOPIC ANALYSIS
OF POLYMERS 125
4.2.4 TRANSMISSION FTIR VS ATR/FTIR SPECTROSCOPY 126
4.3 EXPERIMENTAL METHODS IN ATR/FTIR SPECTROSCOPY 128
4.3.1 INTERNAL REFLECTION ELEMENTS 128
4.3.2 INTERNAL REFLECTION ATTACHMENTS 129
4.3.3 METAL UNDERLAYER ATR/FTIR SPECTROSCOPY 130
4.3.3.1 EFFECT OF METAL UNDERLAYER ON PENETRATION DEPTH IN ATR/FTIR
SPECTROSCOPIC ANALYSIS OF POLYMERS 133
4.4 POTENTIALS AND LIMITATIONS OF ATR/FTIR SPECTROSCOPY 137
4.5 APPLICATIONS OF ATR/FTIR SPECTROSCOPY 138
4.5.1 ATR/FTIR SPECTROSCOPY IN POLYMER SCIENCE 138
4.5.2 IN SITU ATR/FTIR SPECTROSCOPY OF TRIBOCHEMICAL PHENOMENA 140
ACKNOWLEDGMENTS 147
REFERENCES 147
DALIA YABLON
5 SCANNING PROBE MICROSCOPY OF POLYMERS 153
5.1 INTRODUCTION 153
5.2 SAMPLE PREPARATION 155
5.3 PHASE IMAGING 156
5.3.1 BACKGROUND ON PHASE IMAGING 156
5.3.2 APPLICATIONS OF PHASE IMAGING TO POLYMER MATERIALS 156
5.4 MULTIFREQUENCY IMAGING 159
5.5 NANORHEOLOGICAL MAPPING 160
5.6 THERMAL/SPECTROSCOPIC MEASUREMENTS 163
5.7 ENVIRONMENTAL MEASUREMENTS 164
5.8 CONCLUSIONS 165
REFERENCES 166
X * CONTENTS
MIROSLAV §LOUF, TAT'ANA VACKOVA, FRANTISEK LEDNICKY, AND PETR WANDROL
6 POLYMER SURFACE MORPHOLOGY: CHARACTERIZATION BY ELECTRON
MICROSCOPIES 169
6.1 INTRODUCTION 169
6.2 SCANNING ELECTRON MICROSCOPY 169
6.2.1 SEM: PRINCIPLES 169
6.2.1.1 MICROSCOPE AND IMAGE FORMATION *169
6.2.1.2 INTERACTION OF THE ELECTRON BEAM WITH THE SPECIMEN *171
6.2.2 SEM: CLASSICAL MODES 173
6.2.2.1 SE IMAGING 174
6.2.2.2 BSE IMAGING 174
6.2.2.3 EDX SPECTRA 175
6.2.2.4 STEM IMAGING 177
6.2.3 SEM: MODERN TRENDS 177
6.2.3.1 VARIABLE-PRESSURE SEM 177
6.2.3.2 VARIABLE-TEMPERATURE SEM 179
6.2.3.3 LOW-VOLTAGE SEM 180
6.2.3.4 MULTIDIMENSIONAL SEM 180
6.2.4 SEM: FURTHER POSSIBILITIES 181
6.2.4.1 SPECTROSCOPIC METHODS 181
6.2.4.2 METHODS CONNECTED WITH CRYSTAL STRUCTURE OF SAMPLES 182
6.2.4.3 METHODS USING SAMPLE-SPECIFIC INTERACTIONS WITH ELECTRON BEAM
182
6.3 TRANSMISSION ELECTRON MICROSCOPY 182
6.4 SAMPLE PREPARATION 183
6.4.1 OVERVIEW OF POLYMER MATERIALS 183
6.4.2 SPECIFIC FEATURES OF POLYMER MATERIALS *183
6.4.2.1 CHARGING AND ELECTRON-BEAM DAMAGE *183
6.4.2.2 SKIN-CORE EFFECT 184
6.4.2.3 LOW CONTRAST BETWEEN COMPONENTS 185
6.4.3 PREPARATION TECHNIQUES FOR POLYMER MATERIALS 185
6.4.3.1 DIRECT OBSERVATION OF POLYMER SURFACE 186
6.4.3.2 FRACTURING 186
6.4.3.3 ETCHING 187
6.4.3.4 CUTTING AND STAINING 188
6.4.3.5 SPECIAL TECHNIQUES 189
6.5 APPLICATIONS 191
6.5.1 HOMOPOLYMERS 191
6.5.2 COPOLYMERS 193
6.5.3 POLYMER BLENDS 195
6.5.4 POLYMER COMPOSITES 197
6.5.5 SPECIAL APPLICATIONS 198
6.5.5.1 LOW-VOLTAGE SEM IN POLYMER SCIENCE 198
CONTENTS
XI
6.5.5.2 WET SPECIMENS IN POLYMER SCIENCE 199
6.5.5.3 FURTHER APPLICATIONS 200
ACKNOWLEDGMENTS 201
REFERENCES 201
FABIO PALUMBOAND ROSA DI MUNDO
7 WETTABILITY: SIGNIFICANCE AND MEASUREMENT * 207
7.1 INTRODUCTION 207
7.2 CA AND SURFACE ENERGY 210
7.2.1 SURFACE ENERGY EVALUATION 211
7.2.1.1 CRITICAL SURFACE ENERGY METHOD 212
7.2.1.2 MULTICOMPONENT APPROACHES 215
7.2.1.3 PARTICULAR CASES: HIGH-ENERGY SURFACES AND GRANULAR MATERIALS
215
7.2.2 CONSIDERATIONS ON SURFACE ENERGY EVALUATION 216
7.3 CA HYSTERESIS 218
7.4 MEASUREMENT METHODS FOR CA 222
7.4.1 DIRECT MEASUREMENT BY OPTICAL GONIOMETRY 222
7.4.2 FORCE TENSIOMETRY 225
7.4.3 APPROACH COMPARISON 226
7.5 APPLICATION OF CA MEASUREMENT 227
7.5.1 FROM HYDROPHOBIC TO WATER- AND OIL-REPELLENT MATERIALS 227
7.5.2 HYDROPHILIC TO SUPER-HYDROPHILIC MATERIALS 233
7.5.3 HYDROPHOBIC RECOVERY OF HYDROPHILIC SURFACES 235
7.5.4 CA ON POROUS SURFACES 238
7.5.5 ACID-BASE CHARACTERIZATION OF POLYMERIC SURFACES * 239
REFERENCES 241
EVA BITTRICH AND KLAUS-JOCHEN EICHHORN
8 ADVANCES OF SPECTROSCOPIC ELLIPSOMETRY IN THE ANALYSIS OF THIN POLYMER
FILMS-POLYMER INTERFACES 247
8.1 INTRODUCTION 247
8.1.1 BASICS OF ELLIPSOMETRY 247
8.2 NEW ELLIPSOMETRIC METHODS, TECHNIQUES, AND ASPECTS 250
8.2.1 OPTICAL DISPERSION 250
8.2.2 IN SITU SETUPS 253
8.2.2.1 LIQUID CELLS FOR MEASUREMENTS IN SOLUTION 253
8.2.2.2 COUPLING ELLIPSOMETRY WITH QUARTZ CRYSTAL MICROBALANCE 254
8.2.2.3 TOTAL INTERNAL REFLECTION ELLIPSOMETRY 256
8.2.3 IN-LINE MONITORING 257
8.2.3.1 MONITORING PROCESSES IN A VACUUM CHAMBER 258
8.2.3.2 R2R FABRICATION PROCESSES 258
8.2.4 MICROPATTERNED FILMS 259
XII * CONTENTS
8.2.4.1 VIS IMAGING ELLIPSOMETRY 259
8.2.4.2 MICROFOCUS-MAPPING IR ELLIPSOMETRY 260
8.3 SELECTED ARCHITECTURES OF POLYMER FILMS, BLENDS,
AND COMPOSITES 261
8.3.1 POLYMER BLENDS AND CROSS-LINKED POLYMER FILMS 261
8.3.2 TG IN THIN POLYMER FILMS OF DIFFERENT ARCHITECTURES:
CONFINEMENT EFFECTS * 262
8.3.3 POLYMER-NP COMPOSITES 264
8.3.4 POLYMERS IN NANOSTRUCTURED SURFACES 266
8.4 POLYMER LAYERS ABSORBING IN THE VIS SPECTRAL RANGE 267
8.4.1 CHEMICAL MODIFICATION WITH DYE MOLECULES 267
8.4.2 SEMICONDUCTING POLYMERS AND BLENDS FOR OPV AND OLED 268
8.5 SWELLING AND ADSORPTION PROCESSES: PROTEINS AND STIMULI-RESPONSIVE
POLYMERS 271
8.5.1 SWELLING OF STIMULI-RESPONSIVE POLYMER LAYERS 271
8.5.2 PROTEIN ADSORPTION AT SOFT POLYMER SURFACES 274
REFERENCES 278
INDEX * 287 |
| any_adam_object | 1 |
| author2 | Sabbatini, Luigia |
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| author_facet | Sabbatini, Luigia |
| building | Verbundindex |
| bvnumber | BV042072039 |
| classification_rvk | UV 3300 UV 7000 VE 8000 |
| ctrlnum | (OCoLC)864644702 (DE-599)DNB1031968768 |
| dewey-full | 620.1920427 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 620 - Engineering and allied operations |
| dewey-raw | 620.1920427 |
| dewey-search | 620.1920427 |
| dewey-sort | 3620.1920427 |
| dewey-tens | 620 - Engineering and allied operations |
| discipline | Chemie / Pharmazie Maschinenbau / Maschinenwesen Physik |
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| id | DE-604.BV042072039 |
| illustrated | Illustrated |
| indexdate | 2024-09-10T01:24:02Z |
| institution | BVB |
| isbn | 3110275082 9783110275087 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-027513280 |
| oclc_num | 864644702 |
| open_access_boolean | |
| owner | DE-11 DE-703 |
| owner_facet | DE-11 DE-703 |
| physical | XIV, 292 S. Ill., graph. Darst. 24 cm |
| publishDate | 2014 |
| publishDateSearch | 2014 |
| publishDateSort | 2014 |
| publisher | <<De>> Gruyter |
| record_format | marc |
| series2 | De Gruyter graduate |
| spelling | Polymer surface characterization ed. by Luigia Sabbatini Berlin ; Boston, Mass. <<De>> Gruyter 2014 XIV, 292 S. Ill., graph. Darst. 24 cm txt rdacontent n rdamedia nc rdacarrier De Gruyter graduate Literaturangaben Oberflächeneigenschaft (DE-588)4219221-3 gnd rswk-swf Kunststoff (DE-588)4033676-1 gnd rswk-swf Oberflächenphysik (DE-588)4134881-3 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Oberflächenanalyse (DE-588)4172243-7 gnd rswk-swf Grenzflächenphysik (DE-588)4452968-5 gnd rswk-swf Polymere (DE-588)4046699-1 s Kunststoff (DE-588)4033676-1 s Oberflächenanalyse (DE-588)4172243-7 s DE-604 Oberflächenphysik (DE-588)4134881-3 s Grenzflächenphysik (DE-588)4452968-5 s Oberflächeneigenschaft (DE-588)4219221-3 s Sabbatini, Luigia edt Erscheint auch als Online-Ausgabe 978-3-11-028811-7 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4269445&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027513280&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Polymer surface characterization Oberflächeneigenschaft (DE-588)4219221-3 gnd Kunststoff (DE-588)4033676-1 gnd Oberflächenphysik (DE-588)4134881-3 gnd Polymere (DE-588)4046699-1 gnd Oberflächenanalyse (DE-588)4172243-7 gnd Grenzflächenphysik (DE-588)4452968-5 gnd |
| subject_GND | (DE-588)4219221-3 (DE-588)4033676-1 (DE-588)4134881-3 (DE-588)4046699-1 (DE-588)4172243-7 (DE-588)4452968-5 |
| title | Polymer surface characterization |
| title_auth | Polymer surface characterization |
| title_exact_search | Polymer surface characterization |
| title_full | Polymer surface characterization ed. by Luigia Sabbatini |
| title_fullStr | Polymer surface characterization ed. by Luigia Sabbatini |
| title_full_unstemmed | Polymer surface characterization ed. by Luigia Sabbatini |
| title_short | Polymer surface characterization |
| title_sort | polymer surface characterization |
| topic | Oberflächeneigenschaft (DE-588)4219221-3 gnd Kunststoff (DE-588)4033676-1 gnd Oberflächenphysik (DE-588)4134881-3 gnd Polymere (DE-588)4046699-1 gnd Oberflächenanalyse (DE-588)4172243-7 gnd Grenzflächenphysik (DE-588)4452968-5 gnd |
| topic_facet | Oberflächeneigenschaft Kunststoff Oberflächenphysik Polymere Oberflächenanalyse Grenzflächenphysik |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4269445&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027513280&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT sabbatiniluigia polymersurfacecharacterization |