Calorimetry: fundamentals, instrumentation and applications
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| Main Authors: | , , |
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| Format: | Book |
| Language: | English |
| Published: |
Weinheim
Wiley-VCH
2014
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| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | XVIII, 280 S. Ill., graph. Darst. 25 cm |
| ISBN: | 9783527327614 9783527649372 9783527649389 |
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| 245 | 1 | 0 | |a Calorimetry |b fundamentals, instrumentation and applications |c Stefan M. Sarge ; Günther W. H. Höhne and Wolfgang Hemminger |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2014 | |
| 300 | |a XVIII, 280 S. |b Ill., graph. Darst. |c 25 cm | ||
| 336 | |b txt |2 rdacontent | ||
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| 700 | 1 | |a Hemminger, Wolfgang |d 1941- |e Verfasser |0 (DE-588)123656249 |4 aut | |
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Record in the Search Index
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CONTENTS
PREFACE XIII
LIST OF QUANTITIES AND UNITS XV
INTRODUCTION CALORIMETRY: DEFINITION, APPLICATION FIELDS AND UNITS 1
DEFINITION OF CALORIMETRY 1
APPLICATION FIELDS FOR CALORIMETRY 1
FIRST EXAMPLE FROM LIFE SCIENCES 2
SECOND EXAMPLE FROM MATERIAL SCIENCE 2
THIRD EXAMPLE FROM LEGAL METROLOGY 2
UNITS 3
FURTHER READING 4
REFERENCES 5
PART ONE FUNDAMENTALS OF CALORIMETRY 7
1 METHODS OF CALORIMETRY 9
1.1 COMPENSATION OF THE THERMAL EFFECT 9
1.1.1 COMPENSATION BY A PHASE TRANSITION 9
1.1.2 COMPENSATION BY ELECTRIC EFFECTS 12
1.2 MEASUREMENT OF TEMPERATURE DIFFERENCES 13
1.2.1 MEASUREMENT OF TIME-DEPENDENT TEMPERATURE DIFFERENCES 13
1.2.2 MEASUREMENT OF LOCAL TEMPERATURE DIFFERENCES 15
1.2.2.1 FIRST EXAMPLE: FLOW CALORIMETER 15
1.2.2.2 SECOND EXAMPLE: HEAT FLOW RATE CALORIMETER 15
1.3 SUMMARY OF MEASURING PRINCIPLES 16
REFERENCES 17
2 MEASURING INSTRUMENTS 19
2.1 MEASUREMENT OF AMOUNT OF SUBSTANCE 19
2.1.1 WEIGHING 20
2.1.2 VOLUME MEASUREMENT 20
HTTP://D-NB.INFO/1038860849
VI | CONTENTS
2.1.3 PRESSURE MEASUREMENT 21
2.1.4 FLOW MEASUREMENT 21
2.2 MEASUREMENT OF ELECTRIC QUANTITIES 21
2.3 MEASUREMENT OF TEMPERATURES 22
2.3.1 THERMOMETERS 23
2.3.1.1 LIQUID-IN-GLASS THERMOMETERS 23
2.3.1.2 GAS THERMOMETERS 24
2.3.1.3 VAPOR PRESSURE THERMOMETERS 24
2.3.1.4 RESISTANCE THERMOMETERS 25
2.3.1.5 SEMICONDUCTORS 26
2.3.1.6 PYROMETERS 26
2.3.2 THERMOCOUPLES 27
2.4 CHEMICAL COMPOSITION 29
REFERENCES 29
3 FUNDAMENTALS OF THERMODYNAMICS 31
3.1 STATES AND PROCESSES 31
3.1.1 THERMODYNAMIC VARIABLES (FUNCTIONS OF STATE) 31
3.1.2 FORMS OF ENERGY, FUNDAMENTAL FORM, AND THERMODYNAMIC
POTENTIAL FUNCTION 34
3.1.2.1 FUNDAMENTAL FORM 35
3.1.2.2 THERMODYNAMIC POTENTIAL FUNCTION 35
3.1.3 EQUILIBRIUM 38
3.1.4 REVERSIBLE AND IRREVERSIBLE PROCESSES 41
3.1.5 THE LAWS OF THERMODYNAMICS 42
3.1.5.1 THE ZEROTH LAW 42
3.1.5.2 THE FIRST LAW 42
3.1.5.3 THE SECOND LAW 42
3.1.5.4 THE THIRD LAW 43
3.1.6 MEASUREMENT OF THERMODYNAMIC STATE FUNCTIONS 43
3.2 PHASES AND PHASE TRANSITIONS 47
3.2.1 MULTIPHASE SYSTEMS 47
3.2.2 PHASE TRANSITIONS 50
3.2.3 GIBBS PHASE RULE 52
3.2.4 MEASUREMENT OF VARIABLES OF STATE DURING PHASE TRANSITIONS 56
REFERENCES 59
4 HEAT TRANSPORT PHENOMENA 61
4.1 HEAT CONDUCTION 61
4.2 CONVECTION 64
4.3 HEAT RADIATION 65
4.4 HEAT TRANSFER 67
4.5 ENTROPY INCREASE DURING HEAT EXCHANGE 67
4.6 CONCLUSIONS CONCERNING CALORIMETRY 68
REFERENCES 71
CONTENTS I VII
5 SURROUNDINGS AND OPERATING CONDITIONS 73
5.1 THE ISOTHERMAL CONDITION 74
5.2 THE ISOPERIBOL CONDITION 75
5.3 THE ADIABATIC CONDITION 75
5.4 THE SCANNING CONDITION 76
REFERENCE 79
6 MEASUREMENTS AND EVALUATION 81
6.1 CONSEQUENCES OF TEMPERATURE RELAXATION WITHIN THE SAMPLE 81
6.1.1 FIRST EXAMPLE: CHEMICAL REACTION 81
6.1.2 SECOND EXAMPLE: BIOLOGICAL SYSTEM 82
6.1.3 THIRD EXAMPLE: FIRST-ORDER PHASE TRANSITIONS 83
6.2 TYPICAL RESULTS FROM DIFFERENT CALORIMETERS 86
6.2.1 ADIABATIC CALORIMETERS 86
6.2.2 ISOPERIBOL CALORIMETERS 89
6.2.3 DIFFERENTIAL SCANNING CALORIMETERS 93
6.3 RECONSTRUCTION OF THE TRUE SAMPLE HEAT FLOW RATE FROM THE
MEASURED FUNCTION 101
6.3.1 RECONSTRUCTION OF THE TEMPERATURE FIELD FOR NEGATIVE TIMES 101
6.3.2 THE CONVOLUTION INTEGRAL AND ITS VALIDITY 102
6.3.3 SOLUTION OF THE CONVOLUTION INTEGRAL 105
6.3.4 OBTAINING THE APPARATUS FUNCTION 106
6.3.5 APPLICATION LIMITS AND ESTIMATION OF UNCERTAINTY 107
6.4 SPECIAL EVALUATIONS 109
6.4.1 DETERMINATION OF THE SPECIFIC HEAT CAPACITY 109
6.4.2 DETERMINATION OF THE KINETIC PARAMETERS OF A
CHEMICAL REACTION 109
6.4.3 DETERMINATION OF PHASE TRANSITION TEMPERATURES 111
6.4.4 DETERMINATION OF HEATS OF TRANSITION 112
6.4.5 DETERMINATION OF THE PURITY OF A SUBSTANCE 114
6.5 DETERMINATION OF THE MEASUREMENT UNCERTAINTY 115
REFERENCES 121
PART TWO PRACTICE OF CALORI
METRY 123
7 CALORIMETERS 125
7.1 FUNCTIONAL COMPONENTS AND ACCESSORIES 125
7.2 HEATING METHODS 126
7.3 COOLING METHODS 126
7.4 COMMENTS ON CONTROL SYSTEMS 128
7.5 THERMOSTATS 131
7.6 ON THE CLASSIFICATION OF CALORIMETERS 131
1J ON THE CHARACTERIZATION OF CALORIMETERS 132
7.8 ISOTHERMAL CALORIMETERS 134
7.8.1 PHASE TRANSITION CALORIMETERS 134
VIIII
CONTENTS
7.8.1.1 FIRST EXAMPLE: ICE CALORIMETER 135
7.8.1.2 SECOND EXAMPLE: CALORIMETER WITH LIQUID-GAS PHASE TRANSITION 137
7.8.2 ISOTHERMAL CALORIMETERS WITH ELECTRICAL COMPENSATION 141
7.8.2.1 FIRST EXAMPLE: CALORIMETER ACCORDING TO TIAN 142
7.8.2.2 SECOND EXAMPLE: ISOTHERMAL TITRATION CALORIMETER 143
7.8.2.3 THIRD EXAMPLE: ISOTHERMAL FLOW CALORIMETER 144
7.9 CALORIMETERS WITH HEAT EXCHANGE BETWEEN THE SAMPLE AND
SURROUNDINGS 144
7.9.1 ISOPERIBOL CALORIMETERS WITH UNCONTROLLED HEAT EXCHANGE 145
7.9.1.1 FIRST EXAMPLE: CLASSIC LIQUID (OR MIXING) CALORIMETER 145
7.9.1.2 SECOND EXAMPLE: COMBUSTION CALORIMETER 148
7.9.1.3 THIRD EXAMPLE: DROP CALORIMETER 151
7.9.2 ISOPERIBOL CALORIMETER WITH CONTROLLED HEAT EXCHANGE 154
7.9.2.1 FIRST EXAMPLE: ACTIVITY MONITOR 159
7.9.2.2 SECOND EXAMPLE: LARGE-VOLUME BATTERY CALORIMETER 160
7.9.2.3 THIRD EXAMPLE: CALVET CALORIMETER
161
7.9.2.4 FOURTH EXAMPLE: WHOLE-BODY CALORIMETER 169
7.9.3 ISOPERIBOL FLOW CALORIMETER 170
7.9.3.1 FIRST EXAMPLE: THE PICKER CALORIMETER 175
7.9.3.2 SECOND EXAMPLE: FLOW CALORIMETER FOR HIGH-PRESSURE AND HIGH-
TEMPERATURE MEASUREMENTS 176
7.9.3.3 THIRD EXAMPLE: GAS COMBUSTION CALORIMETER 177
7.9.3.4 FOURTH EXAMPLE: MICROCHIP FLOW CALORIMETER 177
7.9.4 CALORIMETERS WITH LINEAR TEMPERATURE CHANGE OF THE
SURROUNDINGS 178
7.9.4.1 FIRST EXAMPLE: HEAT FLOW DIFFERENTIAL SCANNING CALORIMETER 179
7.9.4.2 SECOND EXAMPLE: POWER-COMPENSATED DIFFERENTIAL SCANNING
CALORIMETER 183
7.9.4.3 THIRD EXAMPLE: PRIVALOV CALORIMETER 185
7.9.5 CALORIMETERS WITH NONLINEAR TEMPERATURE CHANGE OF THE
SURROUNDINGS 186
7.9.5.1 FIRST EXAMPLE: TEMPERATURE-MODULATED DSC 187
7.9.5.2 SECOND EXAMPLE: STEPSCAN DIFFERENTIAL SCANNING CALORIMETRY 189
7.9.5.3 THIRD EXAMPLE: ADVANCED MULTIFREQUENCY TMDSC 189
7.10 ADIABATIC CALORIMETERS 190
7.10.1 CALORIMETERS WITH A THERMALLY ISOLATED SAMPLE 190
7.10.1.1 FIRST EXAMPLE: NERNST CALORIMETER 191
7.10.1.2 SECOND EXAMPLE: LOW-TEMPERATURE CALORIMETER 192
7.10.1.3 THIRD EXAMPLE: AC CALORIMETER 194
7.10.1.4 FOURTH EXAMPLE: 3 U TECHNIQUE 195
7.10.1.5 NERNST'S METHOD WITH A CONTACTLESS ENERGY SUPPLY 196
7.10.2 CALORIMETERS WITH ZERO TEMPERATURE DIFFERENCE AGAINST THE
SURROUNDINGS 197
7.10.2.1 FIRST EXAMPLE: ADIABATIC REACTION CALORIMETER 198
7.10.2.2 SECOND EXAMPLE: ADIABATIC FLOW CALORIMETER 199
CONTENTS
IIX
7.10.2.3 THIRD EXAMPLE: ADIABATIC WHOLE-BODY CALORIMETER 199
7.10.2.4 FOURTH EXAMPLE: ADIABATIC SCANNING CALORIMETER 200
7.10.3 QUASI-ADIABATIC CALORIMETRY BY SUDDEN HEAT EVENTS 201
7.10.3.1 EXAMPLE: PULSE HEATING CALORIMETER 201
7.11 OTHER CALORIMETERS 202
7.11.1 REACTION CALORIMETERS 202
7.11.1.1 FIRST EXAMPLE: REACTION CALORIMETER 203
7.11.1.2 SECOND EXAMPLE: ACCELERATING RATE CALORIMETER (ARC) 204
7.11.2 SPECIAL CALORIMETERS 206
7.11.2.1 PHOTOCALORIMETERS 206
7.11.2.2 PRESSURE CALORIMETERS 206
7.11.2.3 PRESSURE PERTURBATION CALORIMETER 206
7.11.2.4 CEMENT CALORIMETER 207
REFERENCES 207
8 RECENT DEVELOPMENTS 213
8.1 MICROCHIP CALORIMETRY 214
8.1.1 FIRST EXAMPLE: THIN-FILM DIFFERENTIAL SCANNING CALORIMETER 216
8.1.2 SECOND EXAMPLE: LOW-TEMPERATURE AC NANOCALORIMETER 217
8.2 ULTRAFAST CALORIMETRY 217
8.2.1 FIRST EXAMPLE: ULTRAFAST NANOCALORIMETER 218
8.2.2 SECOND EXAMPLE: FLASH DIFFERENTIAL SCANNING CALORIMETER 220
8.3 EXTREME RANGES OF STATE 220
8.3.1 HIGH PRESSURE 221
8.3.1.1 EXAMPLE: POWER-COMPENSATED HIGH-PRESSURE DSC 222
8.3.2 HIGH TEMPERATURE 222
8.3.2.1 EXAMPLE: LEVITATION CALORIMETRY ON NICKEL, IRON, VANADIUM, AND
NIOBIUM 223
8.3.3 STRONG MAGNETIC FIELDS 224
8.3.3.1 EXAMPLE: INFLUENCE OF MAGNETIC FIELDS ON POINT DEFECTS 224
8.3.4 PLASMA SURROUNDINGS 224
8.3.4.1 EXAMPLE: CALIBRATION USING A LASER BEAM 224
8.4 CALORIMETRY AS AN ANALYTICAL AND DIAGNOSTIC TOOL 225
8.4.1 FIRST EXAMPLE: "ARTIFICIAL NOSE" 225
8.4.2 SECOND EXAMPLE: INFECTION DIAGNOSTICS 225
REFERENCES 226
9 CALORIMETRIC MEASUREMENTS: GUIDELINES AND APPLICATIONS 229
9.1 GENERAL CONSIDERATIONS 229
9.1.1 SENSITIVITY (AX/QOR AX/ATF ) 230
9.1.2 NOISE (8QOR 8$) 230
9.1.3 LINEARITY (XO
UT
= K* XI*) AND
LINEARITY ERROR (8K/K) 232
9.1.4 APPARATUS FUNCTION (F
APP
(T))
232
9.1.5 ACCURACY AND TOTAL ERROR ({QMEASURED - QTRUE}/QTRUE) 233
9.1.6 REPEATABILITY AND RANDOM UNCERTAINTY (AQ/Q) 235
X I
CONTENTS
CONCLUSION 235
9.2
GUIDELINES TO CALORIMETRIC EXPERIMENTS 235
9.2.1
DEFINITION OF THE PROBLEM TO BE INVESTIGATED
236
9.2.2
SELECTION OF THE PROPER CALORIMETER 237
9.2.2.1
CALORIMETER REQUIREMENTS 237
9.2.2.2
SELECTION OF THE CALORIMETER 238
9.2.3
TESTING OF THE CALORIMETER 239
9.2.3.1 CALIBRATION 239
9.2.3.2 OTHER TESTING 242
9.2.4
PERFORMING THE EXPERIMENT 243
9.2.4.1
PREPARATION OF THE SAMPLE 243
9.2.4.2
CALORIMETRIC MEASUREMENT 244
9.2.4.3 EVALUATION OF THE MEASUREMENT 245
9.2.5
INTERPRETATION OF THE RESULTS 245
9.2.6
UNCERTAINTY ESTIMATION 246
9.3
CALORIMETRIC APPLICATIONS 246
9.3.1
EXAMPLE FROM MATERIAL SCIENCE 247
9.3.1.1
DEFINITION OF THE PROBLEM TO BE INVESTIGATED
247
9.3.1.2 SELECTION OF THE CALORIMETER 247
9.3.1.3
CALORIMETRIC EXPERIMENTS 248
9.3.1.4 EVALUATION OF THE MEASUREMENTS 248
9.3.1.5
INTERPRETATION OF THE RESULTS 251
9.3.1.6
UNCERTAINTY ESTIMATION 252
9.3.2
EXAMPLES FROM BIOLOGY 25 6
9.3.2.1
DEFINITION OF THE PROBLEM TO BE INVESTIGATED
256
9.3.2.2
SELECTION OF THE PROPER CALORIMETER 256
9.3.2.3
CALORIMETRIC EXPERIMENTS 257
9.3.2.4
EVALUATION OF THE RESULTS 258
9.3.2.5
CALORIMETRY ON HORNETS 258
9.3.2.6 UNCERTAINTY ESTIMATION 259
9.3.3 EXAMPLE FROM MEDICINE 259
9.3.3.1
DEFINITION OF THE PROBLEM TO BE INVESTIGATED
259
9.3.3.2 SELECTION OF THE PROPER CALORIMETER 259
9.3.3.3 CALORIMETRIC EXPERIMENT 260
9.3.3.4
EVALUATION OF THE MEASUREMENTS 260
9.3.3.5
INTERPRETATION OF THE RESULTS 260
9.3.3.6 UNCERTAINTY ESTIMATION 261
9.3.4 EXAMPLE FROM CHEMISTRY 261
9.3.4.1
DEFINITION OF THE PROBLEM TO BE INVESTIGATED
262
9.3.4.2
SELECTION OF THE PROPER CALORIMETER 262
9.3.4.3
CALORIMETRIC EXPERIMENT 263
9.3.4.4 EVALUATION OF THE MEASUREMENTS 263
9.3.4.5
INTERPRETATION OF THE RESULTS 264
9.3.4.6
UNCERTAINTY ESTIMATION 265
9.3.5
EXAMPLE FROM COMBUSTION CALORIMETRY 265
9.3.5.1 DEFINITION OF THE PROBLEM TO BE INVESTIGATED
9.3.5.2 SELECTION OF THE PROPER CALORIMETER 265
9.3.5.3 CALORIMETRIC EXPERIMENT 267
9.3.5.4 EVALUATION OF THE MEASUREMENTS 267
9.3.5.5 INTERPRETATION OF THE RESULTS 268
9.3.5.6 UNCERTAINTY ESTIMATION 268
REFERENCES 269
INDEX 271 |
| any_adam_object | 1 |
| author | Sarge, Stefan M. Höhne, Günther 1937- Hemminger, Wolfgang 1941- |
| author_GND | (DE-588)1049865413 (DE-588)118000330 (DE-588)123656249 |
| author_facet | Sarge, Stefan M. Höhne, Günther 1937- Hemminger, Wolfgang 1941- |
| author_role | aut aut aut |
| author_sort | Sarge, Stefan M. |
| author_variant | s m s sm sms g h gh w h wh |
| building | Verbundindex |
| bvnumber | BV041793841 |
| classification_rvk | VG 7100 |
| ctrlnum | (OCoLC)864546115 (DE-599)DNB1038860849 |
| dewey-full | 543.26 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543.26 |
| dewey-search | 543.26 |
| dewey-sort | 3543.26 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV041793841 |
| illustrated | Illustrated |
| indexdate | 2024-09-10T01:12:01Z |
| institution | BVB |
| isbn | 9783527327614 9783527649372 9783527649389 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-027239400 |
| oclc_num | 864546115 |
| open_access_boolean | |
| owner | DE-29T DE-11 DE-703 DE-1050 DE-355 DE-BY-UBR DE-1043 DE-210 DE-19 DE-BY-UBM DE-1029 |
| owner_facet | DE-29T DE-11 DE-703 DE-1050 DE-355 DE-BY-UBR DE-1043 DE-210 DE-19 DE-BY-UBM DE-1029 |
| physical | XVIII, 280 S. Ill., graph. Darst. 25 cm |
| publishDate | 2014 |
| publishDateSearch | 2014 |
| publishDateSort | 2014 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Sarge, Stefan M. Verfasser (DE-588)1049865413 aut Calorimetry fundamentals, instrumentation and applications Stefan M. Sarge ; Günther W. H. Höhne and Wolfgang Hemminger Weinheim Wiley-VCH 2014 XVIII, 280 S. Ill., graph. Darst. 25 cm txt rdacontent n rdamedia nc rdacarrier Kalorimetrie (DE-588)4029367-1 gnd rswk-swf Kalorimetrie (DE-588)4029367-1 s DE-604 Höhne, Günther 1937- Verfasser (DE-588)118000330 aut Hemminger, Wolfgang 1941- Verfasser (DE-588)123656249 aut Erscheint auch als Online-Ausgabe 978-3-527-64936-5 Erscheint auch als Online-Ausgabe 978-3-527-64939-6 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4431075&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027239400&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Sarge, Stefan M. Höhne, Günther 1937- Hemminger, Wolfgang 1941- Calorimetry fundamentals, instrumentation and applications Kalorimetrie (DE-588)4029367-1 gnd |
| subject_GND | (DE-588)4029367-1 |
| title | Calorimetry fundamentals, instrumentation and applications |
| title_auth | Calorimetry fundamentals, instrumentation and applications |
| title_exact_search | Calorimetry fundamentals, instrumentation and applications |
| title_full | Calorimetry fundamentals, instrumentation and applications Stefan M. Sarge ; Günther W. H. Höhne and Wolfgang Hemminger |
| title_fullStr | Calorimetry fundamentals, instrumentation and applications Stefan M. Sarge ; Günther W. H. Höhne and Wolfgang Hemminger |
| title_full_unstemmed | Calorimetry fundamentals, instrumentation and applications Stefan M. Sarge ; Günther W. H. Höhne and Wolfgang Hemminger |
| title_short | Calorimetry |
| title_sort | calorimetry fundamentals instrumentation and applications |
| title_sub | fundamentals, instrumentation and applications |
| topic | Kalorimetrie (DE-588)4029367-1 gnd |
| topic_facet | Kalorimetrie |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4431075&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027239400&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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