Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes:
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| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
2013
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIII, 130 S. graph. Darst. 30 cm |
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| 245 | 1 | 0 | |a Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes |c von Yang Zhang |
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Datensatz im Suchindex
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| adam_text | TABLE OF CONTENTS
ZUSAMMENFASSUNG I
ABSTRACT ILL
TABLE OF CONTENTS V
LIST OF FIGURES VII
CHAPTER 1 INTRODUCTION 1
1.1 SYNTHESIS AND ISOLATION OF ENDOHEDRAL FULLERENES 1
1.2 PROPERTIES OF METAL NITRIDE CLUSTERFULLERENES 3
1.2.1 SPECTROSCOPIC PROPERTIES 3
1.2.2 ELECTROCHEMICAL AND SPECTROELECTROCHEMICAL PROPERTIES 6
1.2.3 MAGNETIC PROPERTIES 11
1.3 MOTIVATION 16
CHAPTER 2 SYNTHESIS AND ISOLATION OF MIXED METAL NITRIDE
CLUSTERFULLERENES 19
2.1 INTRODUCTION 19
2.2 SYNTHESIS AND ISOLATION OF HO
X
M3.
X
N@CSO 21
2.2.2 SYNTHESIS AND ISOLATION OF HO
X
SC3-
X
N@C8O (X= 1, 2) 21
2.2.2 SYNTHESIS AND ISOLATION OF HO
X
Y3-
X
N@CGO (X=L, 2) 26
2.2.3 SYNTHESIS AND ISOLATION OF HO
X
LU3-
X
N@CGO (X=L, 2) 30
2.3 SYNTHESIS AND ISOLATION OF CE-BASED MMNCFS 35
2.3.1 SYNTHESIS AND ISOLATION OF CEY2N@CGO (I) 35
2.3.2 SYNTHESIS AND ISOLATION OF CE
X
Y3.
X
N@C2
N
(2N= 84-88) 37
2.3.3 SYNTHESIS AND ISOLATION OF CESC2N@C8O (II) 41
2.4 SYNTHESIS AND ISOLATION OF PR-BASED MMNCFS 44
2.5 CONCLUSION 48
CHAPTER 3 SPECTROSCOPIC CHARACTERIZATION OF MIXED METAL NITRIDE
CLUSTERFULLERENES... 49
3.1 UV-VIS-NIR SPECTROSCOPY OF MMNCFS 49
3.2 VIBRATIONAL SPECTROSCOPY OF MMNCFS 56
3.2.1 FTIR VIBRATIONAL SPECTROSCOPIC STUDY OF MMNCFS 56
3.2.2 RAMAN SPECTROSCOPIC STUDY OF MMNCFS 63
3.3 NMR SPECTROSCOPY OF LN-BASED MMNCFS 68
3.4 CONCLUSION 71
CHAPTER 4 MAGNETIC PROPERTIES OF MIXED METAL NITRIDE CLUSTERFULLERENES
72
4.1
13
C NMR SPECTROSCOPIC STUDY OF CEM
2
N@CG
0
72
HTTP://D-NB.INFO/1046474596
TABLE OF CONTENTS
4.2
45
SC NMR SPECTROSCOPIC STUDY OF MMNCFS 80
4.3 THE ANALYSIS OF NMR SPECTROSCOPY OF LNSC2N@CGO 87
4.4 CONCLUSION 91
CHAPTER 5 ELECTROCHEMICAL STUDY OF CE-BASED MIXED METAL NITRIDE
CLUSTERFULLERENES.. 92
5.1 ELECTROCHEMICAL STUDY OF CEY2N@CGO 93
5.2 ELECTROCHEMICAL STUDY OF CE
X
Y3_
X
N@C2
N
(2N= 84, 86, 88) 99
5.3 CONCLUSION 108
CONCLUSION OF THESIS 109
REFERENCE 112
ACKNOWLEDGEMENT 125
APPENDIX I: EXPERIMENTAL DETAILS 126
1. SYNTHESIS AND EXTRACTION 126
2. HPLC ISOLATION 126
3. SPECTROSCOPIC AND ELECTROCHEMICAL CHARACTERIZATIONS 127
CURRICULUM VITAE 128
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| any_adam_object | 1 |
| author | Zhang, Yang 1983- |
| author_GND | (DE-588)1046474316 |
| author_facet | Zhang, Yang 1983- |
| author_role | aut |
| author_sort | Zhang, Yang 1983- |
| author_variant | y z yz |
| building | Verbundindex |
| bvnumber | BV041584702 |
| ctrlnum | (OCoLC)869886235 (DE-599)DNB1046474596 |
| dewey-full | 546.681426 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 546 - Inorganic chemistry |
| dewey-raw | 546.681426 |
| dewey-search | 546.681426 |
| dewey-sort | 3546.681426 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| illustrated | Illustrated |
| indexdate | 2024-07-10T01:00:11Z |
| institution | BVB |
| language | English |
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| physical | XIII, 130 S. graph. Darst. 30 cm |
| publishDate | 2013 |
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| spelling | Zhang, Yang 1983- Verfasser (DE-588)1046474316 aut Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes von Yang Zhang 2013 XIII, 130 S. graph. Darst. 30 cm txt rdacontent n rdamedia nc rdacarrier Jena, Univ., Diss., 2013 (DE-588)4113937-9 Hochschulschrift gnd-content DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027029898&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Zhang, Yang 1983- Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes |
| subject_GND | (DE-588)4113937-9 |
| title | Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes |
| title_auth | Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes |
| title_exact_search | Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes |
| title_full | Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes von Yang Zhang |
| title_fullStr | Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes von Yang Zhang |
| title_full_unstemmed | Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes von Yang Zhang |
| title_short | Metal nitride cluster as a template to tune the electronic and magnetic properties of rare-earth metal containing endohedral fullerenes |
| title_sort | metal nitride cluster as a template to tune the electronic and magnetic properties of rare earth metal containing endohedral fullerenes |
| topic_facet | Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027029898&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT zhangyang metalnitrideclusterasatemplatetotunetheelectronicandmagneticpropertiesofrareearthmetalcontainingendohedralfullerenes |