Amphiphilic polymers in microemulsions: The influence on structure and formation kinetics
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Göttingen
Cuvillier Verl.
2013
|
| Ausgabe: | 1. Aufl. |
| Schlagworte: | |
| Online-Zugang: | Klappentext Inhaltsverzeichnis |
| Beschreibung: | 273 S. Ill., graph. Darst. |
| ISBN: | 9783954045587 |
Internformat
MARC
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| 020 | |a 9783954045587 |9 978-3-95404-558-7 | ||
| 035 | |a (OCoLC)873400131 | ||
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| 245 | 1 | 0 | |a Amphiphilic polymers in microemulsions |b The influence on structure and formation kinetics |c Helge F. M. Klemmer |
| 250 | |a 1. Aufl. | ||
| 264 | 1 | |a Göttingen |b Cuvillier Verl. |c 2013 | |
| 300 | |a 273 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |a Zugl.: Köln, Univ., Diss., 2013 | ||
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Datensatz im Suchindex
| _version_ | 1804151562368450560 |
|---|---|
| adam_text | Content
1
Introduction
.............................................................................................................1
1.1
Surfactant
Technology -
History and Application
...........................................................1
1.2
Objectives
........................................................................................................................5
2
Fundamentals
...........................................................................................................7
2.1
Microemulsions
...............................................................................................................7
2.1.1
Phase Behaviour of Binary Mixtures
................................................................................8
2.1.2
The Phase Prism
................................................................................................................9
2.1.3
Isoplethal Sections through the Phase Prism
..................................................................11
2.1.3.1
The
Γ(γ)-
Section
-
the so called Fish
taiľ -cut
.....................................................11
2.1.3.2
The Optimal State
..................................................................................................13
2.1.3.3
The
F(wa)-
Section
-
Oil-rich Microemulsions
......................................................15
2.1.4
Microstructure
and the Amphiphilic Film
.......................................................................18
2.1.4.1
The Amphiphilic Film
...........................................................................................18
2.1.4.2
Structural Evolution
...............................................................................................22
2.1.5
Amphiphilic Block Copolymers as Efficiency Booster
..................................................28
2.2
Neutron Scattering
.........................................................................................................31
2.2.1
General Aspects
..............................................................................................................31
2.2.2
Small Angle Neutron Scattering
.....................................................................................34
2.2.3
Raw Data Treatment
.......................................................................................................35
2.2.4
Scattering from Particles
.................................................................................................35
2.2.5
Scattering Models for Cylindrical
Microemulsion
Droplets
...........................................39
2.2.6
Scattering Model for Emulsion Droplets in the Presence of other Droplets
...................40
2.2.7
Structure Factors for
Microemulsion
Droplets
...............................................................42
2.2.8
Inhomogeneous Systems
.................................................................................................45
2.2.9
Debye Model
...................................................................................................................46
2.2.10
Ornstein-Zernicke Model
................................................................................................47
2.2.11
Teubner-Strey Model
......................................................................................................47
2.2.12
Porod
and Invariant
Porod
Analysis
...............................................................................49
2.3
Kinetics
..........................................................................................................................51
2.3.1
General Aspects
..............................................................................................................51
2.3.2
Stopped-Flow Measurements
..........................................................................................53
2.4
Experimental Methods
...................................................................................................56
2.4.1 Determination
of the Phase Boundaries of Microemulsions
..........................................56
2.4.2
Stopped-Flow Measurements
.........................................................................................58
2.4.3
Static and Time-Resolved Small Angle Neutron Scattering
..........................................60
2.4.4
Electric Conductivity Measurements
..............................................................................62
3
Polymeric Additives and their Influence on Phase Behaviour and Structure
Formation
................................................................................................................63
3.1
Theoretical Background and Synthesis of the Proposed Polymers
..............................64
3.2
Influence on the Lamellar Phase in Balanced Microemulsions
....................................67
3.2.1
An Average Technical Polymer
-
Tego
EBE 55x
...........................................................69
3.2.2
Model Polymer PBO4-PPO3-PEO4
...............................................................................73
3.2.3
Model Polymer PBO5-PEO5
..........................................................................................76
3.2.4
Model Polymer PBO5
-
PPO0.5
-
PEO5
........................................................................80
3.2.5
Model Polymer BO2-EO
................................................................................................84
3.2.6
Evaluation of the Trends Observed
................................................................................87
3.2.7
Systematic Small Angle Neutron Scattering Experiments
.............................................90
3.2.8
Summary
&
Discussion
................................................................................................109
3.3
Network Phase Transitions and the Closed Loop in Oil-Rich Microemulsions with
Diblock Copolymers
...................................................................................................115
3.3.1
Theoretical Background
................................................................................................115
3.3.2
The Closed Loop as a Function of Polymer Content
....................................................120
3.3.3
Network Transitions within Oil-rich Microemulsions as a Function of Polymer Content
131
3.3.4
Summary and Discussion
..............................................................................................138
4
Formation Kinetics of Oil-Rich Non-ionic Microemulsions
...........................139
4.1
Theoretical Background
..............................................................................................140
4.2
Setup and Calibration of the Stopped-Flow
................................................................144
4.3
Phase Behaviour of the Systems studied
....................................................................153
4.4
Mixing of Two Identical Microemulsions
..................................................................159
4.5
Mixing of Two Slightly Different Microemulsions
....................................................163
4.6
Mixing of an Unstructured Binary Mixture with Water
.............................................167
4.7
The Influence of Polymeric Additives
........................................................................175
4.7.1
Evaluation of Two Identical Microemulsions
..............................................................176
4.7.2 Microemulsion
Formation with
б
= 0.05
in Bulk Contrast
...........................................180
4.7.3 Microemulsion
Formation with
б
= 0.05
in Film Contrast
...........................................187
4.7.4 Microemulsion
Formation with
б
= 0.10
in Bulk Contrast
...........................................194
4.7.5 Microemulsion
Formation with
б
= 0.10
in Film Contrast
...........................................200
4.8
The Resulting Formation Mechanism
.........................................................................207
4.8.1
Polymer-free Formation Mechanism
............................................................................207
4.8.2
Polymer-containing Formation Mechanism
..................................................................210
5
Summary
..............................................................................................................213
6
Appendix
..............................................................................................................219
6.1
Abbreviations and Symbols
.........................................................................................219
6.2
Chemicals Used
...........................................................................................................231
6.3
End-to-End Distances of the Polymer Blocks and their Approximation
....................232
6.4
Derivation of the Relation between
УХ
and
¿/ţs^ts
......................................................234
6.5
Fit Parameters of the Bicontinuous Polymer Systems
................................................236
6.6
Data Analysis of the Aqueous Polymer Solution used in the Stopped-Flow
Experiments
................................................................................................................237
6.7
Time-resolved Small Angle Neutron Scattering Fit Parameters
.................................243
6.8
Literature
.....................................................................................................................251
CONTENT
1 INTRODUCTION 1
1.1 SURFACTANT TECHNOLOGY - HISTORY AND APPLICATION 1
1.2 OBJECTIVES 5
2 FUNDAMENTALS 7
2.1 MICROEMULSIONS 7
2.1.1 PHASE BEHAVIOUR OF BINARY MIXTURES 8
2.1.2 THE PHASE PRISM 9
2.1.3 ISOPLETHAL SECTIONS THROUGH THE PHASE PRISM 11
2.1.3.1 THE 71(Y)-SECTION
- THE SO CALLED FISH TAIL -CUT 11
2.1.3.2 THE OPTIMAL STATE 13
2.1.3.3 THE 7T
(M A
)-SECTION
- OIL-RICH MICROEMULSIONS 15
2.1.4 MICROSTRUCTURE AND THE AMPHIPHILIC FILM 18
2.1.4.1 THE AMPHIPHILIC FILM 18
2.1.4.2 STRUCTURAL EVOLUTION 22
2.1.5 AMPHIPHILIC BLOCK COPOLYMERS AS EFFICIENCY BOOSTER 28
2.2 NEUTRON SCATTERING 31
2.2.1 GENERAL ASPECTS 31
2.2.2 SMALL ANGLE NEUTRON SCATTERING 34
2.2.3 RAW DATA TREATMENT 35
2.2.4 SCATTERING FROM PARTICLES 35
2.2.5 SCATTERING MODELS FOR CYLINDRICAL MICROEMULSION DROPLETS 39
2.2.6 SCATTERING MODEL FOR EMULSION DROPLETS IN THE PRESENCE OF OTHER
DROPLETS 40
2.2.7 STRUCTURE FACTORS FOR MICROEMULSION DROPLETS 42
2.2.8 INHOMOGENEOUS SYSTEMS 45
2.2.9 DEBYE MODEL 46
2.2.10 ORNSTEIN-ZERNICKE MODEL 47
2.2.11 TEUBNER-STREY MODEL 47
2.2.12 POROD AND INVARIANT POROD ANALYSIS 49
2.3 KINETICS 51
2.3.1 GENERAL ASPECTS 51
2.3.2 STOPPED-FLOW MEASUREMENTS 53
2.4 EXPERIMENTAL METHODS 56
HTTP://D-NB.INFO/1044598409
2.4.1 DETERMINATION OF THE PHASE BOUNDARIES OF MICROEMULSIONS 56
2.4.2 STOPPED-FLOW MEASUREMENTS 58
2.4.3 STATIC AND TIME-RESOLVED SMALL ANGLE NEUTRON SCATTERING 60
2.4.4 ELECTRIC CONDUCTIVITY MEASUREMENTS 62
3 POLYMERIC ADDITIVES AND THEIR INFLUENCE ON PHASE BEHAVIOUR AND
STRUCTURE
FORMATION. 63
3.1 THEORETICAL BACKGROUND AND SYNTHESIS OF THE PROPOSED POLYMERS 64
3.2 INFLUENCE ON THE LAMELLAR PHASE IN BALANCED MICROEMULSIONS 67
3.2.1 AN AVERAGE TECHNICAL POLYMER - TEGO EBE 55X 69
3.2.2 MODEL POLYMER PB04-PP03-PE04 73
3.2.3 MODEL POLYMER PB05-PE05 76
3.2.4 MODEL POLYMER PB05 - PPOO.5 - PE05 80
3.2.5 MODEL POLYMER B02-E0 84
3.2.6 EVALUATION OF THE TRENDS OBSERVED 87
3.2.7 SYSTEMATIC SMALL ANGLE NEUTRON SCATTERING EXPERIMENTS 90
3.2.8 SUMMARY & DISCUSSION 109
3.3 NETWORK PHASE TRANSITIONS AND THE CLOSED LOOP IN OIL-RICH
MICROEMULSIONS WITH
DIBLOCK COPOLYMERS 115
3.3.1 THEORETICAL BACKGROUND 115
3.3.2 THE CLOSED LOOP AS A FUNCTION OF POLYMER CONTENT 120
3.3.3 NETWORK TRANSITIONS WITHIN OIL-RICH MICROEMULSIONS AS A FUNCTION
OF POLYMER CONTENTL31
3.3.4 SUMMARY AND DISCUSSION 138
4 FORMATION KINETICS OF OIL-RICH NON-IONIC MICROEMULSIONS 139
4.1 THEORETICAL BACKGROUND 140
4.2 SETUP AND CALIBRATION OF THE STOPPED-FLOW 144
4.3 PHASE BEHAVIOUR OF THE SYSTEMS STUDIED 153
4.4 MIXING OF TWO IDENTICAL MICROEMULSIONS 159
4.5 MIXING OF TWO SLIGHTLY DIFFERENT MICROEMULSIONS 163
4.6 MIXING OF AN UNSTRUCTURED BINARY MIXTURE WITH WATER 167
4.7 THE INFLUENCE OF POLYMERIC ADDITIVES 175
4.7.1 EVALUATION OF TWO IDENTICAL MICROEMULSIONS 176
4.7.2 MICROEMULSION FORMATION WITH 8 = 0.05 IN BULK CONTRAST 180
4.7.3 MICROEMULSION FORMATION WITH 8 = 0.05 IN FILM CONTRAST 187
4.7.4 MICROEMULSION FORMATION WITH 8 = 0.10 IN BULK CONTRAST 194
4.7.5 MICROEMULSION FORMATION WITH 8 = 0.10 IN FILM CONTRAST 200
4.8 THE RESULTING FORMATION MECHANISM 207
4.8.1 POLYMER-FREE FORMATION MECHANISM 207
4.8.2 POLYMER-CONTAINING FORMATION MECHANISM 210
5 SUMMARY 213
6 APPENDIX 219
6.1 ABBREVIATIONS AND SYMBOLS 219
6.2 CHEMICALS USED 231
6.3 END-TO-END DISTANCES OF THE POLYMER BLOCKS AND THEIR APPROXIMATION
232
6.4 DERIVATION OF THE RELATION BETWEEN F
A
AND ^
TS/4TS
234
6.5 FIT PARAMETERS OF THE BICONTINUOUS POLYMER SYSTEMS 236
6.6 DATA ANALYSIS OF THE AQUEOUS POLYMER SOLUTION USED IN THE
STOPPED-FLOW
EXPERIMENTS . . 237
6.7 TIME-RESOLVED SMALL ANGLE NEUTRON SCATTERING FIT PARAMETERS 243
6.8 LITERATURE 251
|
| any_adam_object | 1 |
| author | Klemmer, Helge F. M. 1984- |
| author_GND | (DE-588)1044734620 |
| author_facet | Klemmer, Helge F. M. 1984- |
| author_role | aut |
| author_sort | Klemmer, Helge F. M. 1984- |
| author_variant | h f m k hfm hfmk |
| building | Verbundindex |
| bvnumber | BV041442627 |
| classification_rvk | VK 8007 |
| ctrlnum | (OCoLC)873400131 (DE-599)BVBBV041442627 |
| discipline | Chemie / Pharmazie |
| edition | 1. Aufl. |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV041442627 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T00:56:47Z |
| institution | BVB |
| isbn | 9783954045587 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-026889359 |
| oclc_num | 873400131 |
| open_access_boolean | |
| owner | DE-703 |
| owner_facet | DE-703 |
| physical | 273 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Cuvillier Verl. |
| record_format | marc |
| spelling | Klemmer, Helge F. M. 1984- Verfasser (DE-588)1044734620 aut Amphiphilic polymers in microemulsions The influence on structure and formation kinetics Helge F. M. Klemmer 1. Aufl. Göttingen Cuvillier Verl. 2013 273 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Zugl.: Köln, Univ., Diss., 2013 Amphiphile Verbindungen (DE-588)4142278-8 gnd rswk-swf Mikroemulsion (DE-588)4169812-5 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Polymere (DE-588)4046699-1 s Amphiphile Verbindungen (DE-588)4142278-8 s Mikroemulsion (DE-588)4169812-5 s DE-604 Digitalisierung UB Bayreuth - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026889359&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Klappentext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026889359&sequence=000003&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Klemmer, Helge F. M. 1984- Amphiphilic polymers in microemulsions The influence on structure and formation kinetics Amphiphile Verbindungen (DE-588)4142278-8 gnd Mikroemulsion (DE-588)4169812-5 gnd Polymere (DE-588)4046699-1 gnd |
| subject_GND | (DE-588)4142278-8 (DE-588)4169812-5 (DE-588)4046699-1 (DE-588)4113937-9 |
| title | Amphiphilic polymers in microemulsions The influence on structure and formation kinetics |
| title_auth | Amphiphilic polymers in microemulsions The influence on structure and formation kinetics |
| title_exact_search | Amphiphilic polymers in microemulsions The influence on structure and formation kinetics |
| title_full | Amphiphilic polymers in microemulsions The influence on structure and formation kinetics Helge F. M. Klemmer |
| title_fullStr | Amphiphilic polymers in microemulsions The influence on structure and formation kinetics Helge F. M. Klemmer |
| title_full_unstemmed | Amphiphilic polymers in microemulsions The influence on structure and formation kinetics Helge F. M. Klemmer |
| title_short | Amphiphilic polymers in microemulsions |
| title_sort | amphiphilic polymers in microemulsions the influence on structure and formation kinetics |
| title_sub | The influence on structure and formation kinetics |
| topic | Amphiphile Verbindungen (DE-588)4142278-8 gnd Mikroemulsion (DE-588)4169812-5 gnd Polymere (DE-588)4046699-1 gnd |
| topic_facet | Amphiphile Verbindungen Mikroemulsion Polymere Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026889359&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026889359&sequence=000003&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT klemmerhelgefm amphiphilicpolymersinmicroemulsionstheinfluenceonstructureandformationkinetics |