Principles of polymer design and synthesis:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
Springer
2013
|
| Schriftenreihe: | Lecture Notes in Chemistry
82 |
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XIII, 306 S. Ill., graph. Darst. |
| ISBN: | 3642387292 9783642387296 |
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Datensatz im Suchindex
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| adam_text |
CONTENTS
1 INTRODUCTION 1
1.1 TYPES OF POLYMERS 3
1.2 TYPES OF POLYMERIZATION 3
1.3 NOMENCLATURE OF POLYMERS 4
1.4 POLYMER RECYCLING 7
1.5 PROBLEMS 7
REFERENCES 8
2 POLYMER SIZE AND POLYMER SOLUTIONS 9
2.1 THE MOLECULAR WEIGHT OF POLYMER 9
2.2 POLYMER SOLUTIONS 12
2.3 MEASUREMENT OF MOLECULAR WEIGHT 16
2.4 PROBLEMS 24
REFERENCES 25
3 STRUCTURE MORPHOLOGY FLOW OF POLYMER 27
3.1 CHEMICAL AND MOLECULAR STRUCTURE OF POLYMER 27
3.2 CRYSTAL STRUCTURE OF HOMOPOLYMER 31
3.3 CRYSTAL STRUCTURE OF COPOLYMER 33
3.4 LIQUID CRYSTALLINE POLYMER 37
3.5 CROSSLINKED POLYMER 43
3.6 POLYMER BLEND 44
3.7 POLYMER FLOW UNDER SHEAR FORCE 46
3.8 POLYMER FLOW UNDER THERMAL STRESS 52
3.9 PROBLEMS 56
REFERENCES 58
4 CHEMICAL AND PHYSICAL PROPERTIES OF POLYMERS 61
4.1 CHEMICAL PROPERTY OF POLYMER 61
4.2 MECHANICAL PROPERTY OF POLYMER 66
4.3 THERMAL PROPERTY OF POLYMER 68
4.4 ELECTRICAL PROPERTY OF POLYMER 72
HTTP://D-NB.INFO/103451461X
X
CONTENTS
4.5 OPTICAL PROPERTY OF POLYMER 76
4.6 PROCESSABILITY OF POLYMER 83
4.7 PROBLEMS 86
REFERENCES 87
5 CHARACTERIZATION OF POLYMER 89
5.1 INSTRUMENTS AND TESTING METHODS FOR POLYMER
CHARACTERIZATION 89
5.2 CHARACTERIZATION OF CHEMICAL STRUCTURES OF POLYMERS 90
5.2.1 CHEMICAL REACTION METHOD 90
5.2.2 INFRARED SPECTROSCOPY 90
5.2.3 RAMAN SPECTROSCOPY 92
5.2.4 UV-VISIBLE SPECTROSCOPY 93
5.2.5 NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY 95
5.2.6 ELECTRON SPIN RESONANCE 98
5.3 CHARACTERIZATION OF MORPHOLOGY AND PHYSICAL STRUCTURE
OF POLYMER 100
5.3.1 TRANSMISSION ELECTRON MICROSCOPY 100
5.3.2 X-RAY SCATTERING 102
5.3.3 ATOMIC FORCE MICROSCOPY 103
5.4 CHARACTERIZATION OF THERMAL PROPERTIES OF POLYMERS 104
5.4.1 DIFFERENTIAL THERMAL ANALYSIS AND DIFFERENTIAL
SCANNING CALORIMETRY 104
5.4.2 THERMOMECHANICAL ANALYSIS 106
5.4.3 THERMOGRAVIMETRIC ANALYSIS 107
5.4.4 FLAMMABILITY TEST 108
5.5 PROBLEMS 109
REFERENCES 110
6 STEP POLYMERIZATION ILL
6.1 CHEMICAL REACTIONS AND REACTION MECHANISMS
OF STEP POLYMERIZATION ILL
6.1.1 CARBONYL ADDITION: ELIMINATION
REACTION MECHANISM 113
6.1.2 CARBONYL ADDITION: SUBSTITUTION
REACTION MECHANISM 115
6.1.3 NUCLEOPHILIC SUBSTITUTION REACTION MECHANISM 116
6.1.4 DOUBLE-BOND ADDITION REACTION MECHANISM 116
6.1.5 FREE-RADICAL COUPLING 117
6.1.6 AROMATIC ELECTROPHILIC-SUBSTITUTION
REACTION MECHANISM 117
6.2 REACTION KINETICS OF STEP POLYMERIZATION 117
6.3 MOLECULAR WEIGHT CONTROL IN STEP POLYMERIZATION 119
6.4 MOLECULAR WEIGHT DISTRIBUTION 122
6.5 NETWORK FORMATION FROM STEP POLYMERIZATION 124
CONTENTS XI
6.6 STEP COPOLYMERIZATION 127
6.7 TECHNIQUES OF STEP POLYMERIZATION 129
6.8 SYNTHESIS OF DENDRITIC POLYMERS 130
6.8.1 DIVERGENT METHOD 130
6.8.2 CONVERGENT SYSTEM 131
6.8.3 MOLECULAR WEIGHT OF DENDRIMER 133
6.9 HYPERBRANCHED COPOLYMER 133
6.10 PROBLEMS 134
REFERENCES 135
7 RADICAL CHAIN POLYMERIZATION 137
7.1 EFFECT OF CHEMICAL STRUCTURE OF MONOMER
ON THE STRUCTURAL ARRANGEMENT OF POLYMER 138
7.2 INITIATORS OF RADICAL CHAIN POLYMERIZATION 142
7.2.1 THERMAL INITIATORS J42
7.2.2 DECOMPOSITION TEMPERATURE AND HALF-LIFE
OF THERMAL INITIATORS 144
7.2.3 INITIATION PROMOTERS 147
7.2.4 REDOX INITIATORS 147
7.2.5 PHOTOINITIATORS 148
7.2.6 ELECTROCHEMICAL INITIATION 149
7.3 TECHNIQUES OF FREE RADICAL CHAIN POLYMERIZATION 150
7.3.1 BULK POLYMERIZATION 150
7.3.2 SUSPENSION POLYMERIZATION 150
7.3.3 SOLUTION POLYMERIZATION 151
7.3.4 EMULSION POLYMERIZATION 151
7.4 REACTION MECHANISM OF FREE RADICAL CHAIN
POLYMERIZATION 153
7.5 KINETICS OF FREE RADICAL CHAIN POLYMERIZATION 155
7.5.1 RATE OF POLYMERIZATION 156
7.5.2 AVERAGE KINETIC CHAIN LENGTH V 157
7.5.3 CHAIN TRANSFER REACTIONS 158
7.6 LIVING POLYMERIZATION 162
7.6.1 LIVING RADICAL POLYMERIZATION 162
7.6.2 ATOM TRANSFER RADICAL POLYMERIZATION 163
7.6.3 NITROXIDE-MEDIATED POLYMERIZATION 164
7.6.4 RADICAL ADDITION-FRAGMENTATION TRANSFER 164
7.7 POLYMERIZATION OF DIENES 165
7.8 TEMPERATURE EFFECT OF THE FREE RADICAL POLYMERIZATION 168
7.8.1 ACTIVATION ENERGY AND FREQUENCY FACTOR 169
7.8.2 RATE OF POLYMERIZATION 170
7.8.3 DEGREE OF POLYMERIZATION 171
XII CONTENTS
7.9 THERMODYNAMICS OF FREE RADICAL POLYMERIZATION 172
7.9.1 MONOMER REACTIVITY 173
7.9.2 CEILING TEMPERATURE 175
7.9.3 CHARACTERISTICS OF AS VALUES OF FREE RADICAL
POLYMERIZATION 176
7.10 MOLECULAR WEIGHT DISTRIBUTION AT LOW CONVERSION 176
7.11 SYNTHESIS OF COMMERCIAL POLYMERS 178
7.11.1 POLYETHYLENE 178
7.11.2 POLYSTYRENE 179
7.11.3 POLYVINYL CHLORIDE 180
7.11.4 POLYVINYL ACETATE 180
7.11.5 POLYVINYLIDENE CHLORIDE 180
7.11.6 ACRYL POLYMER 180
7.11.7 FLUOROPOLYMERS 181
7.11.8 COST OF COMMON POLYMERS 182
7.12 PROBLEMS 182
REFERENCES 183
8 IONIC CHAIN POLYMERIZATION 185
8.1 CHARACTERISTICS OF IONIC CHAIN POLYMERIZATION 187
8.2 CATIONIC POLYMERIZATION 189
8.2.1 INITIATORS OF CATIONIC POLYMERIZATION 189
8.2.2 REACTION MECHANISMS OF CATIONIC POLYMERIZATION . 190
8.2.3 KINETICS OF CATIONIC POLYMERIZATION 196
8.2.4 COMMERCIAL CATIONIC POLYMERIZATION 200
8.3 ANIONIC POLYMERIZATION 201
8.3.1 REACTION MECHANISMS OF ANIONIC POLYMERIZATION. . . . 201
8.3.2 KINETICS OF ANIONIC POLYMERIZATION
WITH TERMINATION 204
8.4 GROUP TRANSFER POLYMERIZATION 209
8.5 CHAIN POLYMERIZATION OF CARBONYL MONOMER 213
8.5.1 ANIONIC POLYMERIZATION OF CARBONYL MONOMER 213
8.5.2 CATIONIC POLYMERIZATION OF CARBONYL MONOMER 215
8.5.3 RADICAL POLYMERIZATION OF CARBONYL MONOMER 215
8.5.4 END-CAPPING POLYMERIZATION 216
8.6 PROBLEMS 217
REFERENCES 218
9 COORDINATION POLYMERIZATION 219
9.1 HETEROGENEOUS ZIEGLER-NATTA POLYMERIZATION 219
9.1.1 CATALYSTS 219
9.1.2 REACTION MECHANISMS 222
9.2 HOMOGENEOUS ZIEGLER-NATTA POLYMERIZATION 225
9.3 ZIEGLER-NATTA COPOLYMERIZATION 229
CONTENTS XIII
9.4 METATHESIS POLYMERIZATION 230
9.5 PROBLEMS 231
REFERENCES 232
10 CHAIN COPOLYMERIZATION 233
10.1 REACTION KINETICS OF FREE RADICAL COPOLYMERIZATION 234
10.1.1 TYPES OF COPOLYMERIZATION BEHAVIOR 237
10.1.2 EFFECT OF REACTION CONDITIONS ON RADICAL
COPOLYMERIZATION 241
10.1.3 REACTIVITY AND COMPOSITION
OF FREE RADICAL COPOLYMERIZATION 243
10.1.4 RATE OF POLYMERIZATION OF FREE RADICAL
COPOLYMERIZATION 253
10.2 CATIONIC COPOLYMERIZATION 256
10.3 ANIONIC COPOLYMERIZATION 259
10.4 COPOLYMERIZATION INVOLVING DIENES 260
10.5 BLOCK COPOLYMERS 261
10.6 COMMERCIAL COPOLYMERS 263
10.7 PROBLEMS 263
REFERENCES 265
11 RING-OPENING POLYMERIZATION 267
11.1 REACTIVITY OF CYCLIC MONOMERS 267
11.2 GENERAL ASPECTS OF MECHANISMS AND KINETICS 270
11.3 CYCLIC ETHERS 271
11.3.1 ANIONIC POLYMERIZATION OF EPOXIDES 272
11.3.2 CATIONIC POLYMERIZATION OF EPOXIDES 277
11.3.3 POLYMERIZATION OF CYCLIC ACETALS 282
11.3.4 KINETIC CHARACTERISTICS 283
11.3.5 THERMODYNAMIC CHARACTERISTICS 285
11.3.6 COMMERCIAL APPLICATIONS OF POLYMERS
OF CYCLIC ETHER 287
11.4 LACTAMS 288
11.4.1 CATIONIC POLYMERIZATION 288
11.4.2 HYDROLYTIC POLYMERIZATION 290
11.4.3 ANIONIC POLYMERIZATION 291
11.4.4 REACTIVITY OF LACTAM 294
11.5 CYCLOSILOXANES 294
11.6 COPOLYMERIZATION 296
11.7 PROBLEMS 298
REFERENCES 299
INDEX 301 |
| any_adam_object | 1 |
| author | Su, Wei-Fang |
| author_GND | (DE-588)1044994754 |
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| discipline | Chemie / Pharmazie Chemie Werkstoffwissenschaften / Fertigungstechnik |
| format | Book |
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| illustrated | Illustrated |
| indexdate | 2024-09-10T01:02:25Z |
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| isbn | 3642387292 9783642387296 |
| language | English |
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| physical | XIII, 306 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Springer |
| record_format | marc |
| series | Lecture Notes in Chemistry |
| series2 | Lecture Notes in Chemistry |
| spelling | Su, Wei-Fang Verfasser (DE-588)1044994754 aut Principles of polymer design and synthesis Wei-Fang Su Berlin [u.a.] Springer 2013 XIII, 306 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Lecture Notes in Chemistry 82 Chemie Chemistry Polymers Industrial engineering Surfaces (Physics) Polymere (DE-588)4046699-1 gnd rswk-swf Polymerisation (DE-588)4046704-1 gnd rswk-swf Polymere (DE-588)4046699-1 s DE-604 Polymerisation (DE-588)4046704-1 s Erscheint auch als Online-Ausgabe 978-3-642-38730-2 Lecture Notes in Chemistry 82 (DE-604)BV000000216 82 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4327672&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026840940&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Su, Wei-Fang Principles of polymer design and synthesis Lecture Notes in Chemistry Chemie Chemistry Polymers Industrial engineering Surfaces (Physics) Polymere (DE-588)4046699-1 gnd Polymerisation (DE-588)4046704-1 gnd |
| subject_GND | (DE-588)4046699-1 (DE-588)4046704-1 |
| title | Principles of polymer design and synthesis |
| title_auth | Principles of polymer design and synthesis |
| title_exact_search | Principles of polymer design and synthesis |
| title_full | Principles of polymer design and synthesis Wei-Fang Su |
| title_fullStr | Principles of polymer design and synthesis Wei-Fang Su |
| title_full_unstemmed | Principles of polymer design and synthesis Wei-Fang Su |
| title_short | Principles of polymer design and synthesis |
| title_sort | principles of polymer design and synthesis |
| topic | Chemie Chemistry Polymers Industrial engineering Surfaces (Physics) Polymere (DE-588)4046699-1 gnd Polymerisation (DE-588)4046704-1 gnd |
| topic_facet | Chemie Chemistry Polymers Industrial engineering Surfaces (Physics) Polymere Polymerisation |
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