NMR spectroscopic studies of organocopper compounds and Zintl anions:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
2012
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| Schlagworte: | |
| Online-Zugang: | Volltext https://nbn-resolving.org/urn:nbn:de:bvb:355-epub-264633 Inhaltsverzeichnis |
| Beschreibung: | 120 S. Ill., graph. Darst. |
Internformat
MARC
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| 245 | 1 | 0 | |a NMR spectroscopic studies of organocopper compounds and Zintl anions |c vorgelegt von Maria Neumeier |
| 264 | 1 | |c 2012 | |
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Datensatz im Suchindex
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| adam_text | TABLE OF CONTENTS
TABLE OF CONTENTS
1. INTRODUCTION AND OUTLINE 1
1.1 ORGANOCUPRATES AND THEIR INTERMEDIATES IN CROSS COUPLING REACTIONS 1
1.2 THE CHEMISTRY OF ZINTL ANIONS IN LIQUID AMMONIA 2
2. LIGAND EXCHANGE REACTIONS IN CU(ILL) COMPLEXES: MECHANISTIC INSIGHTS
BY
COMBINED NMR AND DFT STUDIES 5
2.1 ABSTRACT 6
2.2 DISCUSSION 6
2.3 REFERENCES 10
2.4 SUPPORTING INFORMATION 11
2.4.1. EXPERIMENTAL SECTION. II
2.4.2. NMR DATA COLLECTING AND PROCESSING 11
2.4.3. INCREASED FOIMATION OFME CU APPLYING AN EXCESS OF MELI 12
2.4.4. ANALYSIS OF THE ISOTOPIC PATTERN OF ETHANE IN THE REACTION OF
C-LABELED CYANOCUPRATE
CONVENED WITH MEL AND AN EXCESS OF C-LABELED MELI 13
2.4.5. DFT FUNCTIONAL CALCULATIONS 14
2.4.6. ENERGIES AND CARTESIANS COORDINATES OF STATIONARY POINTS 14
2.4.7. ATTEMPTED STUDY OF INTRAMOLECULAR ISOMERIZATION OF
ORGANOCOPPER(LLL) COMPLEX 18
3. NMR SPECTROSCOPIC INVESTIGATIONS ON ORGANOCOPPER(L) COMPLEXES AND
THEIR
REACTIVITY IN CROSS COUPLING REACTIONS WITH ALKYL HALIDES 21
3.1 ABSTRACT 22
3.2 INTRODUCTION 22
3 J RESULTS AND DISCUSSION .28
3.3.1. MODEL SYSTEM 28
3.3.2. FORMATION OF LODOCOPPCR(L) COMPLEXES IN DIETHYL ETHER 29
3.3.3. STRUCTURES OF LODOCOPPER L) COMPLEXES IN DIETHYL ETHER 31
3.3.4. FORMATION AND STRUCTURES OF CYANOCOPPERTH COMPLEXES IN DIETHYL
ETHER 35
1
HTTP://D-NB.INFO/104418664X
TABLE OF CONTENTS
3.3.5. REACTIVITY OF LODO- AND CYANOCOPPER L) COMPLEXES IN CROSS
COUPLING REACTIONS WITH METHYL
IODIDE 36
3.4 CONCLUSIONS
;
39
3.5 EXPERIMENTAL SECTION 40
3.5.1. SAMPLE PREPARATION 40
3.5.2. NMR DATA COLLECTING AND PROCESSING 40
3.5.3. DETERMINATION OF DIFLIISION COEFFICIENTS 41
3.5.4. INTERNAL VISCOSITY REFERENCE 41
3.5.5. INTEGRAL ANALYSIS OF THE REACTIONS BETWEEN 3A*LIX (X * I.
I5
CN) AND 4A 41
3.6 REFERENCES 42
3.7 SUPPORTING INFORMATION 44
3.7.1. NMR DATA FOR STARTING MATERIALS, COMPLEXES AND PRODUCTS 46
3.7.2. APPROPRIATE TEMPERATURE FOR NMR INVESTIGATIONS ON COMPLEXES 3A-F
47
3.7.3. SIGNAL ASSIGNEMENT FOR THE COMPLEXES 3A*LII-3E 47
3.7.4. INTEGRAL ANALYSIS OF THE H NMR DATA OF COMPLEXES 3A*LII-3E 50
3.7.5. ELUCIDATION OF THE MONOMERIC STRUCTURE 3C 51
3.7.6. CALCULATION OF THEORETICAL DIFFUSION COEFFICIENTS 52
3.7.7. SIGNAL ASSIGNMENT FOR THE COMPLEXES 3A
1
LI
L,
CN AND 3F 52
3.7.8. STRUCTURE ELUCIDATION OF3A*LI CN AND 3F 54
3.7.9. ADDITIONAL NMR SPECTRA 55
3.7. LO.REFERENCES 57
4. THE ELUSIVE HIGHLY CHARGED ZINTL ANIONS: NMR DETECTION OF SI/
-
AND IN
LIQUID AMMONIA 59
4.1 ABSTRACT 60
4.2 INTRODUCTION .60
4 J RESULTS AND DISCUSSION 62
4.4 CONCLUSIONS 66
4.5 REFERENCES 66
4.6 SUPPORTING INFORMATION 68
II
TABLE OF CONTENTS
4.6.1. SYNTHESIS 68
4.6.2. PHASE DETERMINATION 69
4.6.3. NMR INVESTIGATIONS IN SOLUTION 1I
5.
,L9
SN NMR INVESTIGATIONS ON THE SOLUTION CHEMISTRY OF POLYSTANNIDES IN
LIQUID
AMMONIA: ON THE WAY TO A TARGETED MATERIAL RESEARCH 77
5.1 ABSTRACT 78
5.2 INTRODUCTION 78
5 J THE CHEMISTRY OF PURE POIYSTANNIDE SOLUTIONS 81
5.3.1. ADDITIVE-FREE SOLUTIONS: DIRECT REDUCTION 81
5.3.2. ADDITIVE-CONTAINING SOLUTIONS 83
5.4 CONVERSIONS OF POLYSTANNIDES WITH MESITYLCOPPER 88
5.5 CONCLUSIONS
5.6 REFERENCES
5.7 SUPPORTING INFORMATION 94
5.7.1. SYNTHESIS
:
. 94
5.7.2. PHASE DETERMINATION . 5
5.7.3. NMR INVESTIGATIONS IN SOLUTION 97
5.8 ADDITIONAL FINDINGS 98
6. A NEW LIGHT AND X-RAY STABLE AS SOURCE - THE
75
AS NMR SPECTROSCOPIC EVIDENCE
FOR REVERSIBLE AS4 BINDING 101
6.1 ABSTRACT 102
6.2 INTRODUCTION 102
6 J RESULTS AND DISCUSSION 103
6.4 CONCLUSIONS 107
6.5 REFERENCES 08
6.6 SUPPORTING INFORMATION 109
6.6.1. GENERAL CONSIDERATIONS 109
6.6.2. EXPERIMENTAL DETAILS 109
III
TABLE OF CONTENTS
6.6.3. ESI MASS SPECTROMETRY 110
6.6.4. NMR DATA COLLECTING AND PROCESSING 110
6.6.5. PRACTICAL CONSIDERATIONS FOR
75
AS NMR 110
6.6.6. X-RAY STRUCTURE ANALYSIS 111
7. SUMMARY 113
8. ZUSAMMENFASSUNG 117
IV
|
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| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| spelling | Neumeier, Maria Verfasser aut NMR spectroscopic studies of organocopper compounds and Zintl anions vorgelegt von Maria Neumeier 2012 120 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Regensburg, Univ., Diss., 2012 Zintl-Anion (DE-588)4210427-0 gnd rswk-swf Siliciumion (DE-588)4365618-3 gnd rswk-swf Zinnion (DE-588)4782235-1 gnd rswk-swf Kupferorganische Verbindungen (DE-588)4166139-4 gnd rswk-swf Ammoniak (DE-588)4001735-7 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Kupferorganische Verbindungen (DE-588)4166139-4 s NMR-Spektroskopie (DE-588)4075421-2 s DE-604 Zintl-Anion (DE-588)4210427-0 s Siliciumion (DE-588)4365618-3 s Zinnion (DE-588)4782235-1 s Ammoniak (DE-588)4001735-7 s Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:355-epub-264633 http://epub.uni-regensburg.de/26463/ Verlag kostenfrei Volltext https://nbn-resolving.org/urn:nbn:de:bvb:355-epub-264633 Resolving-System DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026815195&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Neumeier, Maria NMR spectroscopic studies of organocopper compounds and Zintl anions Zintl-Anion (DE-588)4210427-0 gnd Siliciumion (DE-588)4365618-3 gnd Zinnion (DE-588)4782235-1 gnd Kupferorganische Verbindungen (DE-588)4166139-4 gnd Ammoniak (DE-588)4001735-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd |
| subject_GND | (DE-588)4210427-0 (DE-588)4365618-3 (DE-588)4782235-1 (DE-588)4166139-4 (DE-588)4001735-7 (DE-588)4075421-2 (DE-588)4113937-9 |
| title | NMR spectroscopic studies of organocopper compounds and Zintl anions |
| title_auth | NMR spectroscopic studies of organocopper compounds and Zintl anions |
| title_exact_search | NMR spectroscopic studies of organocopper compounds and Zintl anions |
| title_full | NMR spectroscopic studies of organocopper compounds and Zintl anions vorgelegt von Maria Neumeier |
| title_fullStr | NMR spectroscopic studies of organocopper compounds and Zintl anions vorgelegt von Maria Neumeier |
| title_full_unstemmed | NMR spectroscopic studies of organocopper compounds and Zintl anions vorgelegt von Maria Neumeier |
| title_short | NMR spectroscopic studies of organocopper compounds and Zintl anions |
| title_sort | nmr spectroscopic studies of organocopper compounds and zintl anions |
| topic | Zintl-Anion (DE-588)4210427-0 gnd Siliciumion (DE-588)4365618-3 gnd Zinnion (DE-588)4782235-1 gnd Kupferorganische Verbindungen (DE-588)4166139-4 gnd Ammoniak (DE-588)4001735-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd |
| topic_facet | Zintl-Anion Siliciumion Zinnion Kupferorganische Verbindungen Ammoniak NMR-Spektroskopie Hochschulschrift |
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