Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Aachen
Shaker
2013
|
| Schriftenreihe: | Berichte aus der Materialwissenschaft
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 140 S. Ill., graph. Darst. |
| ISBN: | 9783844021721 |
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Datensatz im Suchindex
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| adam_text | TABLE OF CONTENTS I
TABLE OF CONTENTS
1. INTRODUCTION 1
1.1. RESEARCH BACKGROUND 1
1.2. AIM OF THE WORK 2
2. LITERATURE REVIEW 4
2.1. FUNCTIONALLY GRADED MATERIALS 4
2.1.1. MICROSTRUCTURAL CONCEPTS 4
2.1.1.1. FGMS WITH DISPERSED SECOND PHASE 4
2.1.1.2. FGMS WITH AN INTERPENETRATING NETWORK OF SECOND PHASE 5
2.1.2. PROCESSING METHODS 6
2.1.2.1. GASEOUS PROCESSES 7
2.1.2.2. LIQUID PROCESSES 8
2.1.2.3. SOLID PROCESSES 12
2.1.3. POWDER METALLURGICAL PROCESSING 13
2.1.3.1. POWDER MIXTURE PREPARATION 13
2.1.3.2. STEPWISE GRADATION 14
2.1.3.3. CONTINUOUS GRADATION 15
2.1.3.4. CIP COMPACTION 16
2.1.3.5. PRESSURELESS CONSOLIDATION 16
2.1.3.6. PRESSURE CONSOLIDATION 17
2.1.4. SHRINKAGE AND SHRINKAGE MATCHING 18
2.1.4.1. SHRINKAGE BEHAVIOR 18
2.1.4.2. SHRINKAGE MATCHING 20
2.2. HIGH-MELTING METAL FOAMS 21
2.2.1. PROCESSING METHODS 21
2.2.1.1. COATING 22
2.2.1.2. CASTING 23
2.2.1.3. POWDER METALLURGICAL PROCESSING 24
2.2.2. PYROLYSIS OF POLYURETHANE 26
2.2.2.1. PYROLYSIS BY CONVENTIONAL HEATING 26
2.2.2.2. MICROWAVE HYBRID HEATING 27
2.3. STARTING MATERIALS 28
2.3.1. ZR0
2
28
2.3.1.1. PHASE AND PHASE TRANSFORMATION 28
HTTP://D-NB.INFO/1038072611
II TABLE OF CONTENTS
2.3.1.2. YTTRIA STABILIZED ZIRCONIA 29
2.3.2. ZRSI0
4
31
2.3.2.1. THERMAL STABILITY 31
2.3.2.2. PROPERTIES AND APPLICATIONS 32
2.3.3. NICR8020 33
3. EXPERIMENTAL 34
3.1. STARTING MATERIALS 34
3.2. ZR0
2
-ZRSI(VNICR FGMS 35
3.2.1. PREPARATION OF SAMPLES FOR SHRINKAGE MATCHING 36
3.2.2. PREPARATION OFFGM SAMPLES 36
3.3. NICR FOAM INTEGRATED ZR0
2
-ZRSI0
4
/NICR FGMS 38
3.3.1. PREPARATION OF NICR FOAMS 38
3.3.1.1. POLYURETHANE FOAMS 39
3.3.1.2. DIP-COATING 40
3.3.1.3. PYROLYSIS AND PRE-SINTERING 40
3.3.2. PREPARATION OF SAMPLES FOR SHRINKAGE MATCHING 42
3.3.3. PREPARATION OFFGM SAMPLES 43
3.4. CHARACTERIZATION 43
3.4.1. STRUCTURAL INVESTIGATION AND ELEMENTARY ANALYSIS 43
3.4.2. PARTICLE SIZE DISTRIBUTION 44
3.4.3. DENSITY AND POROSITY 44
3.4.4. BENDING TEST 44
3.4.5. COMPRESSIVE TEST 45
3.4.6. THERMAL EXPANSION 46
3.4.7. THERMAL CONDUCTIVITY 47
3.4.7.1. THERMAL CONDUCTIVITY OF ZR02-ZRSIC 4/NICR FGMS 47
3.4.7.2. THERMAL CONDUCTIVITY OF NICR FOAMS 48
3.4.8. HIGH-TEMPERATURE OXIDATION 48
4. RESULTS 50
4.1. ZROJ-ZRSIOVNICR FGMS ! 50
4.1.1. SELECTION OF BASIC POWDERS 50
4.1.2. PROCESSING OFFGM WITH THE BASIC POWDERS 51
4.1.3. SHRINKAGE MATCHING PROCESS 55
4.1.4. MICROSTRUCTURE OF THE CONSTITUENT PHASES 61
4.2. NICR FOAM INTEGRATED ZROJ-ZRSIC^/NICR FGMS 62
TABLE OF CONTENTS III
4.2.1. PRE-SINTERED NICR FOAMS 62
4.2.1.1. MACRO- AND MICROSTRUCTURE 62
4.2.1.2. ELEMENTARY ANALYSIS OF CARBON 65
4.2.2. SHRINKAGE MATCHING PROCESS 66
4.2.3. SATURATION OF FOAM STRUTS WITH WATER 67
4.2.4. MACRO- AND MICROSTRUCTURE OF FGM 68
4.3. CHARACTERIZATION 70
4.3.1. PARTICLE SIZE DISTRIBUTION 70
4.3.2. DENSITY AND POROSITY 72
4.3.2.1. DENSITY OF ZR0
2
-ZRSI0
4
/NICR FGMS 72
4.3.2.2. DENSITY OF NICR FOAMS 72
4.3.3. BENDING STRENGTH AND YOUNG S MODULUS 73
4.3.3.1. RELATIVE DENSITY OF PREPARED SAMPLES 73
4.3.3.2. LOAD-DEFLECTION CURVES 73
4.3.3.3. FRACTOGRAPH 75
4.3.3.4. BENDING STRENGTH AND YOUNG S MODULUS 76
4.3.4. COMPRESSIVE STRENGTH AND YOUNG S MODULUS 78
4.3.4.1. MICROSTRUCTURE OF PREPARED SAMPLES 78
4.3.4.2. COMPRESSIVE STRENGTH AND YOUNG S MODULUS 78
4.3.5. THERMAL EXPANSION 81
4.3.5.1. THERMAL EXPANSION OF ZR0
2
-ZRSI0
4
/NICR FGMS 81
4.3.5.2. THERMAL EXPANSION OF NICR FOAMS 83
4.3.6. THERMAL CONDUCTIVITY 83
4.3.6.1. THERMAL CONDUCTIVITY OF ZR02-ZRSI0
4
/NICR FGMS 83
4.3.6.2. THERMAL CONDUCTIVITY OF NICR FOAMS 85
4.3.7. HIGH-TEMPERATURE OXIDATION 86
4.3.7.1. SAMPLES PRIOR TO OXIDATION 86
4.3.7.2. OXIDATION KINETICS 87
4.3.7.3. MICROSTRUCTURE OF OXIDIZED SAMPLES 89
5. DISCUSSION 94
5.1. ZR0
2
-ZRSI0
4
/NICR FGMS 94
5.1.1. EVALUATION OF THE PROCESSING METHOD 94
5.1.1.1. SHRINKAGE MATCHING PROCESS 94
5.1.1.2. FGMS BEFORE AND AFTER SHRINKAGE MATCHING 95
5.1.2. MECHANICAL PROPERTIES 97
5.1.2.1. SAMPLES PREPARED FOR BENDING TEST 97
IV
TABLE OF CONTENTS
5.1.2.2. INFLUENCE OF MICROSTRUCTURE ON DUCTILITY 98
5.1.2.3. INFLUENCE OF MICROSTRUCTURE ON BENDING STRENGTH 98
5.1.2.4. INFLUENCE OF MICROSTRUCTURE ON YOUNG S MODULUS 100
5.1.3. THERMAL PROPERTIES 101
5.1.3.1. INFLUENCE OF MICROSTRUCTURE ON THERMAL EXPANSION 101
5.1.3.2. INFLUENCE OF MICROSTRUCTURE ON THERMAL CONDUCTIVITY 103
5.1.4. HIGH-TEMPERATURE OXIDATION BEHAVIOR 105
5.2. NICR FOAM INTEGRATED ZR0
2
-ZRSI0
4
/NICR FGMS 107
5.2.1. EVALUATION OF THE PROCESSING METHOD OFNICR FOAMS 107
5.2.1.1. PROCESSING TIME 107
5.2.1.2. STABILITY OF MICROWAVE HYBRID HEATING 107
5.2.1.3. RESIDUAL CARBON CONTENT 108
5.2.2. MECHANICAL PROPERTIES OFNICR FOAMS 109
5.2.2.1. SAMPLES PREPARED FOR COMPRESSIVE TEST 109
5.2.2.2. COMPRESSIVE BEHAVIOR 109
5.2.2.3. INFLUENCE OF POROSITY ON COMPRESSIVE STRENGTH 109
5.2.2.4. INFLUENCE OF POROSITY ON YOUNG S MODULUS 110
5.2.3. THERMAL PROPERTIES OFNICR FOAMS 110
5.2.4. EVALUATION OF THE PROCESSING METHOD OF FGMS 111
6. SUMMARY AND OUTLOOK 113
6.1. SUMMARY 113
6.1.1. ZR0
2
-ZRSI0
4
/NICR FGMS 113
6.1.2. NICR FOAM INTEGRATED ZR0
2
-ZRSI0
4
/NICR FGMS 115
6.2. OUTLOOK 116
7. ZUSAMMENFASSUNG UND AUSBLICK 117
7.1. ZUSAMMENFASSUNG 117
7.1.1. ZR0
2
-ZRSI0
4
/NICR GRADIENTENWERKSTOFFE 117
7.1.2. NICR-SCHAUM INTEGRIERTE ZR0
2
-ZRSI0
4
/NICR GRADIENTENWERKSTOFFE 119
7.2. AUSBLICK 121
8. APPENDIX 122
8.1. LIST OF EQUIPMENTS 122
8.2. SYMBOLS 122
8.3. ABBREVIATIONS 124
8.4. LIST OF PUBLICATIONS 124
8.5. CURRICULUM VITAE 125
TABLE OF CONTENTS V
9. REFERENCES 127
|
| any_adam_object | 1 |
| author | Wu, Kangjian |
| author_facet | Wu, Kangjian |
| author_role | aut |
| author_sort | Wu, Kangjian |
| author_variant | k w kw |
| building | Verbundindex |
| bvnumber | BV041286998 |
| classification_rvk | UQ 8500 |
| ctrlnum | (OCoLC)859421946 (DE-599)DNB1038072611 |
| dewey-full | 666.042 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 666 - Ceramic & allied technologies |
| dewey-raw | 666.042 |
| dewey-search | 666.042 |
| dewey-sort | 3666.042 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie Physik |
| format | Thesis Book |
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| id | DE-604.BV041286998 |
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| indexdate | 2024-07-10T00:53:25Z |
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| isbn | 9783844021721 |
| language | English |
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| record_format | marc |
| series2 | Berichte aus der Materialwissenschaft |
| spelling | Wu, Kangjian Verfasser aut Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials vorgelegt von Kangjian Wu Aachen Shaker 2013 140 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Berichte aus der Materialwissenschaft Zugl.: Bayreuth, Univ., Diss., 2013 Funktioneller Gradientenwerkstoff (DE-588)4495404-9 gnd rswk-swf Herstellung (DE-588)4159653-5 gnd rswk-swf Verarbeitungseigenschaft (DE-588)4372382-2 gnd rswk-swf Schrumpfen (DE-588)4180019-9 gnd rswk-swf Druckloses Sintern (DE-588)4586652-1 gnd rswk-swf Keramik-Metall-Verbund (DE-588)4225894-7 gnd rswk-swf Oxidation (DE-588)4137187-2 gnd rswk-swf Thermomechanische Eigenschaft (DE-588)4194417-3 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Keramik-Metall-Verbund (DE-588)4225894-7 s Funktioneller Gradientenwerkstoff (DE-588)4495404-9 s Herstellung (DE-588)4159653-5 s Druckloses Sintern (DE-588)4586652-1 s Schrumpfen (DE-588)4180019-9 s Verarbeitungseigenschaft (DE-588)4372382-2 s Thermomechanische Eigenschaft (DE-588)4194417-3 s Oxidation (DE-588)4137187-2 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026736060&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Wu, Kangjian Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials Funktioneller Gradientenwerkstoff (DE-588)4495404-9 gnd Herstellung (DE-588)4159653-5 gnd Verarbeitungseigenschaft (DE-588)4372382-2 gnd Schrumpfen (DE-588)4180019-9 gnd Druckloses Sintern (DE-588)4586652-1 gnd Keramik-Metall-Verbund (DE-588)4225894-7 gnd Oxidation (DE-588)4137187-2 gnd Thermomechanische Eigenschaft (DE-588)4194417-3 gnd |
| subject_GND | (DE-588)4495404-9 (DE-588)4159653-5 (DE-588)4372382-2 (DE-588)4180019-9 (DE-588)4586652-1 (DE-588)4225894-7 (DE-588)4137187-2 (DE-588)4194417-3 (DE-588)4113937-9 |
| title | Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials |
| title_auth | Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials |
| title_exact_search | Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials |
| title_full | Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials vorgelegt von Kangjian Wu |
| title_fullStr | Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials vorgelegt von Kangjian Wu |
| title_full_unstemmed | Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials vorgelegt von Kangjian Wu |
| title_short | Process development for ZrO 2 -ZrSiO 4 /NiCr functionally graded materials |
| title_sort | process development for zro 2 zrsio 4 nicr functionally graded materials |
| topic | Funktioneller Gradientenwerkstoff (DE-588)4495404-9 gnd Herstellung (DE-588)4159653-5 gnd Verarbeitungseigenschaft (DE-588)4372382-2 gnd Schrumpfen (DE-588)4180019-9 gnd Druckloses Sintern (DE-588)4586652-1 gnd Keramik-Metall-Verbund (DE-588)4225894-7 gnd Oxidation (DE-588)4137187-2 gnd Thermomechanische Eigenschaft (DE-588)4194417-3 gnd |
| topic_facet | Funktioneller Gradientenwerkstoff Herstellung Verarbeitungseigenschaft Schrumpfen Druckloses Sintern Keramik-Metall-Verbund Oxidation Thermomechanische Eigenschaft Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026736060&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT wukangjian processdevelopmentforzro2zrsio4nicrfunctionallygradedmaterials |