Practical raman spectroscopy: an introduction
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Chichester
Wiley
2013
|
| Ausgabe: | 1. publ. |
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XXII,161 S. Ill., graph. Darst. |
| ISBN: | 9780470683187 9780470683194 047068318X |
Internformat
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| 245 | 1 | 0 | |a Practical raman spectroscopy |b an introduction |c Peter Vandenabeele |
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Datensatz im Suchindex
| _version_ | 1806325526299672576 |
|---|---|
| adam_text |
Contents
Preface
xiii
Acknowledgements
xv
Acronyms, Abbreviations and Symbols
xvii
Introduction to Raman spectroscopy
xix
1
Theoretical Aspects
1
1.1
Classical Approach
1
1.2
Selection Rule
7
1.3
Energy Levels and Group Frequencies
13
1.4
Raman Intensity
19
1.5
Raman Bandwidth
35
1.6
The General Appearance of a Raman Spectrum
37
1.7
Summary
38
Intermezzo
1.1
The Hannonic Oscillator and the Position
of the Vibrational Energy Levels
6
Intermezzo
1.2
The Anharmonic Oscillator and the
Position of Vibrational Energy Levels
1
1
Intermezzo
1.3
Raman Intensity Annotations
30
χ
Contents
2
Interferences and Side-effects
39
2.1
Absorption
40
2.2
Fluorescence
40
2.3
Thermal Effects, Photodecomposition and Laser
Ablation
43
2.4
Ambient Light and Background Radiation
44
2.5
Summary
44
3
Enhancement of the Raman Signal
47
3.1
Resonance Raman (RR) Spectroscopy
48
3.2
Surface-Enhanced Raman Spectroscopy
(SERS)
48
3.2.1
Working Principle of
SERS
49
(a) Chemical Enhancement
49
(b) Field Enhancement
51
3.2.2
Preparation of
SERS
Substrates
53
(a) Colloids
54
(b) Sputtering
55
(c) Electrochemical Production
55
(d) Etching
56
3.2.3
SERS Active
Molecules
56
3.2.4
Advantages and Disadvantages of
SERS
57
3.3
Summary
59
Intermezzo
3.1
The Analysis of Organic Dyes by
SERS
58
4
Raman Instrumentation
61
4.1
Lasers
62
4.1.1
Classification According to Safety Category
64
4.1.2
The Operating Principle of the Laser
65
4.1.3
Lasers for Raman Spectroscopy
71
4.2
Detectors
74
4.2.1
Single-Channel Detectors
75
4.2.2
Multi-Channel Detectors
76
Contents xi
4.2.3 Charge-Coupled Device (CCD)
Detectors
76
4.2.4
Semi-conductor Detectors
80
4.3
Filters
81
4.4
Dispersion Systems
83
4.4.1
Systems Based on Diffraction of Light
83
4.4.2
Fourier-Transform (FT-) Systems
86
4.5
Components for Transportation of Light
88
4.6
Sample Chambers and Measurement Probes
91
4.7
Noise in Raman Spectroscopy
95
4.7.1
Noise Originating from the Sample: as
96
4.7.2
Noise Originating from the Raman
Instrument:
σ,
98
4.7.3
Noise Originating from the Signal
Processing:
σρ
99
4.8
Summary
99
Intermezzo
4.1
The Helium-Neon laser
69
5
Raman Spectroscopy in Daily Lab-life
101
5.1
Calibration of a Raman Spectrometer
102
5.1.1
Х
-Axis Calibration
102
5.1.2
Y-Axis Calibration
105
5.2
Raman Spectral Post-processing
108
5.2.1
Digital Filters
109
5.2.2
Scaling
110
5.2.3
Deconvolution
112
5.2.4
Baseline Corrections
113
5.3
Interpretation of Raman Spectra of
Organic Molecules
116
5.3.1
Raman Spectra of Alkanes and Cycloalkanes
120
5.3.2
Raman Spectra of Alkenes and Cycloalkenes
125
5.3.3
Raman Spectra of
Aromates
129
5.4
Interpretation of Raman Spectra of Inorganic
Molecules
131
Xli
Contents
5.5
Quantitative Aspects of Raman Spectroscopy
134
5.6
Fingerprinting and Spectral Searching Algorithms
137
5.7
Raman Mapping and Imaging
141
5.8
Combination with Other Techniques
145
5.9
Summary
147
Intermezzo
5.1
Micro-Raman Spectroscopy in
Microbiology
107
Intermezzo
5.2
Raman Spectroscopy in a Forensics
Laboratory
117
Intermezzo
5.3
Pigment Analysis with Raman
Spectroscopy
132
Intermezzo
5.4
Detection of Counterfeit Medicines
with Raman Spectroscopy
136
Intermezzo
5.5
Exobiology: Raman Spectroscopy Helps
the Search for Life on Mars
139
Intermezzo
5.6
Direct Analysis of Precious Art Objects
144
Responses to Questions
149
Bibliography
153
Glossary of Terms
155
Index
157 |
| any_adam_object | 1 |
| author | Vandenabeele, Peter |
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| dewey-ones | 543 - Analytical chemistry |
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| dewey-search | 543.57 |
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| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| edition | 1. publ. |
| format | Book |
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| institution | BVB |
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| language | English |
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| spelling | Vandenabeele, Peter Verfasser (DE-588)188479023 aut Practical raman spectroscopy an introduction Peter Vandenabeele 1. publ. Chichester Wiley 2013 XXII,161 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Raman-Spektroskopie (DE-588)4176916-8 gnd rswk-swf Raman-Spektrum (DE-588)4218835-0 gnd rswk-swf (DE-588)4151278-9 Einführung gnd-content Raman-Spektrum (DE-588)4218835-0 s DE-604 Raman-Spektroskopie (DE-588)4176916-8 s X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4291972&prov=M&dok_var=1&dok_ext=htm Inhaltstext Digitalisierung UB Regensburg application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026177955&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Vandenabeele, Peter Practical raman spectroscopy an introduction Raman-Spektroskopie (DE-588)4176916-8 gnd Raman-Spektrum (DE-588)4218835-0 gnd |
| subject_GND | (DE-588)4176916-8 (DE-588)4218835-0 (DE-588)4151278-9 |
| title | Practical raman spectroscopy an introduction |
| title_auth | Practical raman spectroscopy an introduction |
| title_exact_search | Practical raman spectroscopy an introduction |
| title_full | Practical raman spectroscopy an introduction Peter Vandenabeele |
| title_fullStr | Practical raman spectroscopy an introduction Peter Vandenabeele |
| title_full_unstemmed | Practical raman spectroscopy an introduction Peter Vandenabeele |
| title_short | Practical raman spectroscopy |
| title_sort | practical raman spectroscopy an introduction |
| title_sub | an introduction |
| topic | Raman-Spektroskopie (DE-588)4176916-8 gnd Raman-Spektrum (DE-588)4218835-0 gnd |
| topic_facet | Raman-Spektroskopie Raman-Spektrum Einführung |
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