Handbook of polymer crystallization:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
Hoboken, NJ
Wiley
2013
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Klappentext |
| Beschreibung: | XVI, 481 S. Ill., graph. Darst. |
| ISBN: | 9780470380239 |
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| 245 | 1 | 0 | |a Handbook of polymer crystallization |c ed. by Ewa Piorkowska ... |
| 264 | 1 | |a Hoboken, NJ |b Wiley |c 2013 | |
| 300 | |a XVI, 481 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
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Datensatz im Suchindex
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| adam_text | CONTENTS
Preface
xiii
Contributors
xv
1
Experimentai
Techniques
1
Benjamin
S.
Hsiao, Feng Zuo, and Yimin
Mao, Christoph Schick
1.1
Introduction,
1
1.2
Optical Microscopy,
2
1.2.1
Reflection and Transmission Microscopy,
2
1.2.2
Contrast Modes,
2
1.2.3
Selected Applications,
3
1.3
Electron Microscopy,
5
1.3.1
Imaging Principle,
5
1.3.2
Sample Preparation,
6
1.3.3
Relevant Experimental Techniques,
7
1.3.4
Selected Applications,
8
1.4
Atomic Force Microscopy,
9
1.4.1
Imaging Principle,
9
1.4.2
Scanning Modes,
9
1.4.3
Comparison between AFM and EM,
10
1.4.4
Recent Development: Video AFM,
10
1.4.5
Selected Applications,
10
1.5
Nuclear Magnetic Resonance,
12
1.5.1
Chemical Shift,
13
1.5.2
Relevant Techniques,
13
1.5.3
Recent Development: Multidimensional NMR,
14
1.5.4
Selected Applications,
14
1.6
Scattering Techniques:
Х
-Ray, Light, and Neutron,
15
1.6.1
Wide-Angle
Х
-Ray Diffraction,
15
1.6.2
Small-Angle
Х
-Ray Scattering,
17
1.6.3
Small-Angle Light Scattering,
19
1.6.4
Small-Angle Neutron Scattering,
21
1.7
Differential Scanning Calorimetry,
22
1.7.1
Modes of Operation,
22
1.7.2
Determination of Degree of Crystallinity,
25
vi
CONTENTS
1.8
Summary,
25
Acknowledgments,
26
References,
26
2
Crystal Structures of Polymers
31
Claudio De
Rosa and Finizia
Aurìemma
2.1
Constitution and Configuration of Polymer Chains,
31
2.2
Conformation of Polymer Chains in Crystals and Conformational
Polymorphism,
33
2.3
Packing of Macromolecules in Polymer Crystals,
43
2.4
Symmetry Breaking,
49
2.5
Packing Effects on the Conformation of Polymer Chains in the
Crystals: The Case of Aliphatic
Polyamides, 50
2.6
Defects and Disorder in Polymer Crystals,
55
2.6.1
Substitutional Isomorphism of Different Chains,
56
2.6.2
Substitutional Isomorphism of Different
Monomeric
Units,
57
2.6.3
Conformational Isomorphism,
58
2.6.4
Disorder in the Stacking of Ordered Layers (Stacking Fault
Disorder),
58
2.7
Crystal Habits,
60
2.7.1
Rounded Lateral Habits,
66
Acknowledgments,
67
References,
67
3
Structure of Polycrystalline Aggregates
73
Buckley Crist
3.1
Introduction,
73
3.2
Crystals Grown from Solution,
75
3.2.1
Facetted Monolayer Crystals from Dilute Solution,
75
3.2.2
Dendritic Crystals from Dilute Solution,
81
3.2.3
Growth Spirals in Dilute Solution,
85
3.2.4
Concentrated Solutions,
92
3.3
Crystals and Aggregates Grown from Molten Films,
94
3.3.1
Structures in Thin Films,
94
3.3.2
Structures in Ultrathin Films,
98
3.3.3
Edge-On Lamellae in Molten Films,
102
3.4
Spherulitic Aggregates,
104
3.4.1
Optical Properties of Spherulites,
105
3.4.2
Occurrence of Spherulites,
108
3.4.3
Development of Spherulites,
110
3.4.4
Banded Spherulites and Lamellar Twist,
116
Acknowledgments,
121
References,
121
4
Polymer Nucleation
125
Kiyoka
N.
Okada and Masamichi Hikosaka
4.1
Introduction,
126
4.2
Classical
Nucłeation
Theory,
126
4.2.1
Nucleation Rate
(ƒ), 126
4.2.2
Free Energy for Formation of a Nucleus AG(N),
127
CONTENTS
vii
4.2.3
Free Energy for Formation of a Critical Nucleus (AC),
127
4.2.4
Shape of a Nucleus Is Related to Kinetic Parameters.
128
4.2.5
Diffusion.
128
4.3
Direct Observation of Nano-Nucleation by Synchrotron
Radiation.
128
4.3.1
Introduction and Experimental Procedure.
128
4.3.2
Observation of Nano-Nucleation by SAXS,
128
4.3.3
Extended Guinier Plot Method and Iteration Method.
129
4.3.4
Kinetic Parameters and Size Distribution of the
Nano-Nucleus.
130
4.3.5
Real Image of Nano-Nucleation.
131
4.3.6
Supercooling Dependence of Nano-nucleation,
133
4.3.7
Relationship between Nano-Nucleation and
Macro-Crystallization.
133
4.4
Improvement of Nucleation Theory.
135
4.4.1
Introduction.
135
4.4.2
Nucleation Theory Based on Direct Observation of
Nucleation.
135
4.4.3
Confirmation of the Theory by Overall Crystallinity,
137
4.5
Homogeneous Nucleation from the Bulk Melt under Elongational
Flow.
139
4.5.1
Introduction and Case Study.
139
4.5.2
Formulation of Elongational Strain Rate ¿.
139
4.5.3
Nano-Oriented Crystals.
140
4.5.4
Evidence of Homogeneous Nucleation.
144
4.5.5
Nano-Nucleation Results in Ultrahigh Performance.
147
4.6
Heterogeneous Nucleation.
148
4.6.1
Introduction,
148
4.6.2
Experimental,
149
4.6.3
Role of Epitaxy in Heterogeneous Nucleation.
150
4.6.4
Acceleration Mechanism of Nucleation of Polymers by Nano-
Sizing of Nucleating Agent.
153
4.7
Effect of Entanglement Density on the Nucleation Rate.
156
4.7.1
Introduction and Experimental.
156
4.7.2
Increase of ve Leads to a Decrease of
/, 157
4.7.3
Change of vc with At.
158
4.7.4
Two-Step Entangling Model.
159
4.8
Conclusion.
160
Acknowledgments.
161
References,
161
5
Growth of Polymer Crystals
165
Kohji Tashiro
5.1
Introduction,
165
5.1.1
Complex Behavior of Polymers,
165
5.2
Growth of Polymer Crystals from Solutions,
167
5.2.1
Single Crystals.
167
5.2.2
Crystallization from Solution under Shear,
168
5.2.3
Solution Casting Method,
168
5.3
Growth of Polymer Crystals from Melt,
169
5.3.1
Positive and Negative Spherulites,
169
5.3.2
Spherulite Morphology and Crystalline Modification,
170
5.3.3
Spherulite Patterns of Blend Samples,
172
viii
COM IN IS
5.4
Crystallization Mechanism
uf
Polymer.
173
5.4.1
Basic ITicory of Crystallization of Polymer.
173
5.4.2
Growth Rate of Spherulites.
177
5.5
Microscopically Viewed Structural Involution in the Growing Pohiner
Crystals. 17S
5.5.1
Experimental Techniques, I7S
5.5.2
Structural Involution in Isothermal Crystallization.
179
5.5.3
Shear-Induced Crystallization of the Melt. lSh
5.6
Crystallization upon Heating from the Glassy State.
1X9
5.6.1
Cold Crystallization.
189
5.6.2
Solvent-Induced Crystallization of Polymer
(ilass.
1X9
5.7
Crystallization Phenomenon Induced by Tensile Force.
191
5.cS Photoinduced Formation and Growth of Polymer Crystals.
191
5.9
Conclusion.
192
References.
193
6
Computer .Modeling of Polymer Crystallization
197
Gregory C. Rut/edge
6.1
Introduction.
197
6.2
Methods,
198
6.2.1
Molecular Dynamics.
199
6.2.2
Langevin
Dynamics.
200
6.2.3
Monte Carlo.
200
6.2.4
Kinetic Monte Carlo.
201
6.3
Single-Chain Behavior in Crystallization.
202
6.3.1
Solid-on-Solid Models.
202
6.3.2
Molecular and
Langevin
Dynamics.
203
6.4
Crystallization from the Melt.
204
6.4.1
Lattice Monte Carlo Simulations.
205
6.4.2
Molecular Dynamics Using Coarse-Grained
Models.
206
6.4.3
Molecular Dynamics Using Atomistic Models.
207
6.5
Crystallization under Deformation or Flow.
208
6.6
Concluding Remarks,
210
References.
211
7
Overall Crystallization Kinetics
215
Ewa
Piorkowska and
Andrzej Galeski
7.1
Introduction.
215
7.2
Measurements.
216
7.3
Simulation.
217
7.4
Theories: Isothermal and Nonisothermal Crystallization.
218
7.4.1
Introductory Remarks.
218
7.4.2
Extended Volume Approach.
218
7.4.3
Probabilistic Approaches.
220
7.4.4
Isokinetic Model,
223
7.4.5
Rate Equations,
223
7.5
Complex Crystallization Conditions: General Models.
224
7.6
Factors Influencing the Overall Crystallization Kinetics,
224
7.6.1
Crystallization in a Uniform Temperature Field.
224
7.6.2
Crystallization in a Temperature Gradient.
225
7.6.3
Crystallization in a Confined Space.
226
7.6.4
Flow-Induced Crystallization,
228
CONTENTS ix
7.7
Analysis of Crystallization Data,
230
7.7.1
Isothermal Crystallization,
230
7.7.2
Nonisothermal Crystallization,
231
7.8
Conclusions,
233
References,
234
8
Epitaxial Crystallization of Polymers: Means and Issues
237
Annette Thierry and Bernard A. Lotz
8.1
Introduction and History,
237
8.2
Means of Investigation of Epitaxial Crystallization,
239
8.2.1
Global Techniques,
239
8.2.2
Thin Film Techniques,
239
8.2.3
Sample Preparation Techniques,
240
8.2.4
Other Samples and Investigation Procedures,
241
8.3
Epitaxial Crystallization of Polymers,
241
8.3.1
General Principles,
241
8.3.2
Epitaxial Crystallization of Linear Polymers,
243
8.3.3
Epitaxy of Helical Polymers,
245
8.3.4
Polymer/Polymer Epitaxy,
250
8.4
Epitaxial Crystallization: Further Issues and Examples,
252
8.4.1
Topographic versus Lattice Matching,
252
8.4.2
Epitaxy of Isotactic Polypropylene on Isotactic
Polyvinylcyclohexane,
254
8.4.3
Epitaxy Involving Fold Surfaces of Polymer Crystals,
254
8.5
Epitaxial Crystallization: Some Issues and Applications,
256
8.5.1
Epitaxial Crystallization and the Design of New Nucleating
Agents,
256
8.5.2
Epitaxial Crystallization and the Design of Composite
Materials,
257
8.5.3
Conformational and Packing Energy Analysis of Polymer
Epitaxy,
258
8.5.4
Epitaxy as a Means to Generate Oriented
Opto- or
Electroactive Materials,
259
8.6
Conclusions,
260
References,
262
9
Melting
265
Marek Pyda
9.1
Introduction to the Melting of Polymer Crystals,
265
9.2
Parameters of the Melting Process,
267
9.3
Change of Conformation,
268
9.4
Heat of Fusion and Degree of Crystallinity,
270
9.4.1
Heat of Fusion,
270
9.4.2
Degree of Crystallinity,
272
9.5
Equilibrium Melting,
274
9.5.1
The Equilibrium Melting Temperature,
274
9.5.2
The Equilibrium Thermodynamic Functions,
275
9.6
Other Factors Affecting the Melting Process of Polymer Crystals,
277
9.6.1
The Influence of the Polymer s Chemical Structure on the
Melting Process,
277
9.6.2
The Effect of Polymer Molar Mass on the Melting
Behavior,
277
9.6.3
Influence of Heating Rate on the Melting,
278
χ ΓΟΝΗ
NTS
9 A4
Multiple Molting Peaks of Polymers.
274
9.6.5
Influence of Pressure on the Melting Process.
2X1
Ч.Ь.Ь
Hie Melting Proeess by Other Methods. 2S1
9.h.7 Diluents Effect: The Influence of Small Diluents on the
Melting Proeess. 2S2
9.7
Irreversible and Reversible Melting,
282
9.8
Conclusions. 2S4
References.
285
10
Crystallization of Polymer Blends
287
Mariano Pnwella
10.1
General Introduction.
287
10.2
Thermodynamics of Polymer Blends.
288
10.2.1
General Principles.
288
10.3
Miscible
Polymer Blends.
290
10.3.1
Introduction.
290
10.3.2
Phase Morphology.
291
10.3.3
Crystal Growth Rate.
292
10.3.4
Overall Crystallization Kinetics.
294
10.3.5
Melting Behavior.
295
10.3.6
Blends with Partial Miscibility.
296
10.3.7
Crystallization Behavior of Amorphous Crystalline Blends.
297
10.3.8
Crystallization Behavior of Crystalline Crystalline Blends. 29S
10.4
Immiscible Polymer Blends,
303
10.4.1
Introduction.
303
10.4.2
Morphology and Crystal Nucleation.
303
10.4.3
Crystal Growth Rate.
304
10.4.4
Crystallization Behavior of Immiscible Blends.
305
10.5
Compatibilized Polymer Blends.
307
10.5.1
Compatibilization Methods,
307
10.5.2
Morphology and Phase Interactions.
308
10.5.3
Crystallization Behavior of Compatibilized Blends.
311
10.6
Polymer Blends with Liquid-Crystalline Components.
314
10.6.1
Introduction.
314
10.6.2
Mesomorphism and Phase Transition Behavior of Liquid
Crystals and Liquid Crystal Polymers.
314
10.6.3
Crystallization Behavior of Polymer LC Blends.
316
10.6.4
Crystallization Behavior of Polymer/LCP Blends.
317
10.7
Concluding Remarks,
320
Abbreviations.
321
References.
322
11
Crystallization in Copolymers
327
Sheng Li and Richard A. Register
11.1
Introduction.
327
11.2
Crystallization in Statistical Copolymers.
328
11.2.1
Flory
s
Model.
328
11.2.2
Solid-State Morphology.
330
11.2.3
Mechanical Properties,
334
11.2.4
Crystallization Kinetics.
335
11.2.5
Statistical Copolymers with Two Crystallizable Units.
337
11.2.6
Crystallization Thermodynamics.
337
CONTENTS xi
11.3
Crystallization of Block Copolymers from Homogeneous or Weakly
Segregated Melts,
340
11.3.1
Solid-State Morphology,
340
11.3.2
Crystallization-Driven Structure Formation,
342
11.4
Summary,
343
References,
344
12
Crystallization in Nano-Confined Polymeric Systems
347
Alejandro J.
Müller,
Maria
Luisa
Amai,
and
Arnaldo
T.
Lorenzo
12.1
Introduction,
347
12.2
Confined Crystallization in Block Copolymers,
348
12.2.1
Crystallization within Diblock Copolymers that are Strongly
Segregated or
Miscible
and Contain only One Crystallizable
Component,
351
12.2.2
Crystallization within Strongly Segregated
Double-Crystalline Diblock Copolymers and
Triblock Copolymers,
355
12.3
Crystallization of Droplet Dispersions and Polymer Layers,
361
12.4
Polymer Blends,
368
12.4.1
Immiscible Polymer Blends,
368
12.4.2
Melt
Miscible
Blends,
371
12.5
Modeling of Confined Crystallization of Macromolecules,
371
12.6
Conclusions,
372
References,
372
13
Crystallization in Polymer Composites and Nanocomposites
379
Ewa Piorkowska
13.1
Introduction,
379
13.2
Microcomposites
with Particulate Fillers,
380
13.3
Fiber-Reinforced Composites,
382
13.4
Modeling of Crystallization in Fiber-Reinforced Composites,
385
13.5
Nanocomposites,
388
13.6
Conclusions,
393
Appendix,
393
References,
394
14
Flow-Induced Crystallization
399
Gerrit
W.M.
Peters,
Luigi Balzano,
and
Rudi
J.
Α.
Steenbakkers
14.1
Introduction,
399
14.2
Shear-Induced Crystallization,
401
14.2.1
Nature of Crystallization Precursors,
405
14.3
Crystallization during Drawing,
407
14.3.1
Spinning,
408
14.3.2
Elongation-Induced Crystallization; Lab Conditions,
409
14.4
Models of Flow-Induced Crystallization,
410
14.4.1
Flow-Enhanced Nucleation,
411
14.4.2
Flow-Induced Shish Formation,
419
14.4.3
Application to Injection Molding,
421
14.5
Concluding Remarks,
426
References,
427
xii CONTENTS
15
Crystallization in Processing Conditions
433
Jean-Marc Htuulin
15.1
Introduction.
433
15.2
General Effects of Processing Conditions on Crystallization.
433
15.2.1
Effects of Flow.
433
15.2.2
Effects of Pressure.
435
15.2.3
Effects of Cooling Rate.
436
15.2.4
Effects of a Temperature Gradient.
437
15.2.5
Effects of Surfaces.
439
15.3
Modeling.
440
15.3.1
General Framework.
440
15.3.2
Simplified Expressions.
441
15.3.3
General Systems of Differential Equations.
441
15.4
Crystallization in Some Selected Processes.
442
15.4.1
Cast Film Extrusion,
442
15.4.2
Fiber Spinning,
445
15.4.3
Film Blowing.
448
15.4.4
Injection Molding.
454
15.5
Conclusion.
458
References.
459
Index
463
International
team of experts reviews the latest
developments in polymer crystallization
The complexity of polymer crystallization has posed a long-standing challenge to the scientific community,
demanding the development and application of a variety of microscopic,
calorimetrie,
and
spectroscopie
experimental methods. By building our understanding ofpolymer crystallization, researchers have helped fuel the
advancement of nanoscience and nanotechnology.
Offering a comprehensive review of the field. Handbook of Polymer Crystallization examines the latest
discoveries, helping readers not only understand polymer crystallization, but also take full advantage of the
phenomenon in order to design new materials and develop new applications. The book also explores the many
problems rhat can arise during the crystallization process, setting forth tested and proven solutions to achieve
desired results.
Handbook oj Polymer Crystallization features contributions from an international team of thermoplastic polymer
scientists and covers such topics as:
•
Experimental techniques for studies ofpolymer crystallization
•
Structure of crystalline polymers, kinetics or nucleation, and growth of the crystalline phase
•
Molecular modeling ofpolymer crystallization and crystallization kinetics
•
Crystallization in copolymers,
miscible
and immiscible polymer blends, and polymer composites
•
Crystallization under confinement
•
Effect of flow on crystallization
Figures provided throughout the book help illustrate the core principles and mechanisms of polymer
crystallization. In addition, references at the end of each chapter guide readers to rhe primary lirerarure in
order to investigate individual topics in greater depth.
Examining the most important developments in polymer crystallization, this book is recommended for ail
thermoplastic polymers researchers, offering them the foundation needed to make their own discoveries.
DR.
EWA
PIORKOWSKA, is Professor and the Head of the Department of Polymer Structure at the Cenrre
of Molecular and Macromolecuiar Studies, Polish Academy of Sciences, Poland. Her research interests include
crystallization, structure and properties of polymers, polymer blends, composites and nanocomposites.
DR. GREGORY
С
RUTLEDGE, is rhe Lammot
du Pont
Professor in the Department of Chemical
Engineering at the Massachusetts Institute of Technology. His research interests include polymer science and
engineering, statistical thermodynamics, molecular simularion, and nanotechnology.
Illustrano)
|
| any_adam_object | 1 |
| author_GND | (DE-588)1043690727 |
| building | Verbundindex |
| bvnumber | BV041104574 |
| classification_rvk | UV 3200 ZM 5100 |
| ctrlnum | (OCoLC)858017756 (DE-599)BVBBV041104574 |
| dewey-full | 547.7 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 547 - Organic chemistry |
| dewey-raw | 547.7 |
| dewey-search | 547.7 |
| dewey-sort | 3547.7 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik Werkstoffwissenschaften / Fertigungstechnik |
| format | Book |
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| id | DE-604.BV041104574 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T00:39:43Z |
| institution | BVB |
| isbn | 9780470380239 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-026080898 |
| oclc_num | 858017756 |
| open_access_boolean | |
| owner | DE-703 DE-83 DE-29T |
| owner_facet | DE-703 DE-83 DE-29T |
| physical | XVI, 481 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Wiley |
| record_format | marc |
| spelling | Handbook of polymer crystallization ed. by Ewa Piorkowska ... Hoboken, NJ Wiley 2013 XVI, 481 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Kristallisation (DE-588)4033215-9 gnd rswk-swf Polymere (DE-588)4046699-1 gnd rswk-swf Polymerkristall (DE-588)4175241-7 gnd rswk-swf Polymerkristall (DE-588)4175241-7 s DE-604 Polymere (DE-588)4046699-1 s Kristallisation (DE-588)4033215-9 s Piorkowska, Ewa Sonstige (DE-588)1043690727 oth Digitalisierung UB Bayreuth - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026080898&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis Digitalisierung UB Bayreuth - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026080898&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Klappentext |
| spellingShingle | Handbook of polymer crystallization Kristallisation (DE-588)4033215-9 gnd Polymere (DE-588)4046699-1 gnd Polymerkristall (DE-588)4175241-7 gnd |
| subject_GND | (DE-588)4033215-9 (DE-588)4046699-1 (DE-588)4175241-7 |
| title | Handbook of polymer crystallization |
| title_auth | Handbook of polymer crystallization |
| title_exact_search | Handbook of polymer crystallization |
| title_full | Handbook of polymer crystallization ed. by Ewa Piorkowska ... |
| title_fullStr | Handbook of polymer crystallization ed. by Ewa Piorkowska ... |
| title_full_unstemmed | Handbook of polymer crystallization ed. by Ewa Piorkowska ... |
| title_short | Handbook of polymer crystallization |
| title_sort | handbook of polymer crystallization |
| topic | Kristallisation (DE-588)4033215-9 gnd Polymere (DE-588)4046699-1 gnd Polymerkristall (DE-588)4175241-7 gnd |
| topic_facet | Kristallisation Polymere Polymerkristall |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026080898&sequence=000003&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026080898&sequence=000004&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT piorkowskaewa handbookofpolymercrystallization |