Reaction kinetics of solid fuels during entrained flow gasification:
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
München
Verl. Dr. Hut
2013
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| Ausgabe: | 1. Aufl. |
| Schriftenreihe: | Forschungsschriften des Lehrstuhls für Energiesysteme, Technische Universität München
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| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | Weitere Ausgabe: Online-Ausg., Tremel, Alexander: Reaction Kinetics of Solid Fuels during Entrained Flow Gasification |
| Beschreibung: | XVI, 260 S. Ill., graph. Darst. 21 cm, 420 g |
| ISBN: | 9783843908160 3843908168 |
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IMAGE 1
CONTENTS
PREFACE I
ABSTRACT III
KURZFASSUNG V
ABBREVIATIONS AND NOMENCLATURE X I
1 INTRODUCTION AND BACKGROUND INFORMATION 1
1.1 THE DEVELOPMENT OF OUR ENERGY SYSTEM 1
1.2 GASIFICATION AS A TOOL FOR FUTURE SUSTAINABLE ENERGY UTILISATION 2
1.3 OUTLINE OF THE DISSERTATION 4
2 FUNDAMENTALS 7
2.1 THE GASIFICATION PROCESS OF SOLID FUELS 7
2.1.1 DEVOLATILISATION 7
2.1.2 HETEROGENEOUS GASIFICATION REACTIONS 9
2.1.3 HOMOGENEOUS GAS REACTIONS 12
2.1.4 REACTION RATES OF SINGULAR PROCESSES 13
2.1.5 DEFINITION OF REACTION RATE 15
2.2 EXPERIMENTAL METHODS FOR THE INVESTIGATION OF SOLID FUEL
GASIFICATION . . . 16 2.2.1 FLOW REACTORS 16
2.2.2 THERMOGRAVIMETRIC ANALYSERS 18
2.2.3 WIRE MESH REACTORS 20
2.2.4 FLUIDISED AND FIXED BED REACTORS 21
2.2.5 LABORATORY PROCEDURES FOR FUEL AND CHAR CHARACTERISATION 22
3 LITERATURE REVIEW ON GASIFICATION KINETICS 27
3.1 VOLATILE YIELD AND CHAR PROPERTIES AFTER DEVOLATILISATION 28
3.1.1 EFFECT OF THERMAL HISTORY ON VOLATILE YIELD AND CHAR PROPERTIES .
. 28 3.1.2 EFFECT OF PRESSURE ON VOLATILE YIELD AND CHAR PROPERTIES 38
3.1.3 EFFECT OF GAS ATMOSPHERE ON VOLATILE YIELD AND CHAR PROPERTIES . .
42 3.2 INFLUENCES ON THE HETEROGENEOUS CHAR CONVERSION 43
3.2.1 INFLUENCE OF OPERATION PARAMETERS ON THE INTRINSIC REACTION RATE .
43 3.2.2 MEASUREMENTS OF REACTION RATES AT HIGHER TEMPERATURE 49 3.3
SUMMARY OF THE LITERATURE REVIEW AND RESEARCH DEMAND 54
3.4 AIMS AND RESEARCH STRATEGY O F THE DISSERTATION 58
VII
HTTP://D-NB.INFO/1030510474
IMAGE 2
4 THEORETICAL DEVELOPMENT AND SELECTION OF GASIFICATION MODELS FOR SOLID
FUELS 6 1
4.1 SELECTION OF A PYROLYSIS MODEL 61
4.1.1 OVERVIEW OF PYROLYSIS MODELS FROM LITERATURE 61
4.1.2 DEVELOPMENT OF A PYROLYSIS MODEL BASED ON EXPERIMENTAL DATA . . 63
4.2 DEVELOPMENT AND SELECTION OF CHAR CONVERSION MODELS 67
4.2.1 NOTATION AND DEFINITION OF CHAR REACTIVITY 67
4.2.2 SIMPLE MODEL APPROACH FOR THE OBSERVED REACTION RATE 68 4.2.3
SUBMODELS FOR INTRINSIC CHAR REACTIVITY UNDER REGIME I CONDITIONS 69
4.2.4 SUBMODEL FOR THE VARIATION OF REACTION RATE WITH CONVERSION . . .
74 4.2.5 SUBMODEL FOR THE INFLUENCE OF THERMAL DEACTIVATION 76'
4.2.6 SUBMODEL FOR PORE DIFFUSION 82
4.2.7 SUBMODEL FOR BOUNDARY LAYER DIFFUSION 92
4.2.8 SUBMODEL FOR PARTICLE SIZE AND DENSITY 93
4.2.9 STATE OF THE ART IN CFD MODELLING OF ENTRAINED FLOW GASIFIERS.
96
5 EXPERIMENTAL TECHNIQUES, PROCEDURES, AND RESULTS 99
5.1 FUEL AND REFERENCE CHAR PREPARATION 99
5.1.1 PROCEDURE FOR PROCESSING COAL AND BIOMASS 99
5.1.2 PRODUCTION OF REFERENCE CHAR 100
5.2 METHODS USED IN THE LABORATORY ANALYSIS 101
5.2.1 PROXIMATE AND ULTIMATE ANALYSIS 101
5.2.2 CHAR SURFACE MEASUREMENT 102
5.2.3 MEASUREMENT OF PARTICLE SIZE DISTRIBUTION 102
5.2.4 PARTICLE DENSITY MEASUREMENT 102
5.3 EXPERIMENTAL FACILITIES AND PROCEDURES 103
5.3.1 PRESSURISED HIGH TEMPERATURE ENTRAINED FLOW REACTOR 103 5.3.2 BABY
HIGH TEMPERATURE ENTRAINED FLOW REACTOR 113
5.3.3 PRESSURISED WIRE MESH REACTOR 116
5.3.4 PRESSURISED THERMOGRAVIMETRIC ANALYSER 119
5.3.5 ATMOSPHERIC THERMOGRAVIMETRIC ANALYSER 124
5.4 EXPERIMENTAL RESULTS 126
5.4.1 RESULTS FROM THE ENTRAINED FLOW REACTORS 126
5.4.2 RESULTS FROM THE WIRE MESH REACTOR 154
5.4.3 RESULTS FROM THE PRESSURISED THERMOGRAVIMETRIC ANALYSIS 156 5.4.4
RESULTS FROM THE ATMOSPHERIC THERMOGRAVIMETRIC ANALYSIS 164
6 VALIDATION OF PYROLYSIS MODELS FOR ENTRAINED FLOW GASIFICATION 169 6.1
VOLATILE YIELD AS A FUNCTION OF PRESSURE AND TEMPERATURE 169
6.2 ANALYSIS OF THE DEVOLATILISATION KINETICS 171
7 VALIDATION OF THE CHAR CONVERSION MODELS FOR ENTRAINED FLOW
GASIFICATION 175 7.1 VALIDATION OF THE CHAR GASIFICATION SUBMODELS 175
7.1.1 VALIDATION OF THE INTRINSIC REACTIVITY SUBMODELS 176
7.1.2 VALIDATION OF THE SURFACE AREA SUBMODEL 184
7.1.3 VALIDATION OF THE THERMAL DEACTIVATION SUBMODELS 188
VIII
IMAGE 3
7.2 VALIDATION OF THE MODEL FRAMEWORK BY USING ENTRAINED FLOW DATA 191
7.2.1 VALIDATION OF THE SIMPLE EMPIRICAL CHAR GASIFICATION MODEL 193
7.2.2 VALIDATION OF THE COMPREHENSIVE MODEL FRAMEWORK 198
8 SIMULATION OF INDUSTRIAL SCALE ENTRAINED FLOW GASIFIERS 203
8.1 DESCRIPTION OF THE SIMULATION APPROACH 203
8.1.1 GASIFIER GEOMETRY AND BOUNDARY CONDITIONS 203
8.1.2 CALCULATION OF REACTION RATE, TEMPERATURE, AND GAS COMPOSITION 204
8.1.3 LIMITATIONS OF THE SIMULATION 205
8.2 SIMULATION OF A 500 M W ENTRAINED FLOW GASIFIER FOR LIGNITE R 206
8.2.1 DESIGN OF THE LIGNITE R GASIFIER 206
8.2.2 OPTIMISATION OF THE LIGNITE R GASIFIER 210
8.3 FUEL SPECIFIC ADAPTION OF GASIFIER LAYOUT AND OPERATION 213
8.4 ANALYSIS O F THE REACTION REGIME IN ENTRAINED FLOW GASIFIERS 217
9 DEVELOPMENT OF A FUEL TEST PROCEDURE FOR ENTRAINED FLOW GASIFICATION
221 9.1 ENTRAINED FLOW GASIFICATION EXPERIMENTS 222
9.2 PYROLYSIS EXPERIMENTS 223
9.2.1 ENTRAINED FLOW PYROLYSIS EXPERIMENTS 224
9.2.2 PYROLYSIS EXPERIMENTS IN THE WIRE MESH REACTOR 225
9.3 CHAR ANALYSIS 226
9.3.1 CHAR SPECIFIC SURFACE AREA EVOLUTION DURING CONVERSION 226 9.3.2
QUANTIFICATION OF THERMAL CHAR DEACTIVATION 226
9.3.3 MEASUREMENT OF INTRINSIC CHAR REACTIVITY 227
10 SUMMARY, CONCLUSIONS, AND RECOMMENDATIONS 231
10.1 SUMMARY OF THE DISSERTATION 231
10.1.1 DATA SET FOR FUEL CONVERSION UNDER ENTRAINED FLOW CONDITIONS . .
231 10.1.2 MODEL DEVELOPMENT FOR ENTRAINED FLOW GASIFICATION 232 10.1.3
LAYOUT AND OPTIMISATION OF LARGER SCALE ENTRAINED FLOW GASIFIERS . 233
10.1.4 THE REACTION REGIME DURING ENTRAINED FLOW GASIFICATION 234
10.1.5 DEVELOPMENT OF A TEST PROCEDURE FOR SOLID FUELS 235
10.2 RECOMMENDATIONS FOR FUTURE WORK 235
10.2.1 RECOMMENDATIONS FOR FUTURE EXPERIMENTAL WORK 235
10.2.2 RECOMMENDATIONS FOR FUTURE MODEL AND SIMULATION APPROACHES . .
236
BIBLIOGRAPHY 239
APPENDICES 253
A CALCULATION OF CONVERSION - ASH TRACER METHOD 253
B ERROR CALCULATION 255
C CALCULATION OF CHEMICAL EQUILIBRIUM 259
IX |
| any_adam_object | 1 |
| author | Tremel, Alexander 1981- |
| author_GND | (DE-588)103230491X |
| author_facet | Tremel, Alexander 1981- |
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| bvnumber | BV041103712 |
| ctrlnum | (OCoLC)858922723 (DE-599)DNB1030510474 |
| dewey-full | 665.772 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 665 - Industrial oils, fats, waxes & gases |
| dewey-raw | 665.772 |
| dewey-search | 665.772 |
| dewey-sort | 3665.772 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| edition | 1. Aufl. |
| format | Thesis Book |
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| spelling | Tremel, Alexander 1981- Verfasser (DE-588)103230491X aut Reaction kinetics of solid fuels during entrained flow gasification Alexander Tremel. Technische Universität München, Lehrstuhl für Energiesysteme 1. Aufl. München Verl. Dr. Hut 2013 XVI, 260 S. Ill., graph. Darst. 21 cm, 420 g txt rdacontent n rdamedia nc rdacarrier Forschungsschriften des Lehrstuhls für Energiesysteme, Technische Universität München Weitere Ausgabe: Online-Ausg., Tremel, Alexander: Reaction Kinetics of Solid Fuels during Entrained Flow Gasification Zugl.: München, Techn. Univ., Diss., 2012 Flugstromreaktor (DE-588)4372540-5 gnd rswk-swf Reaktionskinetik (DE-588)4048655-2 gnd rswk-swf Druckvergasung (DE-588)4150774-5 gnd rswk-swf Fester Brennstoff (DE-588)4154170-4 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Fester Brennstoff (DE-588)4154170-4 s Druckvergasung (DE-588)4150774-5 s Flugstromreaktor (DE-588)4372540-5 s Reaktionskinetik (DE-588)4048655-2 s DE-604 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4249335&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026080056&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Tremel, Alexander 1981- Reaction kinetics of solid fuels during entrained flow gasification Flugstromreaktor (DE-588)4372540-5 gnd Reaktionskinetik (DE-588)4048655-2 gnd Druckvergasung (DE-588)4150774-5 gnd Fester Brennstoff (DE-588)4154170-4 gnd |
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| title | Reaction kinetics of solid fuels during entrained flow gasification |
| title_auth | Reaction kinetics of solid fuels during entrained flow gasification |
| title_exact_search | Reaction kinetics of solid fuels during entrained flow gasification |
| title_full | Reaction kinetics of solid fuels during entrained flow gasification Alexander Tremel. Technische Universität München, Lehrstuhl für Energiesysteme |
| title_fullStr | Reaction kinetics of solid fuels during entrained flow gasification Alexander Tremel. Technische Universität München, Lehrstuhl für Energiesysteme |
| title_full_unstemmed | Reaction kinetics of solid fuels during entrained flow gasification Alexander Tremel. Technische Universität München, Lehrstuhl für Energiesysteme |
| title_short | Reaction kinetics of solid fuels during entrained flow gasification |
| title_sort | reaction kinetics of solid fuels during entrained flow gasification |
| topic | Flugstromreaktor (DE-588)4372540-5 gnd Reaktionskinetik (DE-588)4048655-2 gnd Druckvergasung (DE-588)4150774-5 gnd Fester Brennstoff (DE-588)4154170-4 gnd |
| topic_facet | Flugstromreaktor Reaktionskinetik Druckvergasung Fester Brennstoff Hochschulschrift |
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