Engineering catalysis:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
De Gruyter
2013
|
| Schriftenreihe: | De Gruyter graduate
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XI, 364 S. Ill., graph. Darst. |
| ISBN: | 9783110283365 |
Internformat
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| 264 | 1 | |a Berlin [u.a.] |b De Gruyter |c 2013 | |
| 300 | |a XI, 364 S. |b Ill., graph. Darst. | ||
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Datensatz im Suchindex
| _version_ | 1804150443764350976 |
|---|---|
| adam_text | IMAGE 1
CONTENTS
PREFACE IX
1 THE BASICS 1
1.1 CATALYTIC CONCEPTS 1
1.1.1 DEFINITIONS 1
1.1.2 LENGTH AND TIME SCALES IN CATALYSIS 5
1.1.3 CATALYTIC TRINITY: ACTIVITY, SELECTIVITY, STABILITY 6
1.1.4 COMPOSITION OF CATALYSTS 11
1.2 REACTIVITY OF SOLIDS 14
1.2.1 PHYSISORPTION AND CHEMISORPTION 1 6
1.2.2 BASICS OF CHEMISORPTION THEORY 17
1.2.3 SURFACE CRYSTALLOGRAPHY 18
1.2.4 MECHANISMS OF SOME CATALYTIC REACTIONS 22
1.3 CATALYSIS IN INDUSTRY 26
REFERENCES 34
2 ENGINEERING CATALYSTS 37
2.1 CATALYST DESIGN 37
2.1.1 BEING IN SHAPE 38
2.1.2 SCALING OF CATALYSTS 43
2.2 TOOLBOX IN CATALYSIS 44
2.2.1 GENERAL OVERVIEW OF THE CHARACTERIZATION METHODS 44
2.2.2 ADSORPTION METHODS 46
2.2.3 PHYSISORPTION METHODS 47
2.2.4 CHEMISORPTION 56
2.2.5 TEMPERATURE-PROGRAMMED METHODS 59
2.2.6 CALORIMETRY 63
2.2.7 X-RAY DIFFRACTION 64
2.2.8 X-RAY PHOTOELECTRON SPECTROSCOPY AND X-RAY FLUORESCENCE.... 65
2.2.9 INFRARED AND RAMAN SPECTROSCOPIES 68
2.2.10 CATALYST PARTICLE SIZE MEASUREMENTS 73
2.2.11 ELECTRON PARAMAGNETIC/SPIN RESONANCE 73
2.2.12 MOSSBAUER SPECTROSCOPY 75
2.2.13 X-RAY ABSORPTION SPECTROSCOPY 77
2.2.14 NUCLEAR MAGNETIC RESONANCE 78
2.2.15 IMAGING OF CATALYSTS 80
2.2.16 CATALYTIC REACTIONS: PRODUCT ANALYSIS 87
2.2.17 THEORY AS A PART OF A TOOLBOX 91
2.3 PREPARATION OF CATALYTIC MATERIALS 94
2.3.1 GENERAL OVERVIEW 94
2.3.2 UNSUPPORTED METALS 103
HTTP://D-NB.INFO/1021551333
IMAGE 2
X J CONTENTS
2.3.3 PREPARATION OF BULK OXIDES BY PRECIPITATION 106
2.3.4 HETEROPOLYACIDS 111
2.3.5 CATALYSTS SUPPORTS 112
2.3.6 SUPPORTED CATALYSTS 138
2.3.7 CATALYST FORMING OPERATIONS 154
REFERENCES 162
3 ENGINEERING REACTIONS 165
3.1 INTRODUCTION 165
3.2 THERMODYNAMICS 165
3.3 KINETICS 167
3.3.1 DEFINITIONS 167
3.3.2 REACTION MECHANISM 169
3.3.3 KINETICS OF COMPLEX REACTIONS 177
3.3.4 RELATIONSHIP BETWEEN THERMODYNAMICS AND KINETICS 185
3.3.5 NON-IDEAL SURFACES 185
3.4 KINETIC ASPECTS OF SELECTIVITY 188
3.4.1 STRUCTURE SENSITIVITY 192
3.4.2 MECHANISM-FREE KINETICS - KINETIC POLYNOMIAL 194
3.4.3 WHAT IS BEHIND A RATE CONSTANT? 194
3.4.4 DYNAMIC CATALYSIS 197
3.4.5 DEACTIVATION 197
3.4.6 MATHEMATICAL TREATMENT O F EXPERIMENTAL DATA 202
3.5 MASS TRANSFER 207
3.5.1 DIFFUSION EFFECTS IN HETEROGENEOUS CATALYSIS 207
3.5.2 REACTOR DEPENDENT EXTERNAL DIFFUSION (INTERPHASE MASS TRANSFER,
FILM DIFFUSION) 208
3.5.3 CALCULATION O F DIFFUSION COEFFICIENTS 216
3.5.4 SIZE DEPENDENT INTERNAL (PORE) DIFFUSION 219
3.5.5 NON-ISOTHERMAL CONDITIONS 225
3.5.6 MULTIPLE REACTIONS AND DIFFUSIONAL LIMITATIONS 228
3.5.7 DIFFUSION IN MICROPORES 231
3.5.8 CRITERIA FOR THE ABSENCE OF DIFFUSIONAL LIMITATIONS 232
3.6 CATALYTIC REACTORS 236
3.6.1 LABORATORY REACTORS 236
3.6.2 INDUSTRIAL REACTORS 242
3.6.3 TWO-PHASE REACTORS 242
3.6.4 THREE-PHASE CATALYTIC REACTORS 248
3.6.5 REACTOR MODELING 258
3.6.6 CATALYST HANDING IN A PLANT 267
REFERENCES 274
4 ENGINEERING TECHNOLOGY 277
4.1 GENERAL STRUCTURES OF CHEMICAL PROCESSES 277
4.1.1 SAFETY IN DESIGN 279
4.1.2 CONCEPTUAL PROCESS DESIGN: EXAMPLES 280
4.1.3 CONCEPTUAL PROCESS DESIGN: GENERAL COMMENTS 286
4.1.4 REACTOR SELECTION 288
IMAGE 3
CONTENTS | XI
4.2 (PETRO)CHEMICAL INDUSTRY 302
4.3 FLUID CATALYTIC CRACKING 302
4.3.1 FEEDSTOCK 303
4.3.2 REACTIONS/MECHANISM 304
4.3.3 KINETICS/PROCESS VARIABLES 308
4.3.4 CATALYSTS 310
4.3.5 TECHNOLOGY 312
4.4 STEAM REFORMING OF NATURAL GAS 316
4.4.1 GENERAL 316
4.4.2 PROCESS CONDITIONS FOR SULFUR REMOVAL AND PRIMARY REFORMING 319
4.4.3 KINETICS AND MECHANISM 320
4.4.4 TECHNOLOGY 323
4.4.5 CATALYSTS 325
4.5 AMMONIA SYNTHESIS 328
4.5.1 GENERAL 328
4.5.2 THERMODYNAMICS 329
4.5.3 KINETICS 330
4.5.4 CATALYSTS 333
4.5.5 REACTORS AND PROCESS DESIGN 337
4.6 PHTHALIC ANHYDRIDE SYNTHESIS 340
4.6.1 FEEDSTOCK 340
4.6.2 THERMODYNAMICS 341
4.6.3 MECHANISM 343
4.6.4 CATALYST 344
4.6.5 KINETICS 346
4.6.6 TECHNOLOGY, REACTION AND SEPARATION 346
REFERENCES 350
ACKNOWLEDGEMENT 353
RECOMMENDED READING 355
INDEX 359
/
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| author | Murzin, Dmitry 1963- |
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| discipline | Chemie / Pharmazie Physik Chemie Chemie-Ingenieurwesen |
| format | Book |
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| indexdate | 2024-07-10T00:39:01Z |
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| isbn | 9783110283365 |
| language | English |
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| physical | XI, 364 S. Ill., graph. Darst. |
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| spelling | Murzin, Dmitry 1963- Verfasser (DE-588)1035482452 aut Engineering catalysis Dmitry Yu. Murzin Berlin [u.a.] De Gruyter 2013 XI, 364 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier De Gruyter graduate Katalysator (DE-588)4029919-3 gnd rswk-swf Heterogene Katalyse (DE-588)4123377-3 gnd rswk-swf Technische Chemie (DE-588)4078178-1 gnd rswk-swf Catalysis Catalysis / Industrial applications Chemical reactors Chemical engineering Technische Chemie (DE-588)4078178-1 s Heterogene Katalyse (DE-588)4123377-3 s Katalysator (DE-588)4029919-3 s DE-604 Erscheint auch als Online-Ausgabe 978-3-11-028337-2 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026052462&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Murzin, Dmitry 1963- Engineering catalysis Katalysator (DE-588)4029919-3 gnd Heterogene Katalyse (DE-588)4123377-3 gnd Technische Chemie (DE-588)4078178-1 gnd |
| subject_GND | (DE-588)4029919-3 (DE-588)4123377-3 (DE-588)4078178-1 |
| title | Engineering catalysis |
| title_auth | Engineering catalysis |
| title_exact_search | Engineering catalysis |
| title_full | Engineering catalysis Dmitry Yu. Murzin |
| title_fullStr | Engineering catalysis Dmitry Yu. Murzin |
| title_full_unstemmed | Engineering catalysis Dmitry Yu. Murzin |
| title_short | Engineering catalysis |
| title_sort | engineering catalysis |
| topic | Katalysator (DE-588)4029919-3 gnd Heterogene Katalyse (DE-588)4123377-3 gnd Technische Chemie (DE-588)4078178-1 gnd |
| topic_facet | Katalysator Heterogene Katalyse Technische Chemie |
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