From supramolecular self-assembly to two-dimensional covalent organic frameworks:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
2012
|
| Schlagworte: | |
| Online-Zugang: | kostenfrei http://d-nb.info/1034813374/34 https://nbn-resolving.org/urn:nbn:de:bvb:19-156623 Inhaltsverzeichnis |
| Beschreibung: | 172 Blatt Ill., graph. Darst. |
Internformat
MARC
| LEADER | 00000nam a2200000zc 4500 | ||
|---|---|---|---|
| 001 | BV041073611 | ||
| 003 | DE-604 | ||
| 005 | 20130621 | ||
| 007 | t | ||
| 008 | 130606s2012 gw ad|| m||| 00||| eng d | ||
| 015 | |a 13,O06 |2 dnb | ||
| 016 | 7 | |a 1034813374 |2 DE-101 | |
| 035 | |a (OCoLC)854723470 | ||
| 035 | |a (DE-599)DNB1034813374 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
| 041 | 0 | |a eng | |
| 044 | |a gw |c XA-DE-BY | ||
| 049 | |a DE-12 |a DE-384 |a DE-473 |a DE-703 |a DE-1051 |a DE-824 |a DE-29 |a DE-91 |a DE-19 |a DE-1049 |a DE-92 |a DE-739 |a DE-898 |a DE-355 |a DE-706 |a DE-20 |a DE-1102 | ||
| 084 | |a 540 |2 sdnb | ||
| 100 | 1 | |a Dienstmaier, Jürgen |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a From supramolecular self-assembly to two-dimensional covalent organic frameworks |c Jürgen Dienstmaier |
| 264 | 1 | |c 2012 | |
| 300 | |a 172 Blatt |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |a München, Univ., Diss., 2013 | ||
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe |o urn:nbn:de:bvb:19-156623 |
| 856 | 4 | 1 | |u http://edoc.ub.uni-muenchen.de/15662/ |x Verlag |z kostenfrei |3 Volltext |
| 856 | 4 | |u http://d-nb.info/1034813374/34 |x Langzeitarchivierung Nationalbibliothek | |
| 856 | 4 | |u https://nbn-resolving.org/urn:nbn:de:bvb:19-156623 |x Resolving-System | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026050530&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 912 | |a ebook | ||
| 999 | |a oai:aleph.bib-bvb.de:BVB01-026050530 | ||
Datensatz im Suchindex
| _version_ | 1804150440632254464 |
|---|---|
| adam_text | IMAGE 1
CONTENTS
ABSTRACT 3
ABBREVIATIONS 7
1. INTRODUCTION 8
2. EXPERIMENTAL METHODS AND MATERIALS 11
2.1. EXPERIMENTAL METHODS 11
2.1.1. SCANNING TUNNELING MICROSCOPE (STM) 11
2.1.1.1. THEORETICAL BACKGROUND 14
2.1.1.2. IMAGING WITH STM 19
2.1.2. SPECTROSCOPY 20
2.1.2.1. ULTRAVIOLET AND VISIBLE (UV-VIS) ABSORPTION SPECTROSCOPY 20
2.1.2.2. X-RAY PHOTOELECTRON SPECTROSCOPY 22
2.1.2.3. RAMAN SPECTROSCOPY 23
2.1.3. POWDER X-RAY DIFFRACTION (PXRD) 25
2.1.4. THERMOGRAVIMETRIC ANALYSIS (TGA) 26
2.2. MATERIALS 27
2.2.1. CHOICE O F SUBSTRATE 27
2.2.2. SOLVENTS 27
2.2.3. MOLECULAR BUILDING BLOCKS 28
3. SUPRAMOLECULAR SELF-ASSEMBLY ON SURFACES 29
3.1. THERMODYNAMICS 30
3.2. PARAMETERS AFFECTING SUPRAMOLECULAR SELF-ASSEMBLY ON SURFACES 33
3.2.1. MOLECULAR STRUCTURE 33
3.2.2. INTERMOLECULAR FORCES 34
3.2.3. INFLUENCE O F THE SOLVENT 37
3.2.4. CONCENTRATION EFFECTS 40
3.2.5. GUEST MOLECULES 46
3.3. SUMMARY 47
4. COVALENT BOND FORMATION ON SURFACES 49
4.1. SYNTHESIS O F SURFACE SUPPORTED 2D COFS 49
4.2. MOLECULAR PRECURSOR 51
4.3. SYNTHESIS O F WELL-ORDERED COF MONOLAYERS FROM BDBA 52
4.3.1. SYNTHESIS THROUGH PRE-POLYMERIZATION O F PRECURSORS 53
4.3.2. SYNTHESIS VIA DIRECT ON-SURFACE POLYMERIZATION 57
4.4. SYNTHESIS O F ISORETICULAR 2D COFS 57
4.5. ACTIVATION TEMPERATURE FOR SELF-CONDENSATION 59
4.6. FROM SUPRAMOLECULAR SELF-ASSEMBLY TO 2D COF 60
4.7. STABILITY O F THE BOROXINE RING 61
4.8. HETEROMERIC 2D COF VIA BORONIC ESTER FORMATION 62
4.9. SUMMARY 63
5. CONCLUSIONS 65
APPENDIX 1: PREPARATION O F ULTRA FLAT GOLD (111) SURFACES BY PHYSICAL
VAPOR DEPOSITION (PVD) AS SUBSTRATE FOR SUPRAMOLECULAR SELF-ASSEMBLY 68
APPENDIX 2: STEPWISE ASSEMBLY SCHEME AND EVALUATION O F FORMATION
PROBABILITIES FOR TWO DIFFERENT POLYMORPHS FROM THE SAME ADSORBATE 75
5
HTTP://D-NB.INFO/103700549X
IMAGE 2
PUBLICATIONS 80
REFERENCES 158
ACKNOWLEDGEMENTS 171
CURRICULUM VITAE 172
6
|
| any_adam_object | 1 |
| author | Dienstmaier, Jürgen |
| author_facet | Dienstmaier, Jürgen |
| author_role | aut |
| author_sort | Dienstmaier, Jürgen |
| author_variant | j d jd |
| building | Verbundindex |
| bvnumber | BV041073611 |
| collection | ebook |
| ctrlnum | (OCoLC)854723470 (DE-599)DNB1034813374 |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01652nam a2200385zc 4500</leader><controlfield tag="001">BV041073611</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20130621 </controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">130606s2012 gw ad|| m||| 00||| eng d</controlfield><datafield tag="015" ind1=" " ind2=" "><subfield code="a">13,O06</subfield><subfield code="2">dnb</subfield></datafield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">1034813374</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)854723470</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)DNB1034813374</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakddb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="044" ind1=" " ind2=" "><subfield code="a">gw</subfield><subfield code="c">XA-DE-BY</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-12</subfield><subfield code="a">DE-384</subfield><subfield code="a">DE-473</subfield><subfield code="a">DE-703</subfield><subfield code="a">DE-1051</subfield><subfield code="a">DE-824</subfield><subfield code="a">DE-29</subfield><subfield code="a">DE-91</subfield><subfield code="a">DE-19</subfield><subfield code="a">DE-1049</subfield><subfield code="a">DE-92</subfield><subfield code="a">DE-739</subfield><subfield code="a">DE-898</subfield><subfield code="a">DE-355</subfield><subfield code="a">DE-706</subfield><subfield code="a">DE-20</subfield><subfield code="a">DE-1102</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">540</subfield><subfield code="2">sdnb</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Dienstmaier, Jürgen</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">From supramolecular self-assembly to two-dimensional covalent organic frameworks</subfield><subfield code="c">Jürgen Dienstmaier</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="c">2012</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">172 Blatt</subfield><subfield code="b">Ill., graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="502" ind1=" " ind2=" "><subfield code="a">München, Univ., Diss., 2013</subfield></datafield><datafield tag="655" ind1=" " ind2="7"><subfield code="0">(DE-588)4113937-9</subfield><subfield code="a">Hochschulschrift</subfield><subfield code="2">gnd-content</subfield></datafield><datafield tag="776" ind1="0" ind2="8"><subfield code="i">Erscheint auch als</subfield><subfield code="n">Online-Ausgabe</subfield><subfield code="o">urn:nbn:de:bvb:19-156623</subfield></datafield><datafield tag="856" ind1="4" ind2="1"><subfield code="u">http://edoc.ub.uni-muenchen.de/15662/</subfield><subfield code="x">Verlag</subfield><subfield code="z">kostenfrei</subfield><subfield code="3">Volltext</subfield></datafield><datafield tag="856" ind1="4" ind2=" "><subfield code="u">http://d-nb.info/1034813374/34</subfield><subfield code="x">Langzeitarchivierung Nationalbibliothek</subfield></datafield><datafield tag="856" ind1="4" ind2=" "><subfield code="u">https://nbn-resolving.org/urn:nbn:de:bvb:19-156623</subfield><subfield code="x">Resolving-System</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">DNB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026050530&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="912" ind1=" " ind2=" "><subfield code="a">ebook</subfield></datafield><datafield tag="999" ind1=" " ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-026050530</subfield></datafield></record></collection> |
| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV041073611 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T00:38:58Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-026050530 |
| oclc_num | 854723470 |
| open_access_boolean | 1 |
| owner | DE-12 DE-384 DE-473 DE-BY-UBG DE-703 DE-1051 DE-824 DE-29 DE-91 DE-BY-TUM DE-19 DE-BY-UBM DE-1049 DE-92 DE-739 DE-898 DE-BY-UBR DE-355 DE-BY-UBR DE-706 DE-20 DE-1102 |
| owner_facet | DE-12 DE-384 DE-473 DE-BY-UBG DE-703 DE-1051 DE-824 DE-29 DE-91 DE-BY-TUM DE-19 DE-BY-UBM DE-1049 DE-92 DE-739 DE-898 DE-BY-UBR DE-355 DE-BY-UBR DE-706 DE-20 DE-1102 |
| physical | 172 Blatt Ill., graph. Darst. |
| psigel | ebook |
| publishDate | 2012 |
| publishDateSearch | 2012 |
| publishDateSort | 2012 |
| record_format | marc |
| spelling | Dienstmaier, Jürgen Verfasser aut From supramolecular self-assembly to two-dimensional covalent organic frameworks Jürgen Dienstmaier 2012 172 Blatt Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier München, Univ., Diss., 2013 (DE-588)4113937-9 Hochschulschrift gnd-content Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:19-156623 http://edoc.ub.uni-muenchen.de/15662/ Verlag kostenfrei Volltext http://d-nb.info/1034813374/34 Langzeitarchivierung Nationalbibliothek https://nbn-resolving.org/urn:nbn:de:bvb:19-156623 Resolving-System DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026050530&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Dienstmaier, Jürgen From supramolecular self-assembly to two-dimensional covalent organic frameworks |
| subject_GND | (DE-588)4113937-9 |
| title | From supramolecular self-assembly to two-dimensional covalent organic frameworks |
| title_auth | From supramolecular self-assembly to two-dimensional covalent organic frameworks |
| title_exact_search | From supramolecular self-assembly to two-dimensional covalent organic frameworks |
| title_full | From supramolecular self-assembly to two-dimensional covalent organic frameworks Jürgen Dienstmaier |
| title_fullStr | From supramolecular self-assembly to two-dimensional covalent organic frameworks Jürgen Dienstmaier |
| title_full_unstemmed | From supramolecular self-assembly to two-dimensional covalent organic frameworks Jürgen Dienstmaier |
| title_short | From supramolecular self-assembly to two-dimensional covalent organic frameworks |
| title_sort | from supramolecular self assembly to two dimensional covalent organic frameworks |
| topic_facet | Hochschulschrift |
| url | http://edoc.ub.uni-muenchen.de/15662/ http://d-nb.info/1034813374/34 https://nbn-resolving.org/urn:nbn:de:bvb:19-156623 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=026050530&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT dienstmaierjurgen fromsupramolecularselfassemblytotwodimensionalcovalentorganicframeworks |