Microwaves in nanoparticle synthesis: fundamentals and applications
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim, Bergstr
Wiley-VCH
2013
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XV, 332 S. Ill., graph. Darst. 240 mm x 170 mm |
| ISBN: | 3527331972 9783527331970 |
Internformat
MARC
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| 245 | 1 | 0 | |a Microwaves in nanoparticle synthesis |b fundamentals and applications |
| 264 | 1 | |a Weinheim, Bergstr |b Wiley-VCH |c 2013 | |
| 300 | |a XV, 332 S. |b Ill., graph. Darst. |c 240 mm x 170 mm | ||
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Datensatz im Suchindex
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| adam_text | IMAGE 1
CONTENTS
PREFACE X I
LIST O F CONTRIBUTORS X I I I
1 INTRODUCTION TO NANOPARTICLES 1
SATOSHI HORIKOSHI AND NICK SERPONE 1.1 GENERAL INTRODUCTION TO
NANOPARTICLES 1 1.2 METHODS O F NANOPARTICLE SYNTHESIS 8 1.3 SURFACE
PLASMON RESONANCE AND COLORING 10 1.4 CONTROL O F SIZE, SHAPE, AND
STRUCTURE 12 1.4.1 SIZE CONTROL O F NANOPARTICLES 12 1.4.2 SHAPE CONTROL
O F NANOPARTICLES 15
1.4.3 STRUCTURE CONTROL O F NANOPARTICLES 17 1.5 REDUCING AGENT IN
NANOPARTICLE SYNTHESIS 18 1.6 APPLICATIONS O F METALLIC NANOPARTICLES 19
1.6.1 APPLICATION O F NANOPARTICLES IN PAINTS 20 1.6.2 APPLICATION IN
CHEMICAL CATALYSIS 20 1.6.3 APPLICATION O F NANOPARTICLES IN
MICRO-WIRING 22 1.6.4 APPLICATION O F NANOPARTICLES IN MEDICAL
TREATMENTS 22
REFERENCES 23
2 GENERAL FEATURES O F MICROWAVE CHEMISTRY 25 SATOSHI HORIKOSHI AND NICK
SERPONE 2.1 MICROWAVE HEATING 25
2.2 SOME APPLICATIONS O F MICROWAVE HEATING 26 2.3 MICROWAVE CHEMISTRY
29 2.3.1 MICROWAVES IN ORGANIC SYNTHESES 29 2.3.2 MICROWAVES IN POLYMER
SYNTHESES 30 2.3.3 MICROWAVES IN INORGANIC SYNTHESES 31 2.3.4 MICROWAVE
EXTRACTION 32 2.3.5 MICROWAVE DISCHARGE ELECTRODELESS LAMPS 32 2.4
MICROWAVE CHEMICAL REACTION EQUIPMENT 33
REFERENCES 36
HTTP://D-NB.INFO/1026137330
IMAGE 2
V I CONTENTS
3 CONSIDERATIONS O F MICROWAVE HEATING 39
SATOSHI HORIKOSHI AND NICK SERPONE 3.1 GENERAL CONSIDERATIONS O F
MICROWAVE HEATING 39
3.1.1 ELECTROMAGNETIC WAVES AND A DIELECTRIC MATERIAL 39 3.1.2 HEATING A
SUBSTANCE BY THE MICROWAVES ALTERNATING ELECTRIC FIELD 40 3.1.3 HEATING
A DIELECTRIC BY THE MICROWAVES ALTERNATING MAGNETIC FIELD 45 3.1.4
PENETRATION DEPTH O F MICROWAVES IN A DIELECTRIC MATERIAL 45
3.1.5 FREQUENCY EFFECTS IN CHEMICAL REACTIONS 46 3.2 PECULIAR MICROWAVE
HEATING 47 3.2.1 SPECIAL TEMPERATURE DISTRIBUTION 47 3.2.2 SUPERHEATING
49
3.2.3 SELECTIVE HEATING IN CHEMICAL REACTIONS 50 3.3 RELEVANT POINTS O F
EFFECTIVE MICROWAVE HEATING 52 REFERENCES 53
4 COMBINED ENERGY SOURCES IN THE SYNTHESIS O F NANOMATERIALS 55 LUISA
BOFFA, SILVIA TAGLIAPIETRA, AND CIANCARLO CRAVOTTO 4.1 INTRODUCTION 55
4.2 SIMULTANEOUS ULTRASOUND/MICROWAVE TREATMENTS 58 4.3 SEQUENTIAL
ULTRASOUND AND MICROWAVES 63 4.3.1 SEQUENTIAL STEPS O F THE SAME
REACTION 63 4.3.2 SEQUENTIAL REACTIONS 69 4.4 CONCLUSIONS 72
REFERENCES 72
5 NANOPARTICLE SYNTHESIS THROUGH MICROWAVE HEATING 75 SATOSHI HORIKOSHI
AND NICK SERPONE 5.1 INTRODUCTION 75
5.2 MICROWAVE FREQUENCY EFFECTS 76 5.2.1 SYNTHESIS O F AG NANOPARTICLES
THROUGH THE EFFICIENT USE O F 5.8-GHZ MICROWAVES 77 5.2.2 METAL
NANOPARTICLE SYNTHESIS THROUGH THE USE O F 915-MHZ
MICROWAVES 79 5.3 NANOPARTICLE SYNTHESIS UNDER A MICROWAVE MAGNETIC
FIELD 81 5.4 SYNTHESIS OF METAL NANOPARTICLES BY A GREENER MICROWAVE
HYDROTHERMAL
METHOD 84
5.5 NANOPARTICLE SYNTHESIS WITH MICROWAVES UNDER COOLING CONDITIONS 85
5.6 POSITIVE ASPECTS OF MICROWAVES THERMAL DISTRIBUTION IN NANOPARTICLE
SYNTHESIS 87 5.7 MICROWAVE-ASSISTED NANOPARTICLE SYNTHESIS IN CONTINUOUS
FLOW
APPARATUSES 90 5.7.1 MICROWAVE DESKTOP SYSTEM OF NANOPARTICLE SYNTHESIS
IN A CONTINUOUS FLOW REACTOR 91 5.7.2 SYNTHESIS O F METAL NANOPARTICLES
WITH A HYBRID MICROREACTOR/MICROWAVE
SYSTEM 92
IMAGE 3
CONTENTS J V I I
5.7.3 OTHER EXAMPLES O F CONTINUOUS MICROWAVE NANOPARTICLE SYNTHESIS
EQUIPMENT 94 5.7.4 MICROWAVE CALCINATION EQUIPMENT FOR THE FABRICATION O
F NANOMETALLIC INKS 95
5.7.5 SYNTHESIS O F METAL NANOPARTICLE USING MICROWAVE LIQUID PLASMA 96
5.7.6 COMPENDIUM O F MICROWAVE-ASSISTED NANOPARTICLE SYNTHESES 96
REFERENCES 103
6 MICROWAVE-ASSISTED SOLUTION SYNTHESIS O F NANOMATERIALS 107 XIANLUO HU
AND J I M M Y C. YU 6.1 INTRODUCTION 207
6.2 SYNTHESIS O F ZNO NANOCRYSTALS 110 6.2.1 SYNTHESIS O F COLLOIDAL ZNO
NANOCRYSTALS CLUSTERS 111 6.2.2 CONTROLLED GROWTH OF BASIC AND COMPLEX
ZNO NANOSTRUCTURES 113 6.2.3 SYNTHESIS O F ZNO NANOPARTICLES IN BENZYL
ALCOHOL 113 6.3 SYNTHESIS O F A-FE 2 0 3 NANOSTRUCTURES 114 6.3.1 A-FE 2
0 3 HOLLOW SPHERES 115 6.3.2 MONODISPERSE A-FE 2 0 3 NANOCRYSTALS WITH
CONTINUOUS ASPECT-RATIO
TUNING AND PRECISE SHAPE CONTROL 116 6.3.3 SELF-ASSEMBLED HIERARCHICAL
A-FE 2 0 3 NANOARCHITECTURES 118 6.4 ELEMENT-BASED NANOSTRUCTURES AND
NANOCOMPOSITE 118 6.4.1 SILVER NANOSTRUCTURES 118 6.4.2 TE
NANOSTRUCTURES 122 6.4.3 SELENIUM/CARBON COLLOIDS 123 6.5 CHALCOGENIDE
NANOSTRUCTURES 125 6.5.1 CADMIUM CHALCOGENIDES 125 6.5.2 LEAD
CHALCOGENIDES 129
6.5.3 ZINC CHALCOGENIDES 131 6.6 GRAPHENE 132
6.7 SUMMARY 135
REFERENCES 135
7 PRECISELY CONTROLLED SYNTHESIS O F METAL NANOPARTICLES UNDER MICROWAVE
IRRADIATION 145 ZHI CHEN, DAI MOCHIZUKI, AND YUJI WADA
7.1 INTRODUCTION 145
7.1.1 GENERAL INTRODUCTION-GREEN CHEMISTRY 145 7.1.2 MICROWAVE CHEMISTRY
FOR THE PREPARATION O F METAL NANOPARTICLES 147 7.2 PRECISE CONTROL O F
SINGLE COMPONENT UNDER MICROWAVE
IRRADIATION 152 7.2.1 SPHERES 152
7.2.1.1 AU NANOPARTICLES 152 7.2.1.2 AG NANOPARTICLES 154 7.2.1.3 PT
NANOPARTICLES 156
IMAGE 4
V I I I J CONTENTS
7.2.1.4 PD, RU, AND RH NANOPARTICLES 157
7.2.1.5 OTHER TRANSITION METALS 158 7.2.2 NANORODS AND NANOWIRES 160
7.2.2.1 AG NANORODS AND NANOWIRES 160 7.2.2.2 AU, PT, NI NANORODS AND
NANOWIRES 161 7.2.3 OTHER MORPHOLOGIES 162 7.2.3.1 AU 162 7.2.3.2 AG 163
7.2.3.3 PT, PD, NI, AND CO 163 7.3 PRECISE CONTROL O F MULTICOMPONENT
STRUCTURES UNDER MICROWAVE
IRRADIATION 164 7.3.1 MULTICOMPONENT NANOPARTICLES 164 7.3.1.1
CORE-SHELL STRUCTURES 164 7.3.1.2 ALLOYS 168 7.3.2 METAL NANOPARTICLES
ON SUPPORTS 170 7.3.2.1 METAL OXIDE SUPPORTS 170 7.3.2.2 CARBON MATERIAL
SUPPORTS 171 7.3.2.3 OTHER SUPPORTS 176 7.4 AN EXAMPLE OF MASS
PRODUCTION ORIENTED TO APPLICATION 178
7.5 CONCLUSION 180
REFERENCES 180
8 MICROWAVE-ASSISTED NONAQUEOUS ROUTES TO METAL OXIDE NANOPARTICLES AND
NANOSTRUCTURES 185 MARKUS NIEDERBERGER 8.1 INTRODUCTION 185
8.2 NONAQUEOUS SOL-GEL CHEMISTRY 186 8.3 POLYOL ROUTE 189
8.4 BENZYL ALCOHOL ROUTE 191 8.5 OTHER MONO-ALCOHOLS 197 8.6 IONIC
LIQUIDS 198
8.7 NONAQUEOUS MICROWAVE CHEMISTRY BEYOND METAL OXIDES 199 8.8 SUMMARY
AND OUTLOOK 201
REFERENCES 202
9 INPUT OF MICROWAVES FOR NANOCRYSTAL SYNTHESIS AND SURFACE
FUNCTIONALIZATION FOCUS ON IRON OXIDE NANOPARTICLES 207 IRENA MILOSEVIC,
ERWANN CUENIN, YOANN LALATONNE, FARAH BENYETTOU, CAROLINE DE
MONTFERRAND, FREDERIC CEINGUENAUD, AND LAURENCE MOTTE 9.1 INTRODUCTION
207
9.2 BIOMEDICAL APPLICATIONS OF IRON OXIDE NANOPARTICLES 208 9.3
NANOPARTICLE SYNTHESIS 211 9.3.1 SYNTHESIS IN AQUEOUS SOLUTION 211
9.3.1.1 COPRECIPITATION METHOD 211 9.3.1.2 FORCED HYDROLYSIS 211
IMAGE 5
CONTENTS I X
9.3.1.3 HYDROTHERMAL METHOD 212
9.3.1.4 AQUEOUS SOL-GEL METHOD 212 9.3.1.5 DIRECT MICELLES MICROEMULSION
METHOD 212 9.3.2 SYNTHESIS IN NON-AQUEOUS SOLVENT 213 9.3.2.1 REVERSE
MICELLE MICROEMULSION METHOD 213 9.3.2.2 NON-AQUEOUS SOL-GEL METHOD 213
9.3.2.3 POLYOL SYNTHESIS 213 9.3.2.4 THERMAL DECOMPOSITION 214 9.4
NANOPARTICLE SURFACE FUNCTIONALIZATION 214 9.4.1 HYDROPHOBIC
NANOCRYSTALS 215 9.4.1.1 LIGAND EXCHANGE 215 9.4.1.2 SURFACE CHEMICAL
MODIFICATION 236
9.4.1.3 TAILS INTERDIGITATION 216 9.4.1.4 SILICA OR POLYMER SHELL 217
9.4.2 WATER SOLUBLE NANOCRYSTALS 217 9.4.2.1 DIRECT SURFACE
FUNCTIONALIZATION 217 9.4.2.2 TWO-STEP SURFACE FUNCTIONALIZATION 219 9.5
MICROWAVE-ASSISTED CHEMISTRY 222 9.5.1 MICROWAVE-ASSISTED SYNTHESIS O F
NANOPARTICLES 223 9.5.1.1 MICROWAVE-ASSISTED HYDROTHERMAL METHOD 223
9.5.1.2 MICROWAVE-ASSISTED SOLVOTHERMAL METHOD 227 9.5.2
MICROWAVE-ASSISTED FUNCTIONALIZATION O F NANOPARTICLES 229 9.5.2.1 GOLD
NANOPARTICLE MICROWAVE FUNCTIONALIZATION 230 9.5.2.2 IRON OXIDE
NANOPARTICLE MICROWAVE FUNCTIONALIZATION 231 9.5.2.3 MICROWAVE-ASSISTED
SILICA ENCAPSULATION O F IRON OXIDE
NANOPARTICLES 234 9.5.2.4 EUROPIUM OXIDE NANOPARTICLE MICROWAVE
FUNCTIONALIZATION 235 9.6 CONCLUSIONS 236
REFERENCES 236
10 MICROWAVE-ASSISTED CONTINUOUS SYNTHESIS OF INORGANIC NANOMATERIALS
247 NAFTALI N. OPEMBE, HUI HUANG, AND STEVEN L. SUIB 10.1 INTRODUCTION
AND OVERVIEW 247 10.2 MICROWAVE-ASSISTED CONTINUOUS SYNTHESIS O F
INORGANIC
NANOMATERIALS 249 10.3 TYPES O F MICROWAVE APPARATUS USED IN CONTINUOUS
SYNTHESIS 250 10.4 MICROWAVE CONTINUOUS SYNTHESIS O F MOLECULAR SIEVE
MATERIALS 253 10.5 MICROWAVE CONTINUOUS SYNTHESIS O F METAL OXIDES AND
MIXED METAL
OXIDE MATERIALS 259 10.6 MICROWAVE CONTINUOUS SYNTHESIS O F METALLIC
NANOMATERIALS 267 10.7 CONCLUSIONS AND OUTLOOK 268 REFERENCES 269
IMAGE 6
X CONTENTS
11 MICROWAVE PLASMA SYNTHESIS O F NANOPARTIDES: FROM THEORETICAL
BACKGROUND AND EXPERIMENTAL REALIZATION TO NANOPARTIDES WITH SPECIAL
PROPERTIES 271 DOROTHIE VINGA SZABD 11.1 INTRODUCTION 271
11.2 USING MICROWAVE PLASMAS FOR NANOPARTIDE SYNTHESIS 272 11.2.1
GENERAL COMMENTS ON PLASMAS 272 11.2.2 CONSIDERATIONS IN A MICROWAVE
PLASMA 274 11.2.3 PARTICLE FORMATION 277 11.2.4 CHARACTERIZATION OF
NANOPARTIDES 278 11.3 EXPERIMENTAL REALIZATION O F THE MICROWAVE PLASMA
SYNTHESIS 279 11.3.1 CUSTOM-MADE APPLICATORS 279 11.3.2 COATED
NANOPARTIDES AND PARTICLE COLLECTION 280 11.4 INFLUENCE O F EXPERIMENTAL
PARAMETERS 282 11.4.1 PRECURSOR SELECTION 284 11.4.2 INFLUENCE O F
PRECURSOR CONCENTRATION 287
11.4.3 INTERDEPENDENCE O F MICROWAVE POWER, PRESSURE, TEMPERATURE, AND
GAS VELOCITY 288 11.4.4 INFLUENCE OF RESIDENCE TIME IN THE PLASMA ON
PARTICLE SIZE 292 11.4.5 SUMMARY O F EXPERIMENTAL PARAMETERS 292 11.5
NANOPARTIDE PROPERTIES AND APPLICATION 294 11.5.1 FERRIMAGNETIC
NANOPARTIDES 294 11.5.2 GAS-SENSING NANOPARTIDES 297
11.5.3 NANOPARTIDES FOR ANODES IN LI-ION BATTERIES 299 11.6 SUMMARY 300
REFERENCES 301
12 OXIDATION, PURIFICATION AND FUNCTIONALIZATION O F CARBON NANOTUBES
UNDER MICROWAVE IRRADIATION 311 DAVIDE CARELLA AND CIANCARLO CRAVOTTO
12.1 INTRODUCTION 311
12.2 OXIDATION AND PURIFICATION 313 12.3 FUNCTIONALIZATION 316 12.4
CONCLUSION 321
REFERENCES 321
INDEX 325
|
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| id | DE-604.BV040898334 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T00:34:52Z |
| institution | BVB |
| isbn | 3527331972 9783527331970 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-025877858 |
| oclc_num | 852935784 |
| open_access_boolean | |
| owner | DE-11 DE-M347 |
| owner_facet | DE-11 DE-M347 |
| physical | XV, 332 S. Ill., graph. Darst. 240 mm x 170 mm |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Wiley-VCH |
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| spelling | Microwaves in nanoparticle synthesis fundamentals and applications Weinheim, Bergstr Wiley-VCH 2013 XV, 332 S. Ill., graph. Darst. 240 mm x 170 mm txt rdacontent n rdamedia nc rdacarrier Nanopartikel (DE-588)4333369-2 gnd rswk-swf Chemische Synthese (DE-588)4133806-6 gnd rswk-swf Mikrowelle (DE-588)4039246-6 gnd rswk-swf Nanopartikel (DE-588)4333369-2 s Chemische Synthese (DE-588)4133806-6 s Mikrowelle (DE-588)4039246-6 s DE-604 Horikoshi, Satoshi (DE-588)1034443054 edt DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025877858&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Microwaves in nanoparticle synthesis fundamentals and applications Nanopartikel (DE-588)4333369-2 gnd Chemische Synthese (DE-588)4133806-6 gnd Mikrowelle (DE-588)4039246-6 gnd |
| subject_GND | (DE-588)4333369-2 (DE-588)4133806-6 (DE-588)4039246-6 |
| title | Microwaves in nanoparticle synthesis fundamentals and applications |
| title_auth | Microwaves in nanoparticle synthesis fundamentals and applications |
| title_exact_search | Microwaves in nanoparticle synthesis fundamentals and applications |
| title_full | Microwaves in nanoparticle synthesis fundamentals and applications |
| title_fullStr | Microwaves in nanoparticle synthesis fundamentals and applications |
| title_full_unstemmed | Microwaves in nanoparticle synthesis fundamentals and applications |
| title_short | Microwaves in nanoparticle synthesis |
| title_sort | microwaves in nanoparticle synthesis fundamentals and applications |
| title_sub | fundamentals and applications |
| topic | Nanopartikel (DE-588)4333369-2 gnd Chemische Synthese (DE-588)4133806-6 gnd Mikrowelle (DE-588)4039246-6 gnd |
| topic_facet | Nanopartikel Chemische Synthese Mikrowelle |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025877858&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT horikoshisatoshi microwavesinnanoparticlesynthesisfundamentalsandapplications |