Crystallization: basic concepts and industrial applications
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2013
|
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis Inhaltsverzeichnis |
| Beschreibung: | XIV, 346 S. Ill., graph. Darst. |
| ISBN: | 9783527327621 9783527650323 |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV040797313 | ||
| 003 | DE-604 | ||
| 005 | 20140213 | ||
| 007 | t | ||
| 008 | 130305s2013 ad|| |||| 00||| eng d | ||
| 015 | |a 12N35 |2 dnb | ||
| 016 | 7 | |a 102527198X |2 DE-101 | |
| 020 | |a 9783527327621 |c : Gb. : ca. EUR 129.00 (DE) |9 978-3-527-32762-1 | ||
| 020 | |a 9783527650323 |c oBook |9 978-3-527-65032-3 | ||
| 035 | |a (OCoLC)830343789 | ||
| 035 | |a (DE-599)DNB102527198X | ||
| 040 | |a DE-604 |b ger |e aacr | ||
| 041 | 0 | |a eng | |
| 049 | |a DE-11 |a DE-91G |a DE-703 |a DE-92 |a DE-83 |a DE-29T |a DE-19 | ||
| 082 | 0 | |a 660.284298 |2 22/ger | |
| 084 | |a UQ 2000 |0 (DE-625)146482: |2 rvk | ||
| 084 | |a UQ 3000 |0 (DE-625)146503: |2 rvk | ||
| 084 | |a VN 7260 |0 (DE-625)147614:253 |2 rvk | ||
| 084 | |a CIT 210f |2 stub | ||
| 084 | |a CHE 192f |2 stub | ||
| 245 | 1 | 0 | |a Crystallization |b basic concepts and industrial applications |c ed. by Wolfgang Beckmann |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2013 | |
| 300 | |a XIV, 346 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 0 | 7 | |a Kristallwachstum |0 (DE-588)4123579-4 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Kristallisation |0 (DE-588)4033215-9 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Kristallzüchtung |0 (DE-588)4140616-3 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4143413-4 |a Aufsatzsammlung |2 gnd-content | |
| 689 | 0 | 0 | |a Kristallisation |0 (DE-588)4033215-9 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a Kristallwachstum |0 (DE-588)4123579-4 |D s |
| 689 | 1 | 1 | |a Kristallzüchtung |0 (DE-588)4140616-3 |D s |
| 689 | 1 | |5 DE-604 | |
| 700 | 1 | |a Beckmann, Wolfgang |d 19XX- |0 (DE-588)1032546824 |4 edt | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, EPUB |z 978-3-527-65034-7 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, MOBI |z 978-3-527-65033-0 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, PDF |z 978-3-527-65035-4 |
| 856 | 4 | |q text/html |u http://deposit.dnb.de/cgi-bin/dokserv?id=4102903&prov=M&dok_var=1&dok_ext=htm |3 Inhaltstext | |
| 856 | 4 | |m DE-601 |q pdf/application |u http://www.gbv.de/dms/bowker/toc/9783527327621.pdf |3 Inhaltsverzeichnis | |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025777483&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-025777483 | |
Datensatz im Suchindex
| _version_ | 1807955329947795456 |
|---|---|
| adam_text |
IMAGE 1
CONTENTS
LIST O F CONTRIBUTORS XIII
1 CRYSTALLIZATION: INTRODUCTION 1
WOLFGANG BECKMANN
2 MECHANISMS O F CRYSTALLIZATION 7
WOLFGANG BECKMANN
2.1 CRYSTAL LATTICE 7
2.1.1 ARRANGEMENT O F BUILDING BLOCKS AND SYMMETRIES 7 2.1.2 UNIT CELL 9
2.1.3 MILLER INDICES TO DESCRIBE CRYSTAL FACES 11 2.1.4 LATTICE DEFECTS
12
2.1.5 EQUILIBRIUM, GROWTH, AND DISSOLUTION FORM OF CRYSTALS 14 2.1.6
MORPHOLOGY AND HABIT 16 2.2 NUCLEATION OF CRYSTALS 17
2.2.1 MECHANISM O F PRIMARY NUCLEATION 18 2.2.2 METASTABLE ZONE AND
INDUCTION TIME FOR NUCLEATION 20 2.2.3 FORM CRYSTALLIZED: OSTWALD'S LAW
O F STAGES 25 2.3 GROWTH AND GROWTH RATE O F CRYSTALS 25
2.3.1 KINK POSITION AND F, S, AND K FACES 26 2.3.2 GROWTH O F IDEAL
CRYSTALS 27 2.3.3 GROWTH O F REAL CRYSTALS 28 2.3.4 TRANSPORT PHENOMENA
32
FURTHER READING 33
3 SOLUBILITY AND SOLUTION EQUILIBRIA IN CRYSTALLIZATION 35 HEIKE LORENZ
3.1 PHASE EQUILIBRIA AND PHASE DIAGRAMS: GENERAL ISSUES 36 3.1.1 PHASES,
PHASE RULE, AND BINARY SYSTEMS 36
3.1.2 MELT AND SOLUTION EQUILIBRIA 38 3.1.3 THERMODYNAMIC DESCRIPTION O
F SLE: LIQUIDUS CURVE IN THE PHASE DIAGRAM 39 3.1.4 PHASE DIAGRAMS O F
TERNARY AND QUATERNARY SYSTEMS 42
HTTP://D-NB.INFO/102527198X
IMAGE 2
V I CONTENTS
3.2 MELT PHASE DIAGRAMS 44
3.2.1 TYPES O F PHASE DIAGRAMS AND THEIR OCCURRENCE 44 3.2.2 MEASUREMENT
OF MELT PHASE DIAGRAMS 46 3.2.2.1 METHODS 46
3.2.2.2 DSC AND HOW TO MEASURE AND INTERPRET DSC DATA 47 3.2.3 EXAMPLE
OF A DIASTEREOMERIC SYSTEM 50 3.3 SOLUTION EQUILIBRIA 53
3.3.1 SOLUBILITY AND CONCENTRATION UNITS 53 3.3.2 SOLUBILITY CURVES OF
INORGANIC AND ORGANIC SUBSTANCES 54 3.3.2.1 INORGANIC SUBSTANCES 55
3.3.2.2 ORGANIC SUBSTANCES 57
3.3.3 SOLVATES, POLYMORPHS, AND COCRYSTALS 58 3.3.4 INFLUENCE OF
SOLVENTS AND IMPURITIES 60 3.3.5 MEASUREMENT OF SOLUBILITIES AND
CORROBORATION 62 3.3.5.1 ENSURING EQUILIBRIUM CONDITIONS 63 3.3.5.2
EXCESS METHOD AS A CLASSICAL ISOTHERMAL METHOD 64 3.3.5.3 POLYTHERMAL
MEASUREMENTS 65 3.3.5.4 PREDICTION AND CORRELATION O F SOLUBILITIES 67
3.3.6 OILING-OUT 68
3.3.7 TERNARY SOLUTION EQUILIBRIA: CASE OF ENANTIOMERS 70 3.3.8
QUATERNARY SYSTEMS: CASE OF RECIPROCAL SALT PAIRS 72 REFERENCES 74
4 AGGLOMERATION DURING CRYSTALLIZATION 75 WOLFGANG BECKMANN 4.1
MECHANISMS AND KINETICS O F AGGLOMERATION 75 4.1.1 PROCESS O F
AGGLOMERATION 75
4.1.2 KINETICS OF AGGLOMERATION 77 4.2 PARAMETERS INFLUENCING
AGGLOMERATION 77 4.3 AGGLOMERATION DURING CRYSTALLIZATION 80 4.3.1
AGGLOMERATION DURING CRYSTALLIZATION 80
4.3.2 SPHERICAL AGGLOMERATION 83 4.4 MECHANICAL PROPERTIES O F
AGGLOMERATES 83 REFERENCES 84
5 POLYMORPHISM O F CRYSTALLINE SYSTEMS 85 ROLF HILFIKER 5.1 INTRODUCTION
AND DEFINITIONS 85
5.2 OCCURRENCE AND PROPERTIES O F POLYMORPHS AND SOLVATES 86 5.3
THERMODYNAMICS O F POLYMORPHS O F SOLID-STATE FORMS 87 5.3.1 BASICS 87
5.3.2 ENERGY-TEMPERATURE DIAGRAMS 88 5.3.3 RULES TO PREDICT
THERMODYNAMIC RELATIONSHIPS 90 5.4 THERMODYNAMICS O F HYDRATES 91
5.5 EXPERIMENTAL TECHNIQUES TO ELUCIDATE THERMODYNAMICS 94
IMAGE 3
CONTENTS I V I I
5.5.1 DSC 94
5.5.2 SUSPENSION EQUILIBRATION 94 5.5.3 SOLUBILITY MEASUREMENTS 95 5.5.4
OTHER METHODS 96
5.6 FORMATION O F VARIOUS POLYMORPHS AND SOLID-STATE FORMS-POLYMORPH
SCREENS 97 5.6.1 PRINCIPLES 97
5.6.2 CRYSTALLIZATION METHODS AND CHOICE OF SOLVENT 99 5.6.3 TYPES OF
POLYMORPH SCREENS 100 5.7 SELECTION O F OPTIMAL FORM FOR DEVELOPMENT 101
SYMBOLS 102
REFERENCES 102
6 THE INFLUENCE O F ADDITIVES AND IMPURITIES ON CRYSTALLIZATION 105
CHRISTIANE SCHMIDT, MATTHEW J.JONES, AND JOACHIM ULRICH 6.1 INFLUENCE OF
ADDITIVES AND IMPURITIES ON CRYSTALLIZATION 105 6.1.1 SOLUBILITY 105
6.1.1.1 COMMON ION EFFECT 106 6.1.1.2 THERMODYNAMIC BASIS OF SOLUBILITY
AND THE INFLUENCE O F ADDITIVES 106 6.1.1.3 COMPLEX FORMATION 106 6.1.2
RATE OF NUCLEATION AND CRYSTAL GROWTH 107 6.1.2.1 NUCLEATION RATES 107
6.1.2.2 CRYSTAL GROWTH RATES 111 6.1.3 HABIT MODIFICATION 114 6.2
INFLUENCE O F IMPURITIES: MODELING 116 6.2.1 CALCULATING CRYSTAL HABIT
116 6.2.1.1 SURFACE ENERGY MODEL 117 6.2.2 MOLECULAR MODELING 118
6.2.3 MODELING O F ADDITIVES 120 6.3 TAILOR-MADE ADDITIVES 122
6.4 MODELING THE INFLUENCE O F SOLVENTS 122 REFERENCES 124
7 PURIFICATION BY CRYSTALLIZATION 129
HEIKE LORENZ AND WOLFGANG BECKMANN 7.1 INTRODUCTION 129
7.2 MECHANISMS O F IMPURITY INCORPORATION AND PURIFICATION 131 7.2.1
SOLUBILITY IN THE SOLID STATE 132 7.2.2 FRACTIONAL CRYSTALLIZATION 133
7.2.3 INCLUSION AND SURFACE ADSORPTION O F IMPURITIES 134
7.2.4 INFLUENCE O F CRYSTALLIZATION CONDITIONS 136 7.2.4.1 PRODUCT YIELD
136 7.2.4.2 CRYSTALLIZATION TECHNIQUE AND RATE OF CRYSTALLIZATION 137
7.2.4.3 SOLVENT APPLIED 139
7.2.4.4 MIXING 142
IMAGE 4
V I I I I CONTENTS
7.2.5 DOWNSTREAM PROCESSES 142
7.2.5.1 SOLID-LIQUID SEPARATION AND SWEATING 143 7.2.5.2 RESLURRYING AND
WASHING 144 7.2.6 WORKFLOW TO "MANAGE" IMPURITIES IN PROCESS DEVELOPMENT
146 REFERENCES 147
8 CHARACTERIZATION O F CRYSTALLINE PRODUCTS 149 ROLF HILFIKER 8.1
INTRODUCTION 149
8.2 CHARACTERIZATION O F INTRINSIC PROPERTIES O F A SOLID 149 8.2.1
CRYSTAL STRUCTURE 150
8.2.1.1 X-RAY POWDER DIFFRACTION (XRPD) 150 8.2.1.2 VIBRATIONAL
SPECTROSCOPY (RAMAN, IR, NIR, THZ) 151 8.2.1.3 SOLID-STATE NMR (SSNMR)
152 8.2.2 THERMODYNAMIC PROPERTIES 154 8.2.2.1 DIFFERENTIAL SCANNING
CALORIMETRY (DSC) 154 8.2.2.2 ISOTHERMAL MICROCALORIMETRY 157 8.2.3
COMPOSITION 158
8.2.3.1 THEMOGRAVIMETRY (TG, TG-FTIR, AND TG-MS) 158 8.2.3.2 DYNAMIC
VAPOR SORPTION (DVS) 158 8.3 CHARACTERIZATION OF PARTICLE SHAPE AND SIZE
161 8.3.1 PARTICLE SIZE DISTRIBUTION: CHARACTERISTIC VALUES AND GRAPHS
161 8.3.2 OVERVIEW OF AVAILABLE METHODS 162 8.3.2.1 MICROSCOPY 163
8.3.2.2 LASER LIGHT DIFFRACTION 163 8.3.2.3 SIEVING 165
8.4 POWDER FLOW PROPERTIES 165
8.5 IN-PROCESS CHARACTERIZATION 167 8.5.1 TURBIDITY 167
8.5.2 RAMAN 168
8.5.3 FBRM AND PVM 169
REFERENCES 171
9 BASICS O F INDUSTRIAL CRYSTALLIZATION FROM SOLUTION 173 WOLFGANG
BECKMANN 9.1 GENERATION O F SUPERSATURATION I N A CRYSTALLIZER 173 9.2
MASS AND POPULATION BALANCE FOR GROWTH FROM SUSPENSION 176 9.2.1 MASS
BALANCE 176
9.2.2 POPULATION BALANCE 176 9.3 OPERATION OF A CONTINUOUS CRYSTALLIZER:
BASICS 178 9.3.1 CONCEPT AND DESIGN O F CONTINUOUS CRYSTALLIZERS 178
9.3.2 MASS BALANCE IN A CONTINUOUS CRYSTALLIZER 178 9.3.3 POPULATION
BALANCE IN A CONTINUOUS CRYSTALLIZER 178 9.3.4 MEAN PARTICLE SIZE 180
9.3.5 SECONDARY NUCLEATION 180
IMAGE 5
CONTENTS I X
9.4 OPERATION OF A BATCH CRYSTALLIZER: BASICS 183
9.4.1 CONCEPT AND DESIGN O F BATCH CRYSTALLIZERS 183 9.4.2 MASS AND
POPULATION BALANCE IN A BATCH CRYSTALLIZER 184
10 DEVELOPMENT O F BATCH CRYSTALLIZATIONS 187 DIERK WIECKHUSEN 10.1
SETTING GOALS 187
10.2 CRYSTALLIZATION O F ORGANIC MOIETIES 188 10.3 GENERATION O F
SUPERSATURATION IN BATCH CRYSTALLIZATIONS 189 10.3.1 COOLING 189
10.3.2 USE O F ANTISOLVENT 190 * 10.3.3 EVAPORATION 191 10.4 INITIATION
O F CRYSTALLIZATION - NUCLEATION PHASE 192 10.5 SEEDED BATCH
CRYSTALLIZATIONS 193 10.5.1 SEEDING STRATEGY 194 10.5.2 DESIGNING A
SEEDING PROCESS 194 10.5.2.1 QUALITY O F SEEDS 195 10.5.2.2 QUANTITY OF
SEEDS 195 10.5.2.3 PREPARATION O F SEEDS 196 10.5.2.4 SUPERSATURATION AT
THE START O F CRYSTALLIZATION 197 10.5.2.5 HOLDING TIME AFTER SEEDING
197 10.6 CRYSTALLIZATION PERIOD 197 10.7 SCALE-UP CONSIDERATIONS 198
10.7.1 PROCESS TIME - RATE OF CRYSTALLIZATION 198 10.7.2 STIRRING 199
10.7.3 OPERATIONAL ASPECTS 200 10.8 MANIPULATING PARTICLE SHAPE 201
11 CONTINUOUS CRYSTALLIZATION 203 C'UNTER HOFMANN AND CHRISTIAN MELCHES
11.1 CONCEPT AND DESIGN OF CONTINUOUS CRYSTALLIZERS 204 11.1.1
IMPORTANCE O F SECONDARY NUCLEATION 204 11.1.2 CONTROL OF
SUPERSATURATION 205 11.1.3 ADJUSTMENT O F THE GRANULOMETRY - MEAN
CRYSTAL SIZE AND CRYSTAL SIZE
DISTRIBUTION 209
11.1.4 ENERGY INPUT AND RETENTION TIME 212 11.1.5 WHICH TYPE OF
CRYSTALLIZER TO SELECT? 215 11.1.6 SEEDING O F DTB AND OSLO
CRYSTALLIZERS 216 11.2 VARIOUS CONTINUOUS CRYSTALLIZERS 218
11.2.1 FC GROUP 218
11.2.2 DTB GROUP 220
11.2.3 GROUP OF FLUIDIZED BED CRYSTALLIZERS 222 11.2.4 COMMENTS ON
POPULATION BALANCE AND MODELING 223 11.2.5 MANIPULATION O F CRYSTAL SIZE
DISTRIBUTIONS 225 11.3 PERIPHERY 226
IMAGE 6
X I CONTENTS
11.4 SPECIAL FEATURES OF THE PROCESS 229
11.4.1 SURFACE COOLING CRYSTALLIZATION 229 11.4.2 VACUUM COOLING
CRYSTALLIZATION 230 11.4.3 VACUUM EVAPORATION CRYSTALLIZATION 230 11.5
ADJUSTMENT OF SUSPENSION DENSITIES 232
REFERENCES 233
12 PRECIPITATION 235
WOLFGANG BECKMANN
12.1 PRECIPITATION FROM SOLUTION BY MIXING TWO STREAMS 235 12.1.1
DEVICES AND MIXING SCHEMES 235 12.2 SEMI-BATCH PRECIPITATIONS 236 12.3
MODEL O F MIXING DURING PRECIPITATION 238 12.4 PRECIPITATIONS USING
SUPERCRITICAL FLUIDS 239 12.5 CRYSTAL ISSUES 241
12.5.1 POLYMORPHISM O F PRECIPITATES 241 12.5.2 CRYSTAL PERFECTION 243
12.5.3 AGGLOMERATION 244 12.6 PARTICLE SIZE AS A FUNCTION O F OPERATING
CONDITIONS 244
13 MIXING IN CRYSTALLIZATION PROCESSES 247 BERND NIENHAUS 13.1 MIXING IN
BATCH AND CONTINUOUS CRYSTALLIZATION PROCESSES 247 13.2 BASIC MIXING
TASKS - MIXING TASKS IN CRYSTALLIZATION 248 13.3 IMPELLERS AND AGITATION
SYSTEMS 249
13.3.1 GENERAL OVERVIEW AND SELECTION CRITERIA 250 13.3.2 AXIAL
IMPELLERS 250 13.3.2.1 PROPELLER 250 13.3.2.2 PITCHED BLADE TURBINE 250
13.3.2.3 HELICAL RIBBON IMPELLER 252 13.3.3 RADIAL IMPELLERS 252
13.3.3.1 FLAT BLADE DISK TURBINE 252 13.3.3.2 DISPERSER DISK 252
13.3.4 TANGENTIAL IMPELLERS 253 13.4 POWER CONSUMPTION OF AN IMPELLER
SYSTEM [2] 253 13.4.1 DIAMETER RATIO 255 13.4.2 BOTTOM CLEARANCE 256
13.4.3 FILLING LEVEL 256 13.4.4 MULTISTAGE IMPELLERS 256 13.5 BLENDING
256
13.5.1 DEGREE OF HOMOGENEITY 256 13.5.2 TURBULENT BLENDING 257 13.5.3
SIGNIFICANCE OF CIRCULATION RATE 258 13.5.4 LAMINAR BLENDING 258
13.6 SUSPENDING 259
IMAGE 7
CONTENTS X I
13.6.1 SUSPENDING CRITERIA AND DIFFERENT STATES OF SUSPENSION 259
13.6.2 POWER REQUIREMENT FOR THE SUSPENSION OF SOLIDS 262 13.6.3 MODELS
AND MECHANISMS FOR THE SUSPENSION OF SOLIDS 263 13.6.4 DETERMINATION O F
THE SHAFT SPEED NECESSARY FOR SUSPENDING 264 13.6.4.1 PHYSICAL
PARAMETERS O F LIQUIDS AND SOLIDS 265 13.6.4.2 SOLIDS CONCENTRATION 265
13.6.4.3 GEOMETRY 266 13.6.5 DISTRIBUTION O F SOLIDS 266 13.6.6
INFLUENCE ON MASS TRANSFER 267 13.6.7 INFLUENCE ON BLEND TIMES 267 13.7
SCALE-UP OF A CRYSTALLIZATION PROCESS 268 13.7.1 MODEL TESTS 269
13.7.2 "SCALE-UP" RULES 270 13.7.3 BLENDING 270
13.7.4 SUSPENSION 270
13.7.5 DISPERSING 271
13.7.6 HEAT TRANSFER 272
13.7.7 SPECIAL SCALE-UP CONSIDERATIONS 272 13.7.8 SUMMARY 273
REFERENCES 273
14 DOWNSTREAM PROCESSES 275
DIERK WIECKHUSEN AND WOLFGANG BECKMANN 14.1 TRANSFER O F SUSPENSION AND
FILTER CAKE 275 14.2 SOLID-LIQUID SEPARATION 275 14.2.1 CAKE FORMING
FILTRATION 276 14.2.2 CENTRIFUGATION 277 14.2.3 CHARACTERIZATION O F
FILTERABILITY IN THE LABORATORY 277 14.2.4 IMPROVING FILTERABILITY 278
14.2.5 WASHING 280
14.3 DRYING 280
14.3.1 PHASES O F THE DRYING PROCESS 281 14.3.2 DRYING O F HYDRATES AND
SOLVATES 282 14.3.3 CHARACTERIZING THE DRYING BEHAVIOR IN THE LABORATORY
284 14.3.4 AMORPHIZATION DURING DRYING 284 14.3.5 EFFECT O F DRYING ON
THE PARTICLE SIZE DISTRIBUTION 285
REFERENCES 288
15 MELT CRYSTALLIZATION 289
JOACHIM ULRICH AND TORSTEN STELZER 15.1 CHARACTERISTICS O F MELT
CRYSTALLIZATION 289 15.1.1 DEFINITIONS 289
15.1.2 BENEFITS O F MELT CRYSTALLIZATION 290 15.2 PROCESSES O F MELT
CRYSTALLIZATION 292 15.2.1 SOLID LAYER CRYSTALLIZATION 292
IMAGE 8
X I I I CONTENTS
15.2.2 SUSPENSION CRYSTALLIZATION 294
15.3 POSTCRYSTALLIZATION TREATMENTS 295 15.3.1 SWEATING 297
15.3.2 WASHING 298
15.3.3 CHOICES 299
15.3.4 WASH COLUMNS 299
15.4 LABORATORY TECHNIQUES 301 15.4.1 BOTTLE TEST 301
15.4.2 COLD FINGER EXPERIMENTS 301 15.4.3 ZONE MELTING 303
REFERENCES 304
16 EXAMPLES O F REALIZED CONTINUOUS CRYSTALLIZATION PROCESSES 305 CUNTER
HOFMANN AND CHRISTIAN MELCHES 16.1 CHOOSING THE DRAIN POINT IN PROCESS
DESIGN 305 16.2 EXAMPLE CROP CRYSTALLIZATION FOR ORGANIC COMPOUNDS 310
16.2.1 FIELDS O F APPLICATION FOR THE CROP PRINCIPLE 310 16.2.2
DEFINITION OF TASK 311 16.2.3 SELECTION OF THE PROCESS DESIGN 312 16.3
EXAMPLE CRYSTALLIZATION O F TABLE SALT 316 16.3.1 INTRODUCTION 316
16.3.2 PERFORMANCE REQUIREMENTS 318 16.3.3 PROCESS DESIGN 318
16.3.4 DESCRIPTION O F THE PLANT FUNCTION 321 16.4 RESULTS 323
17 DESIGN EXAMPLES O F MELT CRYSTALLIZATION 325 JOACHIM ULRICH AND
TORSTEN STELZER 17.1 CONCEPTS O F MELT CRYSTALLIZATION 325 17.1.1 SOLID
LAYER CRYSTALLIZATION 325 17.1.2 SUSPENSION CRYSTALLIZATION 331 17.2
OUTLOOK 334
REFERENCES 335
INDEX 337 |
| any_adam_object | 1 |
| author2 | Beckmann, Wolfgang 19XX- |
| author2_role | edt |
| author2_variant | w b wb |
| author_GND | (DE-588)1032546824 |
| author_facet | Beckmann, Wolfgang 19XX- |
| building | Verbundindex |
| bvnumber | BV040797313 |
| classification_rvk | UQ 2000 UQ 3000 VN 7260 |
| classification_tum | CIT 210f CHE 192f |
| ctrlnum | (OCoLC)830343789 (DE-599)DNB102527198X |
| dewey-full | 660.284298 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660.284298 |
| dewey-search | 660.284298 |
| dewey-sort | 3660.284298 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie Physik Chemie Chemie-Ingenieurwesen |
| format | Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>00000nam a2200000 c 4500</leader><controlfield tag="001">BV040797313</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20140213</controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">130305s2013 ad|| |||| 00||| eng d</controlfield><datafield tag="015" ind1=" " ind2=" "><subfield code="a">12N35</subfield><subfield code="2">dnb</subfield></datafield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">102527198X</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9783527327621</subfield><subfield code="c">: Gb. : ca. EUR 129.00 (DE)</subfield><subfield code="9">978-3-527-32762-1</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9783527650323</subfield><subfield code="c">oBook</subfield><subfield code="9">978-3-527-65032-3</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)830343789</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)DNB102527198X</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">aacr</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-11</subfield><subfield code="a">DE-91G</subfield><subfield code="a">DE-703</subfield><subfield code="a">DE-92</subfield><subfield code="a">DE-83</subfield><subfield code="a">DE-29T</subfield><subfield code="a">DE-19</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">660.284298</subfield><subfield code="2">22/ger</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">UQ 2000</subfield><subfield code="0">(DE-625)146482:</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">UQ 3000</subfield><subfield code="0">(DE-625)146503:</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">VN 7260</subfield><subfield code="0">(DE-625)147614:253</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">CIT 210f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">CHE 192f</subfield><subfield code="2">stub</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Crystallization</subfield><subfield code="b">basic concepts and industrial applications</subfield><subfield code="c">ed. by Wolfgang Beckmann</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Weinheim</subfield><subfield code="b">Wiley-VCH</subfield><subfield code="c">2013</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XIV, 346 S.</subfield><subfield code="b">Ill., graph. Darst.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Kristallwachstum</subfield><subfield code="0">(DE-588)4123579-4</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Kristallisation</subfield><subfield code="0">(DE-588)4033215-9</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Kristallzüchtung</subfield><subfield code="0">(DE-588)4140616-3</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="655" ind1=" " ind2="7"><subfield code="0">(DE-588)4143413-4</subfield><subfield code="a">Aufsatzsammlung</subfield><subfield code="2">gnd-content</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Kristallisation</subfield><subfield code="0">(DE-588)4033215-9</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="689" ind1="1" ind2="0"><subfield code="a">Kristallwachstum</subfield><subfield code="0">(DE-588)4123579-4</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="1"><subfield code="a">Kristallzüchtung</subfield><subfield code="0">(DE-588)4140616-3</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Beckmann, Wolfgang</subfield><subfield code="d">19XX-</subfield><subfield code="0">(DE-588)1032546824</subfield><subfield code="4">edt</subfield></datafield><datafield tag="776" ind1="0" ind2="8"><subfield code="i">Erscheint auch als</subfield><subfield code="n">Online-Ausgabe, EPUB</subfield><subfield code="z">978-3-527-65034-7</subfield></datafield><datafield tag="776" ind1="0" ind2="8"><subfield code="i">Erscheint auch als</subfield><subfield code="n">Online-Ausgabe, MOBI</subfield><subfield code="z">978-3-527-65033-0</subfield></datafield><datafield tag="776" ind1="0" ind2="8"><subfield code="i">Erscheint auch als</subfield><subfield code="n">Online-Ausgabe, PDF</subfield><subfield code="z">978-3-527-65035-4</subfield></datafield><datafield tag="856" ind1="4" ind2=" "><subfield code="q">text/html</subfield><subfield code="u">http://deposit.dnb.de/cgi-bin/dokserv?id=4102903&prov=M&dok_var=1&dok_ext=htm</subfield><subfield code="3">Inhaltstext</subfield></datafield><datafield tag="856" ind1="4" ind2=" "><subfield code="m">DE-601</subfield><subfield code="q">pdf/application</subfield><subfield code="u">http://www.gbv.de/dms/bowker/toc/9783527327621.pdf</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">DNB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025777483&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="943" ind1="1" ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-025777483</subfield></datafield></record></collection> |
| genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content |
| genre_facet | Aufsatzsammlung |
| id | DE-604.BV040797313 |
| illustrated | Illustrated |
| indexdate | 2024-08-21T00:36:01Z |
| institution | BVB |
| isbn | 9783527327621 9783527650323 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-025777483 |
| oclc_num | 830343789 |
| open_access_boolean | |
| owner | DE-11 DE-91G DE-BY-TUM DE-703 DE-92 DE-83 DE-29T DE-19 DE-BY-UBM |
| owner_facet | DE-11 DE-91G DE-BY-TUM DE-703 DE-92 DE-83 DE-29T DE-19 DE-BY-UBM |
| physical | XIV, 346 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Crystallization basic concepts and industrial applications ed. by Wolfgang Beckmann Weinheim Wiley-VCH 2013 XIV, 346 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Kristallwachstum (DE-588)4123579-4 gnd rswk-swf Kristallisation (DE-588)4033215-9 gnd rswk-swf Kristallzüchtung (DE-588)4140616-3 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Kristallisation (DE-588)4033215-9 s DE-604 Kristallwachstum (DE-588)4123579-4 s Kristallzüchtung (DE-588)4140616-3 s Beckmann, Wolfgang 19XX- (DE-588)1032546824 edt Erscheint auch als Online-Ausgabe, EPUB 978-3-527-65034-7 Erscheint auch als Online-Ausgabe, MOBI 978-3-527-65033-0 Erscheint auch als Online-Ausgabe, PDF 978-3-527-65035-4 text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4102903&prov=M&dok_var=1&dok_ext=htm Inhaltstext DE-601 pdf/application http://www.gbv.de/dms/bowker/toc/9783527327621.pdf Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025777483&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Crystallization basic concepts and industrial applications Kristallwachstum (DE-588)4123579-4 gnd Kristallisation (DE-588)4033215-9 gnd Kristallzüchtung (DE-588)4140616-3 gnd |
| subject_GND | (DE-588)4123579-4 (DE-588)4033215-9 (DE-588)4140616-3 (DE-588)4143413-4 |
| title | Crystallization basic concepts and industrial applications |
| title_auth | Crystallization basic concepts and industrial applications |
| title_exact_search | Crystallization basic concepts and industrial applications |
| title_full | Crystallization basic concepts and industrial applications ed. by Wolfgang Beckmann |
| title_fullStr | Crystallization basic concepts and industrial applications ed. by Wolfgang Beckmann |
| title_full_unstemmed | Crystallization basic concepts and industrial applications ed. by Wolfgang Beckmann |
| title_short | Crystallization |
| title_sort | crystallization basic concepts and industrial applications |
| title_sub | basic concepts and industrial applications |
| topic | Kristallwachstum (DE-588)4123579-4 gnd Kristallisation (DE-588)4033215-9 gnd Kristallzüchtung (DE-588)4140616-3 gnd |
| topic_facet | Kristallwachstum Kristallisation Kristallzüchtung Aufsatzsammlung |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4102903&prov=M&dok_var=1&dok_ext=htm http://www.gbv.de/dms/bowker/toc/9783527327621.pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025777483&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT beckmannwolfgang crystallizationbasicconceptsandindustrialapplications |