Emulsion formation and stability:
Gespeichert in:
| Weitere Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH-Verl.
2013
|
| Schlagworte: | |
| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben |
| Beschreibung: | XV, 252 S. Ill., graph. Darst. 25 cm |
| ISBN: | 9783527319916 9783527647941 |
Internformat
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Datensatz im Suchindex
| _version_ | 1807955263023480832 |
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| adam_text |
IMAGE 1
CONTENTS
PREFACE XI LIST O F CONTRIBUTORS XIII
1 EMULSION FORMATION, STABILITY, AND RHEOLOGY 1 THARWAT F. TADROS 1.1
INTRODUCTION 1
1.1.1 NATURE O F THE EMULSIFIER 1
1.1.2 STRUCTURE O F THE SYSTEM 2
1.1.3 BREAKDOWN PROCESSES IN EMULSIONS 3 1.1.4 CREAMING AND
SEDIMENTATION 3 1.1.5 FLOCCULATION 4
1.1.6 OSTWALD RIPENING (DISPROPORTIONATION) 4 1.1.7 COALESCENCE 4
1.1.8 PHASE INVERSION 4
1.2 INDUSTRIAL APPLICATIONS O F EMULSIONS 4 1.3 PHYSICAL CHEMISTRY O F
EMULSION SYSTEMS 5 1.3.1 THE INTERFACE (GIBBS DIVIDING LINE) 5 1.4
THERMODYNAMICS O F EMULSION FORMATION AND BREAKDOWN 6 1.5 INTERACTION
ENERGIES (FORCES) BETWEEN EMULSION DROPLETS
AND THEIR COMBINATIONS 8 1.5.1 VAN DER WAALS ATTRACTION 8 1.5.2
ELECTROSTATIC REPULSION 9 1.5.3 STERIC REPULSION 12
1.6 ADSORPTION O F SURFACTANTS AT THE LIQUID/LIQUID INTERFACE 14 1.6.1
THE GIBBS ADSORPTION ISOTHERM 14 1.6.2 MECHANISM O F EMULSIFICATION 17
1.6.3 METHODS O F EMULSIFICATION 19 1.6.4 ROLE O F SURFACTANTS IN
EMULSION FORMATION 21 1.6.5 ROLE O F SURFACTANTS IN DROPLET DEFORMATION
22 1.7 SELECTION O F EMULSIFIERS 26
1.7.1 THE HYDROPHILIC-LIPOPHILIC BALANCE (HLB) CONCEPT 26 1.7.2 THE
PHASE INVERSION TEMPERATURE (PIT) CONCEPT 29 1.7.3 THE COHESIVE ENERGY
RATIO (CER) CONCEPT 31
HTTP://D-NB.INFO/1024048136
IMAGE 2
V I | CONTENTS
1.7.4 THE CRITICAL PACKING PARAMETER (CPP) FOR EMULSION SELECTION 32
1.8 CREAMING OR SEDIMENTATION O F EMULSIONS 35 1.8.1 CREAMING OR
SEDIMENTATION RATES 36 1.8.2 PREVENTION O F CREAMING OR SEDIMENTATION 37
1.9 FLOCCULATION O F EMULSIONS 40
1.9.1 MECHANISM O F EMULSION FLOCCULATION 40 1.9.1.1 FLOCCULATION O F
ELECTROSTATICALLY STABILIZED EMULSIONS 41 1.9.1.2 FLOCCULATION O F
STERICALLY STABILIZED EMULSIONS 42 1.9.2 GENERAL RULES FOR REDUCING
(ELIMINATING) FLOCCULATION 43
1.10 OSTWALD RIPENING 44
1.11 EMULSION COALESCENCE 45 1.11.1 RATE O F COALESCENCE 46 1.11.2 PHASE
INVERSION 47
1.12 RHEOLOGY O F EMULSIONS 48 1.12.1 INTERFACIAL RHEOLOGY 48 1.12.1.1
INTERFACIAL TENSION AND SURFACE PRESSURE 48 1.12.1.2 INTERFACIAL SHEAR
VISCOSITY 49
1.12.2 MEASUREMENT OF INTERFACIAL VISCOSITY 49 1.12.3 INTERFACIAL
DILATIONAL ELASTICITY 50 1.12.4 INTERFACIAL DILATIONAL VISCOSITY 51
1.12.5 NON-NEWTONIAN EFFECTS 51
1.12.6 CORRELATION O F EMULSION STABILITY WITH INTERFACIAL RHEOLOGY 51
1.12.6.1 MIXED SURFACTANT FILMS 51 1.12.6.2 PROTEIN FILMS 51 1.13 BULK
RHEOLOGY OF EMULSIONS 53 1.13.1 ANALYSIS O F THE RHEOLOGICAL BEHAVIOR OF
CONCENTRATED EMULSIONS 54 1.14 EXPERIMENTAL RJ T - J) CURVES 57 1.14.1
EXPERIMENTAL TFR - / CURVES 58 1.14.2 INFLUENCE O F DROPLET
DEFORMABILITY 58
1.15 VISCOELASTIC PROPERTIES O F CONCENTRATED EMULSIONS 59 1.15.1 HIGH
INTERNAL PHASE EMULSIONS (HIPES) 61 1.15.2 DEFORMATION AND BREAKUP O F
DROPLETS IN EMULSIONS DURING FLOW 66 REFERENCES 73
2 EMULSION FORMATION IN MEMBRANE AND MICROFLUIDIC DEVICES 77 GORAN T.
VLADISAVLJEVID, ISAO KOBAYASHI, AND MITSUTOSHI NAKAJIMA 2.1 INTRODUCTION
77
2.2 MEMBRANE EMULSIFKATION (ME) 78 2.2.1 DIRECT MEMBRANE EMULSIFICATION
78 2.2.2 PREMIX MEMBRANE EMULSIFICATION 79 2.2.3 OPERATING PARAMETERS IN
MEMBRANE EMULSIFICATION 80
2.2.4 MEMBRANE TYPE 80
2.2.4.1 SURFACTANT TYPE 80 2.2.4.2 TRANSMEMBRANE PRESSURE AND WALL SHEAR
STRESS 81 2.3 MICROFLUIDIC JUNCTIONS AND FLOW-FOCUSING DEVICES 82
IMAGE 3
CONTENTS V I I
2.3.1 MICROFLUIDIC JUNCTIONS 82
2.3.2 MICROFLUIDIC FLOW-FOCUSING DEVICES (MFFD) 83 2.4 MICROFLUIDIC
DEVICES WITH PARALLEL MICROCHANNEL ARRAYS 85 2.4.1 GROOVED-TYPE
MICROCHANNEL ARRAYS 86 2.4.2 STRAIGHT-THROUGH MICROCHANNEL ARRAYS 88 2.5
GLASS CAPILLARY MICROFLUIDIC DEVICES 89 2.6 APPLICATION O F DROPLETS
FORMED IN MEMBRANE AND MICROFLUIDIC
DEVICES 93
2.7 CONCLUSIONS 93
ACKNOWLEDGMENTS 94 REFERENCES 94
3 ADSORPTION CHARACTERISTICS O F IONIC SURFACTANTS AT WATER/HEXANE
INTERFACE OBTAINED BY PAT AND ODBA 99 NENAD MUCIC, VINCENT PRADINES,
ALIYAR JAVADI, ALTYNAY SHARIPOVA, JIIRGEN KRAGEL, MARTIN E. LESER,
EUGENE V. AKSENENKO,
VALENTIN B. FAINERMAN, AND REINHARD MILLER 3.1 INTRODUCTION 99
3.2 EXPERIMENTAL TOOLS 99
3.3 THEORY 101
3.4 RESULTS 102
3.5 SUMMARY 107
ACKNOWLEDGMENTS 107 REFERENCES 107
4 MEASUREMENT TECHNIQUES APPLICABLE TO THE INVESTIGATION O F EMULSION
FORMATION DURING PROCESSING 109 NIMA NIKNAJS, ROBIN D. HANCOCKS, AND IAN
T. NORTON
4.1 INTRODUCTION 109
4.2 ONLINE DROPLET SIZE MEASUREMENT TECHNIQUES 112 4.2.1 LASER SYSTEMS
112
4.2.2 SOUND SYSTEMS 115
4.2.3 DIRECT IMAGING 115
4.2.4 OTHER TECHNIQUES 118
4.3 TECHNIQUES INVESTIGATING DROPLET COALESCENCE 121 4.4 CONCLUDING
REMARKS 123
REFERENCES 125
5 EMULSIFICATION IN ROTOR-STATOR MIXERS 127 ANDRZEJ W. PACEK, STEVEN
HALL, MICHAEL COOKE, AND ADAM J. KOWALSKI 5.1 INTRODUCTION 127
5.2 CLASSIFICATION AND APPLICATIONS O F ROTOR-STATOR MIXERS 128 5.2.1
COLLOID MILLS 129
5.2.2 IN-LINE RADIAL DISCHARGE MIXERS 130 5.2.3 TOOTHED DEVICES 131
IMAGE 4
VIIII CONTENTS
5.2.4 BATCH RADIAL DISCHARGE MIXERS 132
5.2.5 DESIGN AND ARRANGEMENT 133 5.2.6 OPERATION 136
5.3 ENGINEERING DESCRIPTION O F EMULSIFICATION/DISPERSION PROCESSES 138
5.3.1 DROP SIZE DISTRIBUTIONS AND AVERAGE DROP SIZES 138 5.3.2 DROP SIZE
IN LIQUID-LIQUID TWO-PHASE SYSTEMS - THEORY 140 5.3.3 MAXIMUM STABLE
DROP SIZE IN LAMINAR FLOW 141 5.3.4 MAXIMUM STABLE DROP SIZE IN
TURBULENT FLOW 142 5.3.5 CHARACTERIZATION O F FLOW IN ROTOR-STATOR
MIXERS 143 5.3.5.1 SHEAR STRESS 143 5.3.5.2 AVERAGE ENERGY DISSIPATION
RATE 144
5.3.5.3 POWER DRAW 144 5.3.6 AVERAGE DROP SIZE IN LIQUID-LIQUID SYSTEMS
145 5.3.7 SCALING-UP OF ROTOR-STATOR MIXERS 147 5.4 ADVANCED ANALYSIS O
F EMULSIFICATION/DISPERSION PROCESSES IN
ROTOR-STATOR MIXERS 152 5.4.1 VELOCITY AND ENERGY DISSIPATION RATE IN
ROTOR-STATOR MIXERS 153 5.4.1.1 BATCH ROTOR-STATOR MIXERS 154 5.4.1.2
IN-LINE ROTOR-STATOR MIXERS 157 5.4.2 PREDICTION O F DROP SIZE
DISTRIBUTIONS DURING EMULSIFICATION 160 5.5 CONCLUSION 163
N OMENCLATURE 163 REFERENCES 165
6 FORMULATION, CHARACTERIZATION, AND PROPERTY CONTROL O F PARAFFIN
EMULSIONS 169 JORDI ESQUENA AND JON VILASAU 6.1 INTRODUCTION 169
6.1.1 INDUSTRIAL APPLICATIONS OF PARAFFIN EMULSIONS 170 6.1.2 PROPERTIES
O F PARAFFIN 170 6.1.3 PREPARATION O F PARAFFIN EMULSIONS 172 6.2
SURFACTANT SYSTEMS USED IN FORMULATION O F PARAFFIN EMULSIONS 174 6.2.1
PHASE BEHAVIOR 175
6.3 FORMATION AND CHARACTERIZATION O F PARAFFIN EMULSIONS 178 6.4
CONTROL O F PARTICLE SIZE 181
6.5 STABILITY O F PARAFFIN EMULSIONS 185 6.5.1 STABILITY AS A FUNCTION
OF TIME UNDER SHEAR (ORTHOKINETIC STABILITY) 185 6.5.2 STABILITY AS A
FUNCTION O F FREEZE-THAW CYCLES 186 6.5.3 STABILITY AS A FUNCTION O F
ELECTROLYTES 189 6.6 CONCLUSIONS 195
ACKNOWLEDGMENTS 196 REFERENCES 196
IMAGE 5
CONTENTS I I X
7 POLYMERIC O/W NANO-EMULSIONS OBTAINED BY THE PHASE INVERSION
COMPOSITION (PIC) METHOD FOR BIOMEDICAL NANOPARTIDE PREPARATION 199
GABRIELA CALDERO AND CONXITA SOLANS 7.1 INTRODUCTION 199
7.2 PHASE INVERSION EMULSIFICATION METHODS 200 7.3 ASPECTS ON THE CHOICE
O F THE COMPONENTS 201 7.4 ETHYLCELLULOSE NANO-EMULSIONS FOR NANOPARTIDE
PREPARATION 202 7.5 FINAL REMARKS 204
ACKNOWLEDGMENTS 205 REFERENCES 205
8 RHEOLOGY AND STABILITY O F STERICALLY STABILIZED EMULSIONS 209 THARWAT
F. TADROS 8.1 INTRODUCTION 209
8.2 GENERAL CLASSIFICATION O F POLYMERIC SURFACTANTS 210 8.3 INTERACTION
BETWEEN DROPLETS CONTAINING ADSORBED POLYMERIC SURFACTANT LAYERS: STERIC
STABILIZATION 212 8.3.1 MIXING INTERACTION G M ; X 213 8.3.2 ELASTIC
INTERACTION G E I 214 8.4 EMULSIONS STABILIZED BY POLYMERIC SURFACTANTS
216 8.4.1 W/O EMULSIONS STABILIZED WITH PHS-PEO-PHS BLOCK COPOLYMER 219
8.5 PRINCIPLES O F RHEOLOGICAL TECHNIQUES 220 8.5.1 STEADY STATE
MEASUREMENTS 220 8.5.1.1 BINGHAM PLASTIC SYSTEMS 221 8.5.1.2
PSEUDOPLASTIC (SHEAR THINNING) SYSTEM 221 8.5.1.3 HERSCHEL-BULKLEY
GENERAL MODEL 222
8.5.2 CONSTANT STRESS (CREEP) MEASUREMENTS 222 8.5.3 DYNAMIC
(OSCILLATORY) MEASUREMENTS 223 8.6 RHEOLOGY O F OIL-IN-WATER (O/W)
EMULSIONS STABILIZED WITH POLY(VINYL ALCOHOL) 226
8.6.1 EFFECT O F OIL VOLUME FRACTION ON THE RHEOLOGY O F THE EMULSIONS
226 8.6.2 STABILITY O F PVA-STABILIZED EMULSIONS 229 8.6.3 EMULSIONS
STABILIZED WITH AN A-B-A BLOCK COPOLYMER 236 8.6.4 WATER-IN-OIL
EMULSIONS STABILIZED WITH A-B-A BLOCK COPOLYMER 240
REFERENCES 245
INDEX 247 |
| any_adam_object | 1 |
| author2 | Tadros, Tharwat F. 1937-2018 |
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| author_GND | (DE-588)129740837 |
| author_facet | Tadros, Tharwat F. 1937-2018 |
| building | Verbundindex |
| bvnumber | BV040790462 |
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| ctrlnum | (OCoLC)827784935 (DE-599)DNB1024048136 |
| dewey-full | 660.294514 620.5 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering 620 - Engineering and allied operations |
| dewey-raw | 660.294514 620.5 |
| dewey-search | 660.294514 620.5 |
| dewey-sort | 3660.294514 |
| dewey-tens | 660 - Chemical engineering 620 - Engineering and allied operations |
| discipline | Chemie / Pharmazie Maschinenbau / Maschinenwesen |
| format | Book |
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| isbn | 9783527319916 9783527647941 |
| language | English |
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| physical | XV, 252 S. Ill., graph. Darst. 25 cm |
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| publisher | Wiley-VCH-Verl. |
| record_format | marc |
| spelling | Emulsion formation and stability ed. by Tharwat F. Thadros Weinheim Wiley-VCH-Verl. 2013 XV, 252 S. Ill., graph. Darst. 25 cm txt rdacontent n rdamedia nc rdacarrier Literaturangaben Emulsion (DE-588)4014626-1 gnd rswk-swf Nanopartikel (DE-588)4333369-2 gnd rswk-swf Emulsion (DE-588)4014626-1 s Nanopartikel (DE-588)4333369-2 s DE-604 Tadros, Tharwat F. 1937-2018 (DE-588)129740837 edt Erscheint auch als Online-Ausgabe, EPUB 978-3-527-64796-5 Erscheint auch als Online-Ausgabe, MOBI 978-3-527-64795-8 Erscheint auch als Online-Ausgabe, PDF 978-3-527-64797-2 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4071677&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025768603&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Emulsion formation and stability Emulsion (DE-588)4014626-1 gnd Nanopartikel (DE-588)4333369-2 gnd |
| subject_GND | (DE-588)4014626-1 (DE-588)4333369-2 |
| title | Emulsion formation and stability |
| title_auth | Emulsion formation and stability |
| title_exact_search | Emulsion formation and stability |
| title_full | Emulsion formation and stability ed. by Tharwat F. Thadros |
| title_fullStr | Emulsion formation and stability ed. by Tharwat F. Thadros |
| title_full_unstemmed | Emulsion formation and stability ed. by Tharwat F. Thadros |
| title_short | Emulsion formation and stability |
| title_sort | emulsion formation and stability |
| topic | Emulsion (DE-588)4014626-1 gnd Nanopartikel (DE-588)4333369-2 gnd |
| topic_facet | Emulsion Nanopartikel |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4071677&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025768603&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT tadrostharwatf emulsionformationandstability |