Practical instrumental analysis: methods, quality assurance and laboratory management
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| Format: | Buch |
| Sprache: | English |
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2013
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| Beschreibung: | XXIII, 467 S. Ill., graph. Darst. |
| ISBN: | 352732951X 9783527329519 9783527665891 |
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| 020 | |a 9783527329519 |c : Pb. : ca. EUR 49.90 (DE) |9 978-3-527-32951-9 | ||
| 020 | |a 9783527665891 |c oBook |9 978-3-527-66589-1 | ||
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| 100 | 1 | |a Petrozzi, Sergio |e Verfasser |0 (DE-588)141141670 |4 aut | |
| 245 | 1 | 0 | |a Practical instrumental analysis |b methods, quality assurance and laboratory management |c Sergio Petrozzi |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2013 | |
| 300 | |a XXIII, 467 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
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| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, MOBI |z 978-3-527-66590-7 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, PDF |z 978-3-527-66592-1 |
| 856 | 4 | |q text/html |u http://deposit.dnb.de/cgi-bin/dokserv?id=4071680&prov=M&dok_var=1&dok_ext=htm |3 Inhaltstext | |
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Datensatz im Suchindex
| _version_ | 1807954707827654656 |
|---|---|
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IMAGE 1
CONTENTS
PREFACE TO T H E GERMAN EDITION XV PREFACE TO T H E ENGLISH EDITION X I
X DEDICATION X X I FOREWORD X X I I I
1 INTRODUCTION 1
1.1 ANALYTICAL C H E M I S T R Y - T H E HISTORY 1
1.2 ANALYTICAL CHEMISTRY A N D ITS ROLE I N TODAY'S SOCIETY 2
2 INTRODUCTION T O QUALITY MANAGEMENT 5
2.1 HISTORICAL BACKGROUND 5
2.2 VARIABILITY 6
2.3 T H E FOUR PILLARS O F WISDOM (FROM SHEWHART TO DEMING) 10
2.4 ZERO-DEFECT TOLERANCE 10
2.5 W H Y STANDARDS? 11
2.6 THE CONTROLLED PROCESS 11
2.7 ISO GUIDELINES 9004 12
2.8 QUALITY MANAGEMENT SYSTEM (QMS) REQUIREMENTS 15
3 FUNDAMENTALS O F STATISTICS 17
3.1 BASIC CONCEPTS 17
3.1.1 POPULATION A N D SAMPLE 19
3.1.2" DISTRIBUTION O F VALUES 2 0
3.2 IMPORTANT T E R M S 2 2
3.2.1 MEAN, ARITHMETIC MEAN, AVERAGE (X) 2 2 3.2.2 STANDARD DEVIATION
(A, S) 2 2
3.2.3 VARIANCE (VAR,V) 23
3.2.4 STANDARD DEVIATION O F MEAN VALUES (S) 2 4 3.2.5 RELATIVE STANDARD
DEVIATION (RSD) A N D COEFFICIENT O F VARIATION (CV) 3.2.6 CONFIDENCE
INTERVAL (CI), CONFIDENCE LIMITS 2 5 3.3 QUALITY O F RESULTS (ACCURACY A
N D PRECISION) 2 5
3.3.1 MEASUREMENT DEVIATIONS 2 8
HTTP://D-NB.INFO/1024048160
IMAGE 2
V I | CONTENTS
3.3.2 RANDOM DEVIATIONS - INFLUENCE O N PRECISION 3 0
3.3.2.1 PRECISION 3 0
3.3.2.2 DETERMINATION O F RANDOM DEVIATIONS 3 0 3.3.2.3 CAUSES O F
RANDOM DEVIATIONS 31 3.3.3 SYSTEMATIC DEVIATIONS-INFLUENCE O N ACCURACY
31 3.3.3.1 ACCURACY/TRUENESS 31 3.3.3.2 BIAS 31
3.3.3.3 CAUSES O F SYSTEMATIC DEVIATIONS 3 2 3.3.3.4 EFFECTS O N THE
MEASUREMENT 3 2 3.3.3.5 DETERMINATION O F SYSTEMATIC DEVIATIONS 3 2
3.3.3.6 RECOVERY EXPERIMENTS 3 3 3.3.4 GROSS ERRORS 3 3
3.3.4.1 CAUSES O F GROSS ERRORS 3 4
3.3.5 UNCERTAINTY O F MEASUREMENT RESULTS 3 4 3.3.5.1 STANDARD
UNCERTAINTY O F SINGLE MEASUREMENTS 3 4 3.3.5.2 COMBINED UNCERTAINTY 3 5
3.3.5.3 PROCEDURE FOR DETERMINING THE COMBINED UNCERTAINTY 35 3.3.5.4
RULES FOR UNCERTAINTY PROPAGATION 3 7
3.3.5.5 EXTENDED UNCERTAINTY 3 8 3.3.6 NON-STATISTICAL METHODS O F
ESTIMATION 3 8 3.3.6.1 TOLERANCE 3 8
3.3.7 EXPRESSING ANALYTICAL RESULTS 3 9 3.3.7.1 EXPRESSING THE
MEASUREMENT UNCERTAINTY I N THE VALUE O F A QUANTITY 3 9
3.3.7.2 ACCORDANCE WITH THE NATIONAL INSTITUTE O F STANDARDS A N D
TECHNOLOGY, U.S. DEPARTMENT O F COMMERCE (NIST) 3 9 3.3.8 SIGNIFICANT
FIGURES-"BOX-AND-DOT" METHOD 4 0 3.3.9 OUTLIER TESTS 4 2
3.3.9.1 THE 2.5 S BARRIER 4 2
3.3.9.2 TEST ACCORDING TO GRUBBS 42 3.4 REGRESSION 4 3
3.4.1 REGRESSION ANALYSIS 4 3
3.4.2 CALIBRATION FUNCTION 43
3.4.3 THE "OPTIMAL" TREND LINE 4 4
3.4.4 LINEAR REGRESSION 4 5
3.4.4.1 LINEARITY 4 5
3.4.4.2 STATISTICAL INFORMATION FROM LINEAR REGRESSION 4 6 3.4.4.3
ANALYTICAL SENSITIVITY 4 6 3.4.4.4 CORRELATION COEFFICIENT (R) 46
3.4.4.5 COEFFICIENT O F DETERMINATION (J? 2) 4 7
3.4.4.6 REGRESSION EQUATION 4 7
4 THE ANALYTICAL PROCESS 53
4.1 T H E ANALYTICAL PROCESS IN THE OVERALL CONTEXT 53
4.2 PLANNING PHASE 5 5
IMAGE 3
CONTENTS | V I I
4.2.1 ANALYTICAL PROBLEM 5 5
4.2.2 OBJECT O F INVESTIGATION 56
4.2.3 SAMPLE 56
4.2.4 SAMPLING 5 7
4.2.4.1 TYPES O F SAMPLING 5 8 4.2.4.2 SAMPLING ERRORS 59 4.2.4.3 SAMPLE
HANDLING 60 4.2.4.4 DIFFICULTIES O F SAMPLE PROCESSING 60 4.2.5
EXAMINATION PROCEDURES 61 4.2.6 ANALYTE 62
4.2.7 LITERATURE A N D DATABASE RESEARCH 62 4.2.7.1 TYPES O F CHEMICAL
LITERATURE 63 4.2.7.2 FROM T H E QUESTION TO THE DOCUMENT 63 4.2.7.3
FROM THE QUOTATION TO THE DOCUMENT 63 4.2.7.4 THE QUESTION O F TOPIC 65
4.2.7.5 SCIENCE CITATION INDEX EXPANDED 66 4.2.7.6 SCOPUS 66
4.2.7.7 MEDLINE 66
4.2.7.8 CURRENT INFORMATION 6 7 4.2.7.9 SPECIFIC TYPES O F DOCUMENTS
SUCH AS NORMS A N D PATENTS 6 7 4.3 ANALYSIS 6 7
4.3.1 MEASUREMENT 6 7
4.3.2 METHOD OPTIMIZATION 6 8
4.3.3 CALIBRATION 69
4.3.3.1 EXTERNAL CALIBRATION 70 4.3.3.2 INTERNAL STANDARD (ISTD) 71
4.3.3.3 STANDARD ADDITION METHOD (SPIKING METHOD) 71 4.3.3.4 ONE-TIME
ADDITION 71
4.3.3.5 MULTIPLE ADDITIONS 72 4.3.3.6 RECOVERY STANDARD (RSTD) 73 4.4
ASSESSMENT 74
4.4.1 QUANTIFICATION 74
4.4.1.1 TRACEABILITY 74 4.4.2 ("TRUE") CONTENT 74
4.4.2.1 TERMINOLOGY 75 4.5 VALIDATION 75
4.5.1 VALIDATION ELEMENTS 77
4.5.1.1 SELECTIVITY/SPECIFICITY 77 4.5.1.2 WORKING RANGE 78 4.5.1.3
DETECTION, DETERMINATION A N D QUANTITATION LIMIT 78 4.5.1.4 G E R M A N
STANDARD DIN 32645 78
4.5.1.5 CALCULATIONS 81 4.5.1.6 LIMIT O F DETECTION ACCORDING TO KAISER
8 4 4.5.1.7 ROBUSTNESS 86 4.5.2 USING THE COMPUTER 86
IMAGE 4
V I I I | CONTENTS
4.6 FINAL DOCUMENTATION 8 7
4.6.1 REVIEW 8 8
5 EXAMPLE O F A VALIDATION STRATEGY 8 9
5.1 DETERMINATION O F PHENOL IN INDUSTRIAL WASTE WATER 9 0
5.1.1 CONFIRMATION O F IDENTITY 92
5.1.1.1 SELECTIVITY 9 2
5.1.1.2 PRECISION 92
5.1.2 SAMPLE CONTENT DETERMINATION 93 5.1.2.1 ACCURACY 93
5.1.2.2 CALIBRATION FUNCTION-CALIBRATION, LINEARITY, WORKING RANGE 94
5.1.2.3 DETERMINATION O F THE DETECTION, DETERMINATION A N D
QUANTITATION LIMITS ACCORDING TO DIN 32645-DIRECT A N D INDIRECT METHOD
96 5.1.2.4 MEASUREMENT UNCERTAINTY 99 5.1.2.5 ROBUSTNESS 101
5.1.3 SELECTION 102
5.1.3.1 FINAL DOCUMENTATION 102
6 ORGANIZATIONAL AND PRACTICAL PROCEDURES IN T H E TEACHING LABORATORY
PROGRAM 103 6.1 GOALS 103
6.2 SAFETY IN THE LABORATORY CLASS 104
6.3 EXPERIMENTAL PROJECT WORKFLOW 104
6.3.1 PREPARATION 104
6.3.2 LABORATORY NOTEBOOK 105 6.4 REPORTS 110
REFERENCES 114
7 LITERATURE 115
7.1 CITED LITERATURE 115
7.2 RECOMMENDED NORMS (SELECTION) 116
7.2.1 CALIBRATION 116
7.2.2 INTER-LABORATORY TESTS 116
7.2.3 QUALITY MANAGEMENT 117
7.3 SUGGESTED BOOKS (SELECTION) 117
8 PROJECTS 119
8.1 CHROMATOGRAPHY 121
8.1.1 GAS CHROMATOGRAPHY-GC, PROJECT: TANKER ACCIDENT 121 8.1.1.1
ANALYTICAL PROBLEM 121 8.1.1.2 INTRODUCTION 123 8.1.1.3 MATERIAL A N D
METHODS 135
8.1.1.4 QUESTIONS 139
REFERENCES 139
IMAGE 5
CONTENTS | I X
8.1.2 GAS CHROMATOGRAPHY COUPLED WITH MASS SELECTIVE DETECTION-GC/MS,
PROJECT: "CIRCUMVENTION O F THE FORMERLY MANDATORY DECLARATION OF
FRAGRANCES IN PERFUMES?" 139 8.1.2.1 ANALYTICAL PROBLEM 139
8.1.2.2 INTRODUCTION 141 8.1.2.3 MATERIAL A N D METHODS 155 8.1.2.4
QUESTIONS 158
REFERENCES 159
8.1.3 HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY-HPLC, PROJECT: "STRICTER
CONTROL O F DRUGS" 159 8.1.3.1 ANALYTICAL PROBLEM 159
8.1.3.2 INTRODUCTION 161 8.1.3.3 MATERIAL A N D METHODS 170 8.1.3.4
QUESTIONS 173
REFERENCES 173
8.1.4 HIGH-PERFORMANCE LIQUID CHROMATOGRAPHY COUPLED WITH MASSSELECTIVE
DETECTION-LC/MS, PROJECT "COCAINE SCANDAL: HAIR SAMPLE WITH
CONSEQUENCES" 173 8.1.4.1 ANALYTICAL PROBLEM 173 8.1.4.2 INTRODUCTION
175 8.1.4.3 MATERIAL A N D METHODS 189 8.1.4.4 QUESTIONS 193
REFERENCES 194
8.1.5 ION CHROMATOGRAPHY(IC), PROJECT: "WATER IS LIFE" 194 8.1.5.1
ANALYTICAL PROBLEM 194 8.1.5.2 INTRODUCTION 196 8.1.5.3 MATERIAL A N D
METHODS 215 8.1.5.4 QUESTIONS 2 2 0
REFERENCES 2 2 0
8.1.6 HIGH-PERFORMANCE THIN-LAYER CHROMATOGRAPHY (HPTLC), PROJECT:
"ENSURING REGULATORY COMPLIANCE BY QUANTIFICATION O F LEAD COMPOUNDS
(MARKERS) I N HERBAL COMBINATION PRODUCTS" 221 8.1.6.1 ANALYTICAL
PROBLEM 221 8.1.6.2 INTRODUCTION 223
8.1.6.3 MATERIAL A N D METHODS 232 8.1.6.4 QUESTIONS 236
REFERENCES 236
8.2 SPECTROSCOPY 236
8.2.1 UV-VIS SPECTROSCOPY, PROJECT: "EVALUATION O F POTENTIAL SAVING
THROUGH USE O F OPTIMIZED ALLOYS" 236 8.2.1.1 ANALYTICAL PROBLEM 236
8.2.1.2 INTRODUCTION 238
8.2.1.3 BANDWIDTH 242 8.2.1.4 MATERIAL AND METHODS 243
IMAGE 6
X | CONTENTS
8.2.1.5 QUESTIONS 246
REFERENCES 2 4 7
8.2.2 FOURIER-TRANSFORM INFRARED SPECTROSCOPY (FTIR), PROJECT:
"BENCHMARKING WITH A NEW COMPETITIVE JAPANESE PRODUCT" 2 4 7 8.2.2.1
ANALYTICAL PROBLEM 2 4 7 8.2.2.2 INTRODUCTION 249
8.2.2.3 MATERIAL A N D METHODS 259 8.2.2.4 QUESTIONS 263
REFERENCES 264
8.2.3 NEAR-INFRARED (NIR) SPECTROMETRY, PROJECT: "ACCELERATED RAW
MATERIAL INTAKE CONTROL" 264 8.2.3.1 ANALYTICAL PROBLEM 264 8.2.3.2
INTRODUCTION 266 8.2.3.3 MATERIAL A N D METHODS 282 8.2.3.4 QUESTIONS
286
REFERENCE 286
8.2.4 ATOMIC ABSORPTION SPECTROSCOPY (AAS), PROJECT: "RECYCLING O F
SEWAGE SLUDGE I N AGRICULTURE" 286 8.2.4.1 ANALYTICAL PROBLEM 286
8.2.4.2 INTRODUCTION 288
8.2.4.3 MATERIAL A N D METHODS 296 8.2.4.4 QUESTIONS 299
REFERENCES 299
8.3 ELECTROPHORETIC SEPARATION METHODS 299
8.3.1 CAPILLARY ELECTROPHORESIS, PROJECT: "PRESERVATIVES I N COSMETICS:
FRIEND OR FOE" 299
8.3.1.1 ANALYTICAL PROBLEM 299 8.3.1.2 INTRODUCTION 301
8.3.1.3 MATERIAL A N D METHODS 313 8.3.1.4 QUESTIONS 316
REFERENCES 316
8.4 AUTOMATION 316
8.4.1 FLOW INJECTION ANALYSIS (FIA), PROJECT: "PHENOL-LIKE FLAVOR IN
BEER: A QUALITY PARAMETER TO BE MASTERED" 316 8.4.1.1 ANALYTICAL PROBLEM
316 8.4.1.2 INTRODUCTION 3 1 9
8.4.1.3 MATERIAL A N D METHODS 3 2 4 8.4.1.4 QUESTIONS 3 2 7
REFERENCES 3 2 8
8.5 MASS ANALYTICAL DETERMINATION METHODS 3 2 8
8.5.1 KARL FISCHER WATER DETERMINATION, PROJECT: "WATER CONTENT AS A
QUALITY PARAMETER" 3 2 8 8.5.1.1 ANALYTICAL PROBLEM 3 2 8 8.5.1.2
INTRODUCTION 3 3 0
8.5.1.3 MATERIAL A N D METHODS 3 4 4
IMAGE 7
CONTENTS | X I
8.5.1.4 QUESTIONS 3 4 7
REFERENCES 3 4 7
8.6 GENERAL ANALYTICAL METHODS 3 4 8
8.6.1 NITROGEN A N D PROTEIN DETERMINATION ACCORDING TO KJELDAHL,
PROJECT: "OFFICIAL CONTROL AT THE SWISS ALPS DAIRY LTD" 3 4 8 8.6.1.1
ANALYTICAL PROBLEM 3 4 8 8.6.1.2 INTRODUCTION 3 5 0
8.6.1.3 MATERIAL A N D METHODS 3 5 5 8.6.1.4 QUESTIONS 359
REFERENCES 3 5 9
8.6.2 DETERMINATION O F DISSOLVED OXYGEN (DO), PROJECT: "MONITORING THE
EFFICIENCY O F THE BIOLOGICAL STAGE IN A SEWAGE TREATMENT PLANT" 3 5 9
8.6.2.1 ANALYTICAL PROBLEM 359
8.6.2.2 INTRODUCTION 361 8.6.2.3 MATERIAL A N D METHODS 366 8.6.2.4
QUESTIONS 369
REFERENCES 369
8.7 UNIVERSAL SEPARATION METHODS 3 7 0
8.7.1 FIELD FLOW FRACTIONATION (FFF), PROJECT: "CHARACTERIZATION OF
NANOPARTICLES" 3 7 0 8.7.1.1 ANALYTICAL PROBLEM 3 7 0 8.7.1.2
INTRODUCTION 372 8.7.1.3 MATERIAL A N D METHODS 3 8 4
8.7.1.4 QUESTIONS 3 8 7
REFERENCES 3 8 7
APPENDIX A SELECTION O F RECOMMENDED SOURCES BY SUBJECT AREA 3 8 9
A.L GENERAL SOURCES 389
A . L . L ROMPP 389
A.L.2 WIKIPEDIA 389
A.L.3 CRC HANDBOOK O F CHEMISTRY A N D PHYSICS, DAVID R. LIDE (ED.) 3 8
9
A.1.4 MERCK INDEX: ENCYCLOPEDIA O F CHEMICALS, DRUGS A N D BIOLOGICALS 3
9 0 A.L.5 CHEMSPIDER 3 9 0
A.2 ANALYTICAL CHEMISTRY 3 9 0
A.2.1 ENCYCLOPEDIA O F ANALYTICAL CHEMISTRY, RA MEYERS (ED.), JOHN WILEY
& SONS LTD, CHICHESTER (2000) 3 9 0 A.2.2 OFFICIAL METHODS O F ANALYSIS,
ASSOCIATION O F T H E OFFICIAL ANALYTICAL CHEMISTS (1990) 3 9 0
A.3 INORGANIC A N D ORGANOMETALLIC CHEMISTRY 3 9 0 A.3.1 GMELIN HANDBOOK
O F INORGANIC CHEMISTRY 3 9 0 A.3.2 DICTIONARY O F INORGANIC (METALS A N
D ORGANIC) COMPOUNDS 391
IMAGE 8
A.4 CHEMICAL ENGINEERING/TECHNICAL CHEMISTRY/PROCESS
ENGINEERING 391 A.4.1 ULLMANN'S ENCYCLOPEDIA O F INDUSTRIAL CHEMISTRY
391 A.4.2 KIRK-OTHMER ENCYCLOPEDIA O F CHEMICAL TECHNOLOGY 391 A.5
CHEMICALS: DIRECTORY O F SUPPLIERS 391
A.5.1 DATABASES SUBJECT TO CHARGE 391 A.5.2 FREE ACCESS (SELECTION) 391
A.6 ORGANIC CHEMISTRY 3 9 2
A.6.1 SCIENCE O F SYNTHESIS ("HOUBEN-WEYL METHODS OF MOLECULAR
TRANSFORMATIONS, METHODS O F ORGANIC CHEMISTRY") 392 A.7
PHYSICO-CHEMICAL DATA 3 9 2
A.7.1 CRC HANDBOOK O F CHEMISTRY A N D PHYSICS 3 9 2 A.7.2
LANDOLT-BORNSTEIN NUMERICAL DATA A N D FUNCTIONAL RELATIONSHIPS I N
SCIENCE A N D TECHNOLOGY 3 9 2 A.7.3 TRC THERMODYNAMIC TABLES 3 9 3 A.8
POLYMERS A N D MATERIALS 393
A.8.1 DECHEMA MATERIALS TABLE 393 A.8.2 POLYMER HANDBOOK 393
A.9 SPECTRA 393
A.9.1 PRINTED DATA COLLECTIONS 393 A.9.2 ONLINE PRODUCTS REQUIRING A
LICENSE 3 9 4 A.9.3 FREE ACCESS ONLINE PRODUCTS 394 A.10 TOXICOLOGY A N
D SAFETY 394
APPENDIX B STATISTICAL TABLES 395
APPENDIX C OBLIGATORY DECLARATION FOR STUDENTS 399
APPENDIX D THE INTERNATIONAL SYSTEM O F UNITS (SI)-AND T H E "NEW SI"
401
APPENDIX E EVALUATION GUIDE FOR FORMAL REPORTS 413
APPENDIX F SAFETY IN T H E ANALYTICAL LABORATORY 425 F . L GENERAL
PRECAUTIONARY MEASURES 4 1 5
F . L . L MEASURES FOR PERSONAL PROTECTION 415
F.L.2 EYE PROTECTION 415
F.L.3 SKIN PROTECTION 416
F.1.4 PROTECTIVE CLOTHING 416
F.L.5 HEARING PROTECTION 416
F.L.6 RESPIRATORY PROTECTION 416
F.2 FIRST AID 4 1 7
F.2.1 RESCUE 4 1 7
F.2.2 ALERTING EMERGENCY PERSONNEL 4 1 8
IMAGE 9
F.2.3 TREATMENT O F UNCONSCIOUS VICTIM 4 1 8
F.2.4 BLEEDING W O U N D S 4 1 8
F.2.5 SHOCK 4 1 9
F.2.6 EYE INJURIES 4 1 9
F.2.7 BURNS 4 2 0
F.2.8 CAUSTIC BURNS 4 2 0
F.2.9 POISONING 4 2 0
F.3 WORKING WITH CHEMICALS 421
F.3.1 CHEMICALS 421
F.3.2 SOLVENTS 4 2 2
F.3.3 HANDLING O F GLASS A N D GLASS EQUIPMENT 423 F.3.4 ELECTRICAL
APPARATUS, HEATING SOURCES 423
F.3.5 FIRE PREVENTION 4 2 4
F.3.6 SOURCES 4 2 4
F.3.7 F U M E HOOD 4 2 4
F.4 CHEMICAL REACTIONS U N D E R INCREASED PRESSURE 4 2 4
F.4.1 CHEMICALS 425
F.4.2 APPARATUS 4 2 5
F.4.3 WORKING IN CLEAN ROOMS 4 2 5
F.4.3.1 GENERAL CONDUCT 426
F.4.3.2 HANDLING O F CHEMICALS 426 F.4.3.3 DEVICES 426
F.5 DISPOSAL O F CHEMICALS 4 2 7
F.5.1 ORGANIC CHEMICALS 4 2 7
F.5.2 INORGANIC CHEMICALS 4 2 8
F.6 GASES 4 3 0
F.6.1 COMPRESSED GAS BOTTLES WITH SMALL LEAK 4 3 0 F.6.2 COMPRESSED GAS
BOTTLE WITH LARGE LEAK 4 3 0
F.6.3 EXPLOSIVE, FLAMMABLE OR OXIDIZING MATERIALS THAT DEVELOP FLAMMABLE
GAS W H E N COMBINED WITH WATER 4 3 0
F.7 LIQUIDS 431
F.7.1 AQUEOUS 431
F.7.2 ORGANIC 431
F.7.3 MERCURY 431
F.8 WORKING WITH ELECTRICITY 431
F.8.1 GENERAL CONDUCT 4 3 2
F.9 WORKING WITH H I G H VOLTAGE 433
F.9.1 GENERAL FACTS 4 3 4
F.9.2 EXPERIMENTAL SETUP 4 3 4
F.9.3 OPERATION 4 3 4
F.10 HANDLING O F COMPRESSED GAS BOTDES A N D GAS 4 3 5
F.10.1 GENERAL FACTS 4 3 5
F.10.2 TRANSPORT 4 3 5
F.10.3 STORAGE 435
IMAGE 10
X I V | CONTENTS
F.10.4 VALVES A N D FITTINGS 435
F.10.5 AT THE PLACE O F USE 436
F . L L RISK A N D SAFETY PHRASES (R/S PHRASES) 436
F.12 G H S (GLOBALLY HARMONIZED SYSTEM O F CLASSIFICATION A N D LABELING
O F CHEMICALS) 443 F.12.1 PRINCIPLES O F THE GHS 443
F.13 G H S PICTOGRAMS 4 4 4
F.13.1 PRECAUTIONARY STATEMENTS 451
INDEX 4 5 7 |
| any_adam_object | 1 |
| author | Petrozzi, Sergio |
| author_GND | (DE-588)141141670 |
| author_facet | Petrozzi, Sergio |
| author_role | aut |
| author_sort | Petrozzi, Sergio |
| author_variant | s p sp |
| building | Verbundindex |
| bvnumber | BV040659704 |
| classification_rvk | VG 5100 VG 5150 |
| classification_tum | CHE 200f |
| ctrlnum | (OCoLC)823306961 (DE-599)DNB1024048160 |
| dewey-full | 543 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543 |
| dewey-search | 543 |
| dewey-sort | 3543 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| format | Book |
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| id | DE-604.BV040659704 |
| illustrated | Illustrated |
| indexdate | 2024-08-21T00:26:08Z |
| institution | BVB |
| isbn | 352732951X 9783527329519 9783527665891 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-025486485 |
| oclc_num | 823306961 |
| open_access_boolean | |
| owner | DE-91G DE-BY-TUM DE-858 DE-11 DE-92 DE-19 DE-BY-UBM |
| owner_facet | DE-91G DE-BY-TUM DE-858 DE-11 DE-92 DE-19 DE-BY-UBM |
| physical | XXIII, 467 S. Ill., graph. Darst. |
| publishDate | 2013 |
| publishDateSearch | 2013 |
| publishDateSort | 2013 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Petrozzi, Sergio Verfasser (DE-588)141141670 aut Practical instrumental analysis methods, quality assurance and laboratory management Sergio Petrozzi Weinheim Wiley-VCH 2013 XXIII, 467 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Instrumentelle Analytik (DE-588)4222592-9 gnd rswk-swf Instrumentelle Analytik (DE-588)4222592-9 s DE-604 Erscheint auch als Online-Ausgabe, EPUB 978-3-527-66591-4 Erscheint auch als Online-Ausgabe, MOBI 978-3-527-66590-7 Erscheint auch als Online-Ausgabe, PDF 978-3-527-66592-1 text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4071680&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025486485&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Petrozzi, Sergio Practical instrumental analysis methods, quality assurance and laboratory management Instrumentelle Analytik (DE-588)4222592-9 gnd |
| subject_GND | (DE-588)4222592-9 |
| title | Practical instrumental analysis methods, quality assurance and laboratory management |
| title_auth | Practical instrumental analysis methods, quality assurance and laboratory management |
| title_exact_search | Practical instrumental analysis methods, quality assurance and laboratory management |
| title_full | Practical instrumental analysis methods, quality assurance and laboratory management Sergio Petrozzi |
| title_fullStr | Practical instrumental analysis methods, quality assurance and laboratory management Sergio Petrozzi |
| title_full_unstemmed | Practical instrumental analysis methods, quality assurance and laboratory management Sergio Petrozzi |
| title_short | Practical instrumental analysis |
| title_sort | practical instrumental analysis methods quality assurance and laboratory management |
| title_sub | methods, quality assurance and laboratory management |
| topic | Instrumentelle Analytik (DE-588)4222592-9 gnd |
| topic_facet | Instrumentelle Analytik |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4071680&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025486485&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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