Syntheses of multinary lithium (oxo)nitridosilicates:
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
2012
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| Schlagworte: | |
| Online-Zugang: | kostenfrei http://d-nb.info/1025224183/34 https://nbn-resolving.org/urn:nbn:de:bvb:19-147249 Inhaltsverzeichnis |
| Beschreibung: | 152 S. Ill., graph. Darst. |
Internformat
MARC
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| 100 | 1 | |a Lupart, Saskia |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Syntheses of multinary lithium (oxo)nitridosilicates |c Saskia Lupart |
| 264 | 1 | |c 2012 | |
| 300 | |a 152 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |a München, Univ., Diss., 2012 | ||
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| 856 | 4 | 1 | |u http://edoc.ub.uni-muenchen.de/14724/ |x Verlag |z kostenfrei |3 Volltext |
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Datensatz im Suchindex
| _version_ | 1804149592819761152 |
|---|---|
| adam_text | IMAGE 1
TABLE O F CONTENTS
1 INTRODUCTION 1
2 LITHIUM ALKALINE-EARTH NITRIDOSILICATES 8
2.1 O V E R V I E W 8
2.2 T U N I N G THE DIMENSIONALITY O F NITRIDOSILICATES IN L I T H I U M
MELTS 1 3
2.2.1 INTRODUCTION 14
2.2.2 RESULTS AND DISCUSSION 14
2.2.3 CONCLUSION 2 0
2.2.4 EXPERIMENTAL SECTION 2 0
2.2.4.1 X - R A Y DIFFRACTION 2 0
2.2.4.2 SOLID-STATE M A S N M R 2 1
2.2.4.3 MICROANALYSIS 2 1
2.2.4.4 SYNTHESIS 21
2.2.5 REFERENCES 2 2
2.3 LI 4CAJSI2N6 A N D LI4SRVSI2N , - Q U A T E R N A R Y L I T H I U M
NITRIDOSILICATES W I T H ISOLATED
|SI 2N6] IONS 2 6
2.3.1 INTRODUCTION 2 7
2.3.2 RESULTS AND DISCUSSION 2 7
2.3.3 CONCLUSIONS 31
2.3.4 EXPERIMENTAL SECTION 31
2.3.4.1 SYNTHESIS 31
2.3.4.2 X - R A Y DIFFRACTION 3 2
2.3.4.3 MICROANALYSIS 3 2
2.3.5 REFERENCES 3 3
2.4 LICA 3SI2N5 - A LITHIUM NITRIDOSILICATE W I T H A |SI2N5) 7
DOUBLE-CHAIN 3 4
2.4.1 INTRODUCTION 3 5
2.4.2 RESULTS AND DISCUSSION 3 5
2.4.2.1 CRYSTAL STRUCTURE DESCRIPTION 3 5
2.4.2.2 LATTICE ENERGY CALCULATIONS ACCORDING TO THE M A P L E CONCEPT 3
9
2.4.2.3 SOLID-STATE M A S N M R 4 0
2.4.3 CONCLUSIONS 4 2
2.4.4 EXPERIMENTAL SECTION 4 2
2.4.4.1 SYNTHESIS 4 2
2.4.4.2 CHEMICAL ANALYSES 4 3
2.4.4.3 SINGLE CRYSTAL X - R A Y ANALYSIS 4 3
2.4.4.4 X - R A Y P O W D E R DIFFRACTION 4 3
2.4.4.5 SOLID-STATE M A S N M R 4 4
2.4.5 REFERENCES 4 4
HTTP://D-NB.INFO/1026449340
IMAGE 2
TABLE O F CONTENTS
2.5 LI2SR4[SI2NS]N - A L A Y E R E D L I T H I U M NITRIDOSILICATE
NITRIDE 4 6
2.5.1 INTRODUCTION 4 7
2.5.2 RESULTS AND DISCUSSION 4 8
2.5.2.1 SYNTHETICAL A P P R O A C H 4 8
2.5.2.2 D A T A COLLECTION 4 8
2.5.2.3 CRYSTAL STRUCTURE DESCRIPTION 4 9
2.5.2.4 LATTICE E N E R G Y CALCULATIONS ACCORDING TO THE M A P L E
CONCEPT 5 2
2.5.2.5 D F T CALCULATIONS 5 5
2.5.2.6 COMPARISON BETWEEN LATTICE ENERGY CALCULATIONS A N D D F T
CALCULATIONS 5 6
2.5.3 CONCLUSIONS 56
2.5.4 EXPERIMENTAL SECTION 57
2.5.4.1 SYNTHESIS 5 7
2.5.4.2 CHEMICAL ANALYSES 5 9
2.5.4.3 SINGLE CRYSTAL X - R A Y ANALYSIS 5 9
2.5.4.4 COMPUTATIONAL METHODS 5 9
2.5.5 REFERENCES 6 0
3 LITHIUM RARE-EARTH NITRIDOSILICATES 63
3.1 O V E R V I E W 6 3
3.2 C H A I N - T Y P E L I T H I U M RARE-EARTH NITRIDOSILICATES -
LISLNSSUNN WITH L N = L A , C E . 6 7
3.2.1 INTRODUCTION 6 8
3.2.2 RESULTS AND DISCUSSION 6 9
3.2.2.1 SYNTHETICAL APPROACH 6 9
3.2.2.2 CRYSTAL STRUCTURE 70
3.2.2.3 SOLID-STATE M A S N M R 75
3.2.2.4 LATTICE ENERGY CALCULATIONS ACCORDING TO THE M A P L E CONCEPT
76
3.2.3 CONCLUSIONS 77
3.2.4 EXPERIMENTAL SECTION 77
3.2.4.1 SYNTHESIS 77
3.2.4.2 CHEMICAL ANALYSES 78
3.2.4.3 SINGLE CRYSTAL X - R A Y ANALYSIS 78
3.2.4.4 X - R A Y P O W D E R DIFFRACTION 79
3.2.4.5 SOLID-STATE M A S N M R 8 0
3.2.5 REFERENCES 81
3.3 LILA 5SI4NIOO A N D LIPR5SI4NI0O - C H A I N T Y P E
OXONITRIDOSILICATES 8 3
3.3.1 INTRODUCTION 84
3.3.2 RESULTS AND DISCUSSION 8 4
3.3.2.1 SYNTHESIS A N D CRYSTAL STRUCTURE 8 4
3.3.2.2 SOLID-STATE M A S N M R 8 8
IMAGE 3
TABLE O F CONTENTS
3.3.2.3 LATTICE ENERGY CALCULATIONS A C C O R D I N G TO THE M A P L E
CONCEPT 8 9
3.3.3 CONCLUSIONS 9 0
3.3.4 EXPERIMENTAL SECTION 91
3.3.4.1 SYNTHESIS 9 1
3.3.4.2 CHEMICAL ANALYSES 9 1
3.3.4.3 SINGLE CRYSTAL X - R A Y ANALYSIS 9 2
3.3.4.4 X - R A Y P O W D E R DIFFRACTION 9 2
3.3.4.5 SOLID-STATE M A S N M R 93
3.3.5 REFERENCES 9 4
3 . 4 LII 4LNS[SIUNI905]02F2 WITH L N = C E , N D - REPRESENTATIVES O F
A F A M I L Y O F POTENTIAL
L I T H I U M ION CONDUCTORS 9 6
3.4.1 INTRODUCTION 97
3.4.2 EXPERIMENTAL SECTION .-. 9 8
3.4.2.1 SYNTHESIS 9 8
3.4.2.2 CHEMICAL ANALYSIS 99
3.4.2.2 SINGLE CRYSTAL X - R A Y ANALYSIS 9 9
3.4.2.3 X - R A Y P O W D E R DIFFRACTION 100
3.4.2.4 ELECTRICAL CONDUCTIVITY MEASUREMENTS 101
3.4.3 RESULTS AND DISCUSSION 101
3.4.3.1 SYNTHESIS A N D CRYSTAL STRUCTURE 101
3.4.3.2 STRUCTURAL ANALYSIS O F POSSIBLE LITHIUM MIGRATION PATHWAYS 105
3.4.3.3 ELECTRICAL CONDUCTIVITY MEASUREMENTS 105
3.4.4 CONCLUSION 109
3.4.5 REFERENCES 109
3 . 5 LIJSLNSSIAONSOOIF W I T H L N = CE, P R - H I G H L Y C O N D E N
S E D NITRIDOSILICATES 112
3.5.1 INTRODUCTION 113
3.5.2 RESULTS AND DISCUSSION 114
3.5.2.1 CRYSTAL STRUCTURE DESCRIPTION 114
3.5.2.2 LATTICE ENERGY CALCULATIONS ACCORDING TO THE M A P L E CONCEPT
117
3.5.3 CONCLUSIONS 118
3.5.4 EXPERIMENTAL SECTION 119
3.5.4.1 SYNTHESES 119
3.5.4.2 X - R A Y DIFFRACTION 119
3.5.4.3 MICROANALYSIS 120
3.5.5 REFERENCES 120
4 OUTLOOK 122
5 SUMMARY 126
IMAGE 4
TABLE O F CONTENTS
6 APPENDIX 131
6.1 SUPPORTING INFORMATION FOR CHAPTER 2.2 131
6.2 SUPPORTING INFORMATION FOR CHAPTER 3.3 1 3 5
6.3 SUPPORTING INFORMATION FOR CHAPTER 3.4 1 3 7
6.4 SUPPORTING INFORMATION FOR CHAPTER 3.5 1 4 4
7 PUBLICATIONS 148
8 CURRICULUM VITAE 152
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| spelling | Lupart, Saskia Verfasser aut Syntheses of multinary lithium (oxo)nitridosilicates Saskia Lupart 2012 152 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier München, Univ., Diss., 2012 (DE-588)4113937-9 Hochschulschrift gnd-content Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:19-147249 http://edoc.ub.uni-muenchen.de/14724/ Verlag kostenfrei Volltext http://d-nb.info/1025224183/34 Langzeitarchivierung Nationalbibliothek https://nbn-resolving.org/urn:nbn:de:bvb:19-147249 Resolving-System DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=025360511&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Lupart, Saskia Syntheses of multinary lithium (oxo)nitridosilicates |
| subject_GND | (DE-588)4113937-9 |
| title | Syntheses of multinary lithium (oxo)nitridosilicates |
| title_auth | Syntheses of multinary lithium (oxo)nitridosilicates |
| title_exact_search | Syntheses of multinary lithium (oxo)nitridosilicates |
| title_full | Syntheses of multinary lithium (oxo)nitridosilicates Saskia Lupart |
| title_fullStr | Syntheses of multinary lithium (oxo)nitridosilicates Saskia Lupart |
| title_full_unstemmed | Syntheses of multinary lithium (oxo)nitridosilicates Saskia Lupart |
| title_short | Syntheses of multinary lithium (oxo)nitridosilicates |
| title_sort | syntheses of multinary lithium oxo nitridosilicates |
| topic_facet | Hochschulschrift |
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